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NASA NTRS2005

Compositions of Three Lunar Meteorites: Meteorite Hills 01210, Northeast Africa 001, and Northwest Africa 3136

We report on compositions obtained by instrumental neutron activation analysis on three new lunar meteorites, MET 01210 (Meteorite Hills, Antarctica; 23 g), NEA 001 (Northeast Africa, Sudan; 262 g), and NWA 3136 (Northwest Africa, Algeria or Morocco; 95 g). As in previous similar studies, we divided our samples into many (8-9) small (approximately 30 mg) subsamples prior to analysis.

Korotev, R. L.↗
NASA NTRS2005

Method for Determination of Less Than 5 ppm Oxygen in Sodium Samples

Alkali metals used in pumped loops or heat pipes must be sufficiently free of nonmetallic impurities to ensure long heat rejection system life. Life issues are well established for alkali metal systems. Impurities can form ternary compounds between the container and working fluid, leading to corrosion. This Technical Memorandum discusses the consequences of impurities and candidate measurement techniques to determine whether impurities have been reduced to suf.ciently low levels within a single-phase liquid metal loop or a closed two-phase heat transfer system, such as a heat pipe. These techniques include the vanadium wire equilibration, neutron activation analysis, plug traps, distillation, and chemical analysis. Conceptual procedures for performing vanadium wire equilibration purity measurements on sodium contained in a heat pipe are discussed in detail.

Reid, R. S.↗
NASA NTRS2009

Sulfur Speciation in the Martian Regolith Component in Shergottite Glasses

We have shown that Gas-Rich Impact-Melt (GRIM) glasses in Shergotty, Zagami, and EET79001 (Lith A and Lith B) contain Martian regolith components that were molten during impact and quenched into glasses in voids of host rock materials based on neutron-capture isotopes, i.e., Sm-150 excesses and Sm-149 deficits in Sm, and Kr-80 excesses produced from Br [1, 2]. These GRIM glasses are rich in S-bearing secondary minerals [3.4]. Evidence for the occurrence of CaSO4 and S-rich aluminosilicates in these glasses is provided by CaO-SO3 and Al2O3-SO3 correlations, which are consistent with the finding of gypsum laths protruding from the molten glass in EET79001 (Lith A) [5]. However, in the case of GRIM glasses from EET79001 (Lith B), Shergotty and Zagami, we find a different set of secondary minerals that show a FeO-SO3 correlation (but no MgOSO3 correlation), instead of CaO-SO3 and Al2O3-SO3 correlations observed in Lith A. These results might indicate different fluidrock interactions near the shergottite source region on Mars. The speciation of sulfur in these salt assemblages was earlier studied by us using XANES techniques [6], where we found that Lith B predominantly contains Fe-sulfide globules (with some sulfate). On the other hand, Lith A showed predominantly Casulfite/ sulfate with some FeS. Furthermore, we found Fe to be present as Fe2+ indicating little oxidation, if any, in these glasses. To examine the sulfide-sulfate association in these glasses, we studied their Fe/Ni ratios with a view to find diagnostic clues for the source fluid. The Fe-sulfide mineral (Fe(0.93)Ni(0.3)S) in EET79001, Lith A is pyrrhotite [7, 8]. It yields an Fe/Ni ratio of 31. In Shergotty, pyrrhotite occurs with a molar ratio of Fe:S of 0.94 and a Ni abundance of 0.12% yielding a Fe/Ni ratio of approx.500 [8]. In this study, we determined a NiO content of approx.0.1% and FeO/NiO ratio of approx.420 in S-rich globules in #507 (EET79001, Lith B) sample using FE-SEM. In the same sample (bulk), using EMPA, we determined a FeO/NiO ratio of approx.700 (raster mode). Using similar techniques, we determined a NiO content of approx.0.015% and a FeO/NiO ratio of approx.800 in #506 (EET79001, Lith A). Moreover, a NiO content of approx.150 ppm and 6.1% FeO were found in Lith A GRIM glasses using neutron activation analysis [9] yielding a FeO/NiO ratio of approx.420. The FeO/NiO ratios in secondary mineral phases in S-rich pockets of EET79001 (Lith A/B) and Shergotty are high (approx.400) compared to the FeO/NiO ratio of 31 in Lith A pyrrhotite. These results suggest similar kind of fluids interacted with different rock materials to yield the observed variations in GRIM glasses in EET79001 Lith A and B.

