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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 307 records · Page 17
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

Exchange-coupled Fe 3 O 4 /CoFe 2 O 4 nanoparticles for advanced magnetic hyperthermia

We report a systematic study of the effects of core and shell size on the magnetic properties and heating efficiency of exchange-coupled Fe 3 O 4 /CoFe 2 O 4 core/shell nanoparticles. The nanoparticles were synthesized using thermal decomposition of organometallic precursors. Transmission electron microscopy (TEM) confirmed the formation of spherical Fe 3 O 4 and Fe 3 O 4 /CoFe 2 O 4 nanoparticles. Magnetic measurements showed high saturation magnetization for the nanoparticles at room temperature. Increasing core diameter (6.4±0.7, 7.8±0.1, 9.6±1.2 nm) and/or shell thickness (~1, 2, 4 nm) increased the coercive field (H C ), while an optimal value of saturation magnetization (M S ) was achieved for the Fe 3 O 4 (7.8±0.1nm)/CoFe 2 O 4 (2.1±0.1nm) nanoparticles. Magnetic hyperthermia measurements indicated a large increase in specific absorption rate (SAR) for 8.2±1.1 nm Fe 3 O 4 /CoFe 2 O 4 compared to Fe 3 O 4 nanoparticles of same size. The SAR of the Fe 3 O 4 /CoFe 2 O 4 nanoparticles increased from 199 to 461 W/g for 800 Oe as the thickness of the CoFe 2 O 4 shell was increased from 0.9±0.5 to 2.1±0.1 nm. The SAR enhancement is attributed to a combination of the large M S and the large H C . Therefore, these Fe 3 O 4 /CoFe 2 O 4 core/shell nanoparticles can be a good candidate for advanced hyperthermia application.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2018

Modification of carbonyl iron particles by carboxyl-containing polydimethylsiloxanes

The possibility of preparing magnetic particles with the “core–shell” structure was demonstrated. The procedure is based on the treatment of carbonyl iron particles with polydimethylsiloxanes (PDMS) containing terminal or distributed over the chain carboxyl groups attached via the alkyl or aryl spacer. The presence of carboxyl-containing PDMS grafted to the surface of carbonyl iron particles was revealed by electron microscopy. Magnetorheological fluids and magnetic elastomers containing magnetic particles with the “core–shell” structure were obtained, and their rheological properties were studied.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Chemical assembly of the heteronuclear pivalate complex with the Li{sup I} and Fe{sup III} ions

The heteronuclear complex [Fe{sub 4}Li{sub 2}(O){sub 2}(Piv)10(H{sub 2}O){sub 2}] (1, Piv is the pivalic acid anion) was obtained by refluxing Fe{sup III} pivalates with Li{sup I} pivalates in toluene and isolated as the 1•PhCH{sub 3} solvate with a toluene molecule. According to X-ray diffraction data, complex 1 contains the {Fe_4Li_2O_2} core. The Mössbauer spectroscopy data indicate that the core comprises para magnetic Fe{sup III} ions in the high-spin state located in the symmetric octahedral environment of oxygen atoms. Thermolysis of 1 studied by simultaneous thermal analysis demonstrated thermal stability of the complex up to 225 °С. The main end product of thermolysis at 600 °С is the mixed oxide LiFe{sub 5}O{sub 8}.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Optimisation of confinement in a fusion reactor using a nonlinear turbulence model

We report the confinement of heat in the core of a magnetic fusion reactor is optimised using a multidimensional optimisation algorithm. For the first time in such a study, the loss of heat due to turbulence is modelled at every stage using first-principles nonlinear simulations which accurately capture the turbulent cascade and large-scale zonal flows. The simulations utilise a novel approach, with gyrofluid treatment of the small-scale drift waves and gyrokinetic treatment of the large-scale zonal flows. A simple near-circular equilibrium with standard parameters is chosen as the initial condition. The figure of merit, fusion power per unit volume, is calculated, and then two control parameters, the elongation and triangularity of the outer flux surface, are varied, with the algorithm seeking to optimise the chosen figure of merit. A twofold increase in the plasma power per unit volume is achieved by moving to higher elongation and strongly negative triangularity.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2014

Cryogenic performance of a cryocooler-cooled superconducting undulator

A cryocooler-cooled superconducting undulator has been installed and operated with beam at the Advanced Photon Source (APS) at Argonne National Laboratory (ANL). The device consists of a dual-core 42-pole magnet structure that is cooled to 4.2 K with a system of four cryocoolers operating in a zero-boil-off configuration. This effort represents the culmination of a development program to establish concept feasibility and evaluate cryostat design and cryocooler-based refrigeration. Cryostat performance is described including cool-down/warm-up, steady-state operation, cooling margin, and the impact of beam during operation in the APS storage ring. Plans for future devices with longer magnets, which will incorporate lessons learned from the development program, are also discussed.

