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293 records · Page 17
All sourcesNASA NTRSDOE OSTI
NASA NTRS1995

Cogenetic Rock Fragments from a Lunar Soil: Evidence of a Ferroan Noritic-Anorthosite Pluton on the Moon

The impact that produced North Ray Crater, Apollo 16 landing site, exhumed rocks that include relatively mafic members of the lunar ferroan anorthositic suite. Bulk and mineral compositions indicate that a majority of 2-4 mm lithic fragments from sample 67513, including impact breccias and monomict igneous rocks, are related to a common noritic-anorthosite precursor. Compositions and geochemical trends of these lithic fragments and of related samples collected along the rim of North Ray Crater suggest that these rocks derived from a single igneous body. This body developed as an orthocumulate from a mixture of cumulus plagioclase and mafic intercumulus melt, after the plagioclase had separated from any cogenetic mafic minerals and had become concentrated into a crystal mush (approximately 70 wt% plagioclase, 30 wt% intercumulus melt). We present a model for the crystallization of the igneous system wherein "system" is defined as cumulus plagioclase and intercumulus melt. The initial accumulation of plagioclase is analogous to the formation of thick anorthosites of the terrestrial Stillwater Complex; however, a second stage of formation is indicated, involving migration of the cumulus-plagioclase-intercumulus-melt system to a higher crustal level, analogous to the emplacement of terrestrial massif anorthosites. Compositional variations of the lithic fragments from sample 67513 are consistent with dominantly equilibrium crystallization of intercumulus melt. The highly calcic nature of orthocumulus pyroxene and plagioclase suggests some reaction between the intercumulus melt and cumulus plagioclase, perhaps facilitated by some recrystallization of cumulus plagioclase. Bulk compositions and mineral assemblages of individual rock fragments also require that most of the mafic minerals fortned in close contact with cumulus plagioclase, not as separate layers. The distribution of compositions (and by inference, modes) has a narrow peak at anorthosite and a broader, larger peak at noritic anoilhosite. Characteristics of the samples and their geochemical trends imply an origin in a system that was large relative to the (unknown) size of the impact that produced the breccias of ferroan noritic-anorthosite composition that were excavated later by the formation of North Ray Crater, and they appear to be consistent with an origin of the suite within a perched plagioclase cumulate. If the Moon's crust formed by accumulation of plagioclase in a magma ocean, ferroan noritic anothosite, formed as an orthocumulate, is an alternative to extensive adcumulus formation of ferroan anorthosite (greater than 90 vol% plagiclase). This provides a relatively mafic ferroan anorthositic component (approximately 15 vol% mafics), which is required by mass-balance models of compositions of polymict lunar-crustal materials. The inferred bulk composition of the system of cumulus plagioclase and intercumulus melt is similar to that of ferroan regolith breccia MacAlpine Hills 88104/5, a lunar-highland meteorite, and may represent a common and widespread component of the Moon's early highland crust.

Jolliff, B. L.↗
NASA NTRS1993

Heliocentric zoning of the asteroid belt by aluminum-26 heating

Variations in petrology among meteorites attest to a strong heating event early in solar system history, but the heat source has remained unresolved. Aluminum-26 has been considered the most likely high-energy, short-lived radionuclide (half-life 0.72 million years) since the discovery of its decay product - excess Mg-26 - in Allende CAI's. Furthermore, observation of relict Mg-26 in an achondritic clast and in feldspars within ordinary chondrites (3,4) provided strong evidence for live Al-26 in meteorite parent bodies and not just in refractory nebular condensates. The inferred amount of Al-26 is consistent with constraints on the thermal evolution of both ordinary and carbonaceous chondrite parent objects up to a few hundred kilometers in diameter. Meteorites can constrain the early thermal evolution of their parent body locations, provided that a link can be established between asteroid spectrophotometric signature and meteorite class. Asteroid compositions are heliocentrically distributed: objects thought to have experienced high metamorphic or even melting temperatures are located closer to the sun, whereas apparently unaltered or mildly heated asteroids are located farther away. Heliocentric zoning could be the result of Al-26 heating if the initial amount of the radionuclide incorporated into planetesimals was controlled by accretion time, which in turn varies with semimajor axis. Analytic expressions for planetary accretion may be integrated to given the time, tau, required for a planetesimal to grow to a specified radius: tau varies as a(sup n), where n = 1.5 to 3 depending on the assumptions about variations in the surface density of the planetesimal swarm. Numerical simulations of planetesimal accretion at fixed semimajor axis demonstrate that variations in accretion time among small planetesimals can be strongly nonlinear depending on the initial conditions and model assumptions. The general relationship with semimajor axis remains valid because it depends only on the initial orbit properties and distribution of the planesimal swarm. In order to demonstrate the basic dependence of thermal evolution on semimajor axis, we parameterized accretion time across the asteroid belt according to tau varies as a(sup n) and calculated the subsequent thermal history. Objects at a specified semimajor axis were assumed to have the same accretion time, regardless of size. We set the initial Al-26/Al-27 ratio = 6 x 10(exp -5) and treated n and tau(sub 0) at a(sub 0) = 3 AU as adjustable parameters. The thermal model included temperature-dependent properties of ice and rock (CM chondrite analog) and the thermodynamic effects of phase transitions.