Rao, M. N.↗
NASA NTRS2023

The UCLA Cosmochemistry Database

The UCLA Cosmochemistry Database was initiated as part of a data-rescue and -storage project aimed at archiving a variety of cosmochemical data acquired at University of California, Los Angeles (UCLA). The data collection includes elemental compositions of extraterrestrial materials analyzed by UCLA cosmochemists over the last five decades. The analytical techniques include atomic absorption spectrometry (AAS) and neutron activation analysis (NAA) at UCLA. The data collection is stored on the Astromaterials Data System (Astromat). We provide both interactive tables and downloadable datasheets for users to access all data. The UCLA Cosmochemistry Database archives cosmochemical data that are essential tools for increasing our understanding of the nature and origin of extraterrestrial materials. Future studies can reference the data collection in the examination, analysis, and classification of newly acquired extraterrestrial samples.

Bidong Zhang↗
NASA NTRS2015

Neutron Spectrometer Prospecting in the Mojave Volatiles Project Analog Field Test

We know that volatiles are sequestered at the poles of the Moon. While we have evidence of water ice and a number of other compounds based on remote sensing, the detailed distribution, and physical and chemical form are largely unknown. Additional orbital studies of lunar polar volatiles may yield further insights, but the most important next step is to use landed assets to fully characterize the volatile composition and distribution at scales of tens to hundreds of meters. To achieve this range of scales, mobility is needed. Because of the proximity of the Moon, near real-time operation of the surface assets is possible, with an associated reduction in risk and cost. This concept of operations is very different from that of rovers on Mars, and new operational approaches are required to carry out such real-time robotic exploration. The Mojave Volatiles Project (MVP) was a Moon-Mars Analog Mission Activities (MMAMA) program project aimed at (1) determining effective approaches to operating a real-time but short-duration lunar surface robotic mission, and (2) performing prospecting science in a natural setting, as a test of these approaches. Here we describe some results from the first such test, carried out in the Mojave Desert between 16 and 24 October, 2014. The test site was an alluvial fan just E of the Soda Mountains, SW of Baker, California. This site contains desert pavements, ranging from the late Pleistocene to early-Holocene in age. These pavements are undergoing dissection by the ongoing development of washes. A principal objective was to determine the hydration state of different types of desert pavement and bare ground features. The mobility element of the test was provided by the KREX-2 rover, designed and operated by the Intelligent Robotics Group at NASA Ames Research Center. The rover-borne neutron spectrometer measured the neutron albedo at both thermal and epithermal energies. Assuming uniform geochemistry and material bulk density, hydrogen as either hydroxyl/water in mineral assemblages or as moisture will significantly enhance the return of thermalized neutrons. However, in the Mojave test setting there is little uniformity, especially in bulk material density. We find that lighter toned materials (immature pavements, bar and swale, and wash materials) have lower thermal neutron flux, while mature, darker pavements with the greatest desert varnish development have higher neutron fluxes. Preliminary analysis of samples from the various terrain types in the test area indicates a prevailing moisture content of 2-3 wt% H2O. However, soil mineralogy suggests that the welldeveloped Av1 soil horizon beneath the topmost dark pavement clast layer contains the highest clay content. Structural water (including hydroxyl) in these clays may explain the enhanced neutron albedo over dark pavements. On the other hand, surface and subsurface bulk density can also play a role in neutron albedo - lower density of materials found in washes, for example, can result in a reduction in neutron flux. Analysis is ongoing.

rover-borne neutron spectrometer↗
NASA NTRS2013

Neutron Absorption Measurements Constrain Eucrite-Diogenite Mixing in Vesta's Regolith

The NASA Dawn Mission s Gamma Ray and Neutron Detector (GRaND) [1] acquired mapping data during 5 months in a polar, low altitude mapping orbit (LAMO) with approx.460-km mean radius around main-belt asteroid Vesta (264-km mean radius) [2]. Neutrons and gamma rays are produced by galactic cosmic ray interactions and by the decay of natural radioelements (K, Th, U), providing information about the elemental composition of Vesta s regolith to depths of a few decimeters beneath the surface. From the data acquired in LAMO, maps of vestan neutron and gamma ray signatures were determined with a spatial resolution of approx.300 km full-width-at-half-maximum (FWHM), comparable in scale to the Rheasilvia impact basin (approx.500 km diameter). The data from Vesta encounter are available from the NASA Planetary Data System. Based on an analysis of gamma-ray spectra, Vesta s global-average regolith composition was found to be consistent with the Howardite, Eucrite, and Diogenite (HED) meteorites, reinforcing the HED-Vesta connection [2-7]. Further, an analysis of epithermal neutrons revealed variations in the abundance of hydrogen on Vesta s surface, reaching values up to 400 micro-g/g [2]. The association of high concentrations of hydrogen with equatorial, low-albedo surface regions indicated exogenic delivery of hydrogen by the infall of carbonaceous chondrite (CC) materials. This finding was buttressed by the presence of minimally-altered CC clasts in howardites, with inferred bulk hydrogen abundances similar to that found by GRaND, and by studies using data from Dawn s Framing Camera (FC) and VIR instruments [8-10]. In addition, from an analysis of neutron absorption, spatial-variations in the abundance of elements other than hydrogen were detected [2].