43 PARTICLE ACCELERATORS↗
DOE OSTI2021

Electronic nature of chiral charge order in the kagome superconductor CsV 3 Sb 5

Kagome superconductors with T C up to 7 K have been discovered for over 40 y. Recently, unconventional chiral charge order has been reported in kagome superconductor KV 3 Sb 5 , with an ordering temperature of one order of magnitude higher than the T C . However, the chirality of the charge order has not been reported in the cousin kagome superconductor CsV 3 Sb 5 , and the electronic nature of the chirality remains elusive. In this paper, we report the observation of electronic chiral charge order in CsV 3 Sb 5 via scanning tunneling microscopy (STM). We observe a 2 × 2 charge modulation and a 1 × 4 superlattice in both topographic data and tunneling spectroscopy. 2 × 2 charge modulation is highly anticipated as a charge order by fundamental kagome lattice models at van Hove filling, and is shown to exhibit intrinsic chirality. We find that the 1 × 4 superlattices form various small domain walls, and can be a surface effect as supported by our first-principles calculations. Crucially, we find that the amplitude of the energy gap opened by the charge order exhibits real-space modulations, and features 2 × 2 wave vectors with chirality, highlighting the electronic nature of the chiral charge order. STM study at 0.4 K reveals a superconducting energy gap with a gap size 2Δ = 0.85 meV, which estimates a moderate superconductivity coupling strength with 2Δ/k B T C = 3.9. Furthermore, when further applying a c-axis magnetic field, vortex core bound states are observed within this gap, indicative of clean-limit superconductivity.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2023

Vortices in spin-0 superfluids carry magnetic flux

Vortices in spin-0 superfluids generically carry magnetic fields inside their cores, so that even neutral superfluid vortices may be thought of as magnetic flux tubes. We give a systematic analysis of this ‘vortex magnetic effect’ using effective field theory, clarifying earlier literature on the subject. Furthermore, our analysis shows that in superfluid helium-4 the vortex magnetic effect may be large enough to be experimentally detectable.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2017

Continuum Modeling of Inductor Hysteresis and Eddy Current Loss Effects in Resonant Circuits

This paper presents experimental validation of a high-fidelity toroid inductor modeling technique. The aim of this research is to accurately model the instantaneous magnetization state and core losses in ferromagnetic materials. Quasi–static hysteresis effects are captured using a Preisach model. Eddy currents are included by coupling the associated quasi-static Everett function to a simple finite element model representing the inductor cross sectional area. The modeling technique is validated against the nonlinear frequency response from two different series RLC resonant circuits using inductors made of electrical steel and soft ferrite. The method is shown to accurately model shifts in resonant frequency and quality factor. The technique also successfully predicts a discontinuity in the frequency response of the ferrite inductor resonant circuit.

Pries, Jason L.↗
DOE OSTI2024

Investigating Material Properties of Subsurface Rock Formations Modified by Engineering Mineral Precipitation (Final Scientific and Technical Report)