Grimm, R. E.↗
NASA NTRSDate not supplied

Simulating Ordinary Chondrite (Tamdakht) Ablation at the Hypersonic Materials Environmental Test System (HyMETS) Facility.

NASA’s Science Mission Directorate (SMD) created the Asteroid Threat Assessment Project (ATAP) to inform decision-makers of risks associated with Potentially Hazardous Objects (PHOs), which may pose an existential threat to human civilization. ATAP assesses risk, in part, by developing analytical physics-based damage models which draw upon data collected during material property characterization efforts, entry simulations, hazard simulations, and ground-based arc-jet testing. Therefore, a pathfinder test campaign was con-ducted at the Hypersonic Materials Environmental Test System (HyMETS) at the NASA Langley Re-search Center to investigate the ablation mechanisms of an ordinary chondrite (Tamdakht H5) and a terrestrial analog (basalt). The HyMETS facility is a 400 kW constricted arc heater used to screen material performance under simulated aerothermal conditions of hypersonic flow.1 Facility conditions were chosen to simulate Earth entry conditions be-tween the upper-mesosphere and the lower thermo-sphere. The ablation mechanisms of Tamdakht and bas-alt are illustrated with still images collected from high-speed video cameras (fig. 1, Tamdakht). Tamdakht produces a relatively stable melt flow, as evidenced by the perpetual growth of a flange at the sidewall and the exiguous detachment of molten material into the flow. Furthermore, an inspection of high-speed video and chemical analysis of the post-test melt layer suggests that the dominant mode of mass loss for Tamdakht, at these test conditions, is expressed through the vaporization of volatiles (e.g., iron, potassium, sodium, phosphorus, and sulfur). The vaporization rates of Tamdakht are greater than basalt under the most extreme test conditions, which leads to an enhanced blowing layer, in-creased thermal shielding, and reduced recession. The ablation mechanisms of basalt are markedly different from Tamdakht and are attributed to the presence of hydrated minerals dispersed at irregular intervals throughout the silicate matrix. Rapid de-composition of secondary minerals and the subsequent formation of water lead to the ejection of the subsurface and overlying melt layer. Furthermore, the presence of water is suspected of lowering the viscosity of the melt layer resulting in increased mass loss near the edge of the test article where drag forces overcome rheological properties (fig. 1, bas-alt). Finally, the results will be discussed in the broader context of meteorite-based material response model development and the potential impact on the Asteroid Threat Assessment Project (ATAP).

Brody K. Bessire↗
NASA NTRS2010

Oxidation States of Grim Glasses in EET79001 Based on Vanadium Valence

Gas-rich impact-melt (GRIM) glasses in SNC meteorites are very rich in Martian atmospheric noble gases and sulfur suggesting a possible occurrence of regolith-derived secondary mineral assemblages in these samples. Previously, we have studied two GRIM glasses, 506 and 507, from EET79001 Lith A and Lith B, respectively, for elemental abundances and spatial distribution of sulfur using EMPA (WDS) and FE-SEM (EDS) techniques and for sulfur-speciation using K-edge XANES techniques. These elemental and FE-SEM micro-graph data at several locations in the GRIM glasses from Shergotty (DBS), Zagami 994 and EET79001, Lith B showed that FeO and SO3 are positively correlated (SO3 represents a mixture of sulfide and sulfate). FE-SEM (EDS) study revealed that the sulfur-rich pockets in these glasses contain numerous micron-sized iron-sulfide (Fe-S) globules sequestered throughout the volume. However, in some areas (though less frequently), we detected significant Fe-S-O signals suggesting the occurrence of iron sulfate. These GRIM glasses were studied by K-edge microXANES techniques for sulfur speciation in association with iron in sulfur-rich areas. In both samples, we found the sulfur speciation dominated by sulfide with minor oxidized sulfur mixed in with various proportions. The abundance of oxidized sulfur was greater in 506 than in 507. Based on these results, we hypothesize that sulfur initially existed as sulfate in the glass precursor materials and, on shock-impact melting of the precursor materials producing these glasses, the oxidized sulfur was reduced to predominately sulfide. In order to further test this hypothesis, we have used microXANES to measure the valence states of vanadium in GRIM glasses from Lith A and Lith B to complement and compare with previous analogous measurements on Lith C (note: 506 and 507 contain the largest amounts of martian atmospheric gases but the gas-contents in Lith C measured by are unknown). Vanadium is ideal for addressing this re-dox issue because it has multiple valence states and is a well-studied element. Ferrous-dominated iron valences determined by microXANES on the Lith A and Lith B glasses provide little redox sensitivity. Vanadium valence measurements for impact glass in Lith C at three different locations yielded valence values of 3.1, 3.2 and 3.4 with inferred fO2 values of IW-0.7, IW-0.1 and IW+0.7, respectively. This range of oxygen-fugacity values is understandable because the glasses are shock-molten impact glasses which are heterogeneous in nature. Oxygen fugacity values obtained from the analysis of Fe-Ti oxides and Eu partitioning in pyroxenes from EET79001 Lith A and Lith B (host lithologies) were in the range of IW+0.3 to IW+1.9 suggesting that V in the Lith C impact glass was reduced in the impact process. Here, we examine whether the 506 from Lith A and 507 from Lith B GRIM glasses yield similar or different fO2 values from those of Lith C using the vanadium K-edge microXANES technique.