Prettyman, T. H.↗
NASA NTRS1972

Neutron die-away experiment for remote analysis of the surface of the moon and the planets, phase 3

Continuing work on the two die-away measurements proposed to be made in the combined pulsed neutron experiment (CPNE) for analysis of lunar and planetary surfaces is described. This report documents research done during Phase 3. A general exposition of data analysis by the least-squares method and the related problem of the prediction of variance is given. A data analysis procedure for epithermal die-away data has been formulated. In order to facilitate the analysis, the number of independent material variables has been reduced to two: the hydrogen density and an effective oxygen density, the latter being determined uniquely from the nonhydrogeneous elemental composition. Justification for this reduction in the number of variables is based on a set of 27 new theoretical calculations. Work is described related to experimental calibration of the epithermal die-away measurement. An interim data analysis technique based solely on theoretical calculations seems to be adequate and will be used for future CPNE field tests.

Mills, W. R.↗
NASA NTRS2003

Mid-Latitude Composition of Mars from Thermal and Epithermal Neutrons

Epithermal neutron data acquired by Mars Odyssey have been analyzed to determine global maps of water-equivalent hydrogen abundance. By assuming that hydrogen was distributed uniformly with depth within the surface, a map of minimum water abundance was obtained. The addition of thermal neutrons to this analysis could provide information needed to determine water stratigraphy. For example, thermal and epithermal neutrons have been used together to determine the depth and abundance of water-equivalent hydrogen of a buried layer in the south polar region. Because the emission of thermal neutrons from the Martian surface is sensitive to absorption by elements other than hydrogen, analysis of stratigraphy requires that the abundance of these elements be known. For example, recently published studies of the south polar region assumed that the Mars Pathfinder mean soil composition is representative of the regional soil composition. This assumption is partially motivated by the fact that Mars appears to have a well-mixed global dust cover and that the Pathfinder soil composition is representative of the mean composition of the Martian surface. In this study, we have analyzed thermal and epithermal neutron data measured by the neutron spectrometer subsystem of the gamma ray spectrometer to determine the spatial distribution of the composition of elements other than hydrogen. We have restricted our analysis to mid-latitude regions for which we have corrected the neutron counting data for variations in atmospheric thickness.

T H Prettyman↗
NASA NTRS2004

"Chiron": A Proposed Remote Sensing Prompt Gamma Ray Activation Analysis Instrument for a Nuclear Powered Prometheus Mission

Prompt Gamma Ray Activation Analysis (PGAA) from neutron capture is an important experimental method that yields information on the elemental abundance of target materials. Gamma ray analysis has been used in planetary exploration missions by taking advantage of the production of neutrons as a result of Galactic Cosmic Ray interaction within the planetary surfaces. The .gamma ray signal that can be obtained from the GCR production of neutrons is very low, so we seek a superior neutron source. NASA s Project Prometheus and the Dept. of Energy aim to develop a nuclear power system for planetary exploration. This provides us with a tremendous opportunity to harness the reactor as a source of neutrons that can be used for PGAA. We envision a narrow stream of neutrons from the reactor directed toward the surface of an asteroid or comet producing the prompt gamma ray signal for analysis. Under ideal conditions of neutron flux and spacecraft orbit, both the signal strength and the spatial resolution will improved by several orders of magnitude over previously missions.

Floyd, Samuel R.↗
NASA NTRS1976

Atmospheric neutrons

Additional calibrations of the University of California double-scatter neutron detector and additional analysis corrections lead to slightly changed neutron fluxes. The theoretical angular distributions of Merker (1975) are in general agreement with the reported experimental fluxes but do not give the peaks for vertical upward and downward moving neutrons. The theoretical neutron escape current is in agreement with the experimental values from 10 to 100 MeV. The experimental fluxes obtained agree with those of Kanbach et al. (1974) in the overlap region from 70 to 100 MeV.

Preszler, A. M.↗