Montana State University’s (MSU) Energy Research Institute (ERI), in collaboration with the Center for Biofilm Engineering (CBE) and the Department of Civil Engineering (CE), has conducted a long‐term research program aimed at developing a novel cementing agent to address wellbore integrity and reduce the unwanted upward migration of fluids and greenhouse gases from the subsurface. The primary technology developed through this research program is known as ureolysis‐induced calcite precipitation (UICP), which harnesses bio‐chemical processes to precipitate calcium carbonate (CaCO 3 ). The same general process can also be called microbially-induced calcium carbonate precipitation (MICP) when microbes provide the process-catalyzing urease enzyme. Both terms are used in this report. Results have conclusively demonstrated that, if properly controlled, UICP can successfully seal fractures, high permeability zones, and compromised cement in the vicinity of wellbores and in nearby caprock. This technology has been successfully deployed to mitigate annular leakage in two test wells and over sixty commercial wells with a 100% success rate. This success in downhole deployment generates consideration of other subsurface applications where UICP could provide benefit to the energy sector, such as shale property modification for unconventional oil and gas recovery. The focus of this research project was to investigate fundamental material and mechanical properties of select shale cores and analyze how these properties change due to engineered mineral precipitation with the intent to control these properties to achieve a range of engineering objectives. Ultimately, the project aim was to identify valuable new areas where application of UICP might contribute to national energy security and environmental protection. The research workplan coupled UICP treatment of core samples, nuclear magnetic resonance (NMR) characterization, and mechanical strength testing at MSU with advanced X‐Ray micro-computed tomography (μCT) imaging and numerical modeling performed by collaborators at two national laboratories, the National Energy Technology Laboratory (NETL) and Lawrence Berkeley National Laboratory (LBNL). Experimental results are useful to inform geo-mechanical models which could be applied to predict mineralized rock formation behavior at field scale. Our findings suggest that NMR and μCT methods to detect and quantify biomineral formation in shale fractures are complementary and consistent with each other. Either could be used to estimate the volume of new mineral formed by UICP in shale fractures. The use of surfactants and guar gum to enhance biomineral precipitation in shale fractures merits further research. UICP can, under some conditions, increase the tensile strength of sealed shale fractures beyond that of the intact shale. These findings demonstrate that continued research in this area may be valuable to understanding and improving shale resource recovery techniques.

58 GEOSCIENCES↗
DOE OSTI2025

Stability and convergence of nuclear detonations in white dwarf collisions

We investigate the numerical stability of thermonuclear detonations in 1D accelerated reactive shocks and 2D binary collisions of equal-mass magnetized and unmagnetized white dwarf stars. To achieve high resolution at initiation sites, we devised geometric gridding and mesh velocity strategies specially adapted to the unique requirements of head-on collisional geometries, scenarios in which one expects maximum production of iron-group products. We study the effects of grid resolution and the limiting of temperature, energy, and reactants for different stellar masses, separations, magnetic fields, inigenerationtial compositions, detonation mechanisms, and limiter parameters across a range of cell sizes from 1 to 100 km. Our results set bounds on the parameter space of limiter amplitudes for which both temperature- and energy-limiting procedures yield consistent and monotonically convergent solutions. Within these bounds, we find that grid resolutions of 5 km or better are necessary for uncertainties in total released energy and iron-group products to drop below 10%. Intermediate-mass products (e.g., calcium) exhibit similar convergence trends but with somewhat greater uncertainty. These conclusions apply equally to pure C/O white dwarfs, multispecies compositions (including helium shells), magnetized and unmagnetized cores, and either single or multiple detonation scenarios.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

Influence of Viscosity on Dynamic Magnetization of Thermally Blocked Iron Oxide Nanoparticles Characterized by a Sensitive AC Magnetometer

In this work, we show that the viscosity of carrier liquid affects the dynamic magnetization of thermally blocked multi-core iron oxide nanoparticles. The core size of the nanoparticles was determined from the magnetization curve measured by a specially developed high-T{sub c} SQUID magnetometer and calculated to be 11.7 nm. Using an AC magnetometer developed based on induction coils, the dynamic magnetization of the multi-core iron oxide nanoparticle solution was measured from 3 Hz to 10.48 kHz. Later, we reconstructed of the hydrodynamic size distribution of the particles by assuming a log-normal distribution of particle size in an AC susceptibility model by Shliomis and Stepanov, which accounts for anisotropic directions of the easy axes of magnetic nanoparticles with respect to the excitation field direction. The reconstructed hydrodynamic sizes showed an average diameter of 130 nm and agreed with the size determined by dynamic light scattering method. In the case of increasing viscosity of the carrier liquids from 0.89 to 8.11 mPa s, the dynamic magnetization peaks of the imaginary component have shifted to a lower frequency region. We showed that the harmonics ratio and phase delay upon the magnetic field excitation at 30 Hz could also be used to determine the viscosity of carrier liquid independently.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2015