Sutton, S. R.↗
NASA NTRS1997

Constraints on the Nature and Distribution of Iridium Host Phases at the Cretaceous-Tertiary Boundary: Implications for Projectile Identity and dispersal on impact

Among Cretaceous-Tertiary boundary sites worldwide, variations in the concentrations and ratios of elements commonly enriched in meteorites complicate traditional geochemical attempts at impactor identification. Yet they may provide constraints on the physical and chemical processes associated with large-body disruption and dispersal, as well as with diagenesis of projectile components. To this end, we continue our efforts to identify the mineral host-phases of projectile-derived elements, particularly for Ir, and to document their partitioning between crater deposits and ejecta resulting from the Chicxulub basin-forming impact. Building on earlier work, we used INAA to measure Ir concentrations in successively smaller splits of finely powdered impact melt breccia from the Chicxulub Crater in Mexico (sample Y6Nl9-R(b)), and K/T boundary fish clay from Stevns Klint, Denmark (sample FC-1, split from 40 kg of homogenized material intended as an analytical standard). Results for the Chicxulub sample show a heterogeneous Ir distribution and document that at least five discrete Ir-bearing host phases were isolated in subsequent splits, having Ir masses equivalent to pure Ir spheres from about 0.8 to about 3.5 mm in diameter. Three of these are within a sufficiently reduced mass of powder to warrant searching for them using backscattered electron microscopy. In contrast, successively smaller splits of the Stevns Klint fish clay show no statistically significant deviation from the reported value of 32 +/- 2 ng/g Ir, suggesting a uniform Ir host-phase distribution. For the smallest split obtained thus far (100 +/- 40 ng/g Ir), a pure Ir sphere of equivalent Ir mass would be <0.05 min in diameter. (n.b. Although homogenizing and sieving of FC-1 to <75 min obviously obscured variations in stratigraphic distribution, it is unlikely to have affected the size-frequency distribution of Ir host phases.) We previously identified micrometer-scale Ir host phases by electron microscopy in melt-rock samples from two widely separated drill holes at the Chicxulub Basin, including a replicate split of Y6-NI9-R. One is an aggregate of subhedral Ir metal grains enclosed in silicate, in which no other Pt group elements (PGE) were detected. A second particle with twice the mass as the first, concentrated predominantly in a single grain, is associated with minor concentrations of Os, Ru, and Pt, and with adhering particles of corundum and perovskite. A third Ir-rich particle, with a greater apparent Os concentration, was identified before being lost as a result of charging under the electron beam. In addition to demonstrating the preservation of projectile components within the Chicxulub Crater, analogous phase associations in Ca- and Al-rich inclusions (CAI) from C2 and C3 chondrites suggest to us that these melt-rock Ir host phases are relics from a carbonaceous chondrite K/T boundary impactor Although the obviously low Ru/Ir ratios of the Chicxulub Ir host phases are qualitatively consistent with suggested PGE fractionation with distance during condensation in an ejecta cloud, it seems difficult to explain the accumulation of the about 3 x 10(exp 11) Ir atoms required to form a about 10(exp -10) g nugget of pure Ir metal within a jet of vaporized projectile expanding at 1-4 km/s, or to effectively exclude or remove commonly alloyed PGE and siderophile elements by fractionation processes resulting from condensation, oxidation, sulfidization, exsolution, or autometamorphism during cooling of the melt. We do not dismiss the importance of these processes entirely; on the contrary, other geochemical and mineralogical aspects of the melt rocks require them, and condensation from the expanding ejecta cloud appears to best explain the primary Ir host-phase distribution in the fish clay, as well as the high Ir concentrations associated with spinel-bearing spheroids at the K/T boundary in the Pacific Ocean . If the "relict" hypothesis is correct, micronuggets of other PGEs and alloys, not detected by our INAA screening, should also occur in the melt rocks. Possibly, the discrete host phases with lesser Ir masses are such alloys with subordinate Ir, rather than simply smaller, predominantly Ir-bearing particles. A CAI source for the relics would be consistent with either a comet or an asteroid K/T impact at Chicxulub. (Additional information contained in the original.)

Schuraytz, B. C.↗