A Novel Transverse Flux Machine for Vehicle Traction Applications

A novel transverse flux machine topology for electric vehicle traction application using ferrite magnets is presented in this paper. The proposed transverse flux topology utilizes novel magnet arrangements in the rotor that are similar to Halbach-array to boost flux linkage; on the stator side, cores are alternately arranged around a pair of ring windings in each phase to make use of the entire rotor flux that eliminates end windings. Analytical design considerations and finite element methods are used for an optimized design of a scooter in-wheel motor. Simulation results from Finite Element Analysis (FEA) show the motor achieved comparable torque density to conventional rare-earth permanent magnet machines. This machine is a viable candidate for direct drive applications with low cost and high torque density.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2016

Effect of resonant magnetic perturbations on three dimensional equilibria in the Madison Symmetric Torus reversed-field pinch

The orientation of 3D equilibria in the Madison Symmetric Torus (MST) [R. N. Dexter et al., Fusion Technol. 19, 131 (1991)] reversed-field pinch can now be controlled with a resonant magnetic perturbation (RMP). Absent the RMP, the orientation of the stationary 3D equilibrium varies from shot to shot in a semi-random manner, making its diagnosis difficult. Produced with a poloidal array of saddle coils at the vertical insulated cut in MST's thick conducting shell, an m = 1 RMP with an amplitude b{sub r}/B ∼ 10% forces the 3D structure into any desired orientation relative to MST's diagnostics. This control has led to improved diagnosis, revealing enhancements in both the central electron temperature and density. With sufficient amplitude, the RMP also inhibits the generation of high-energy (>20 keV) electrons, which otherwise emerge due to a reduction in magnetic stochasticity in the core. Field line tracing reveals that the RMP reintroduces stochasticity to the core. A m = 3 RMP of similar amplitude has little effect on the magnetic topology or the high-energy electrons.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2024

High Pressure Melting Curve of Fe‐Si: Implication for the Thermal Properties in Mercury's Core

The motion of liquid iron (Fe) alloy materials in the outer core drives the dynamo, which generates Mercury's magnetic field. The assessment of core models requires laboratory measurements of the melting temperature of Fe alloys at high pressure. Here, we experimentally determined the melting curve of Fe9wt%Si and Fe17wt%Si up to 17 GPa using in situ and ex situ measurements of intermetallic fast diffusion that serves as the melting criterion in a large-volume press. Our determined melting slopes are comparable with previous studies up to about 17 GPa. However, when extrapolated, our melting slopes significantly deviate from previous studies at higher pressures. For Mercury's core with a model composition of Fe9wt%Si, the melting temperature-depth profile determined in our study is lower by ∼150–250 K when compared with theoretical calculations. Using the new melting curve of Fe9wt%Si and the electrical resistivity values from a previous study of Fe8.5wt%Si, we estimate that the electronic thermal conductivity of liquid Fe9wt%Si is 30 Wm −1 K −1 at the Mercury's CMB pressure of 5 GPa and 37 Wm −1 K −1 at an assumed ICB of 21 GPa, corresponding to heat flux values of 23 mWm −2 and 32 mWm −2 , respectively. These values provide new constraints on the core models.

58 GEOSCIENCES↗
DOE OSTI2015

Magnetic field directed assembly of superstructures of ferrite-ferroelectric core-shell nanoparticles and studies on magneto-electric interactions

Composites of ferromagnetic and ferroelectric are of interest for studies on mechanical strain mediated magneto-electric (ME) interactions and for useful technologies. Here, we report on magnetic-field-assisted-assembly of barium titanate (BTO)-nickel ferrite (NFO) core-shell particles into linear chains and 2D/3D arrays and measurements of ME effects in such assemblies. First, we synthesized the core-shell nano-particles with 50–600 nm BTO and 10–200 nm NFO by chemical self-assembly by coating the ferroic particles with complementary coupling groups and allowing them to self-assemble in the presence of a catalyst via the “click” reaction. The core-shell structure was confirmed with electron microscopy and scanning probe microscopy. We obtained superstructure of the core-shell particles by subjecting them to a magnetic field gradient that exerts an attractive force on the particles and align them toward the regions of high field strengths. At low particle concentration, linear chains were formed and they evolved into 2D and 3D arrays at high particle concentrations. Magnetoelectric characterization on unassembled films and assembled arrays has been performed through measurements of low-frequency ME voltage coefficient (MEVC) by subjecting the sample to a bias magnetic field and an ac magnetic field. The MEVC is higher for field-assembled samples than for unassembled films and is found to be sensitive to field orientation with a higher MEVC for magnetic fields parallel to the array direction than for magnetic fields perpendicular to the array. A maximum MEVC of 20 mV/cm Oe, one of the highest reported for any bulk nanocomposite, is measured across the array thickness. A model is provided for ME coupling in the superstructures of BTO-NFO particulate composites. First, we estimated the MEVC for a free-standing BTO-NFO core-shell particle and then extended the model to include an array of linear chains of the particles. The theoretical estimates are in qualitative agreement with the data.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2018

Active Field Cancellation to Prevent Saturation in Ferromagnetic-Core Loop Antennas

Ferromagnetic-core loop antennas with high-permeability core materials are typically used in size-constrained applications requiring the detection and reception of weak very low frequency and extremely low frequency signals. However, high-permeability materials are susceptible to saturation in the presence of strong magnetic fields such as those generated by power lines, in research laboratories, or through natural phenomena. Here, a system is presented that actively controls the magnetic flux in the core of the antenna by applying a control signal to an independent set of windings on the same core. This control signal is phase locked to the offending signal and the two signals destructively combine in the core. Our results show that it is possible to actively cancel the fundamental component of a strong interferer in the core of a high sensitivity ferromagnetic-core loop antenna and prevent core saturation. This approach eliminates signal distortion caused by magnetic saturation that passive signal cancellation or signal processing in the receiver do not. Furthermore, high-sensitivity ferromagnetic-core antennas can be used in applications where they were previously thought unsuitable.

42 ENGINEERING↗
DOE OSTI2025

Search for axions from magnetic white dwarfs with Chandra x-ray observations

Low-mass axionlike particles could be produced in abundance within the cores of hot, compact magnetic white dwarf (MWD) stars from electron bremsstrahlung and converted to detectable x-rays in the strong magnetic fields surrounding these systems. In this work, we constrain the existence of such axions from two dedicated Chandra x-ray observations of ∼ 40 ks each in the energy range ∼ 1–10 keV toward the MWDs WD 1859 +148 and PG 0945 + 246. We find no evidence for axions, which constrains the axion-electron times axion-photon coupling to |𝑔 𝑎⁢𝛾⁢𝛾 ⁡𝑔 𝑎⁢𝑒⁢𝑒 | ≲ 1.54 ×10 −25 (3.54 × 10 −25 ) GeV −1 for PG 0945 + 246 (WD 1859 +148) at 95% confidence for axion masses 𝑚 𝑎 ≲ 10 −6 eV. Here, we find an excess of low-energy x-rays between 1 and 3 keV for WD 1859 + 148 but determine that the spectral morphology is too soft to arise from axions; instead, the soft x-rays may arise from nonthermal emission in the MWD magnetosphere.

Axions↗
DOE OSTI2014

Enhanced thermal stability of phosphate capped magnetite nanoparticles

We have studied the effect of phosphate capping on the high temperature thermal stability and magnetic properties of magnetite (Fe{sub 3}O{sub 4}) nanoparticles synthesized through a single-step co-precipitation method. The prepared magnetic nanoparticles are characterized using various techniques. When annealed in air, the phosphate capped nanoparticle undergoes a magnetic to non-magnetic phase transition at a temperature of 689 °C as compared to 580 °C in the uncoated nanoparticle of similar size. The observed high temperature phase stability of phosphate capped nanoparticle is attributed to the formation of a phosphocarbonaceous shell over the nanoparticles, which acts as a covalently attached protective layer and improves the thermal stability of the core material by increasing the activation energy. The phosphocarbonaceous shell prevents the intrusion of heat, oxygen, volatiles, and mass into the magnetic core. At higher temperatures, the coalescence of nanoparticles occurs along with the restructuring of the phosphocarbonaceous shell into a vitreous semisolid layer on the nanoparticles, which is confirmed from the small angle X-ray scattering, Fourier transform infra red spectroscopy, and transmission electron microscopy measurements. The probable mechanism for the enhancement of thermal stability of phosphocarbonaceous capped nanoparticles is discussed.

77 NANOSCIENCE AND NANOTECHNOLOGY↗