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DOE OSTI2020

Opportunities and Challenges of High-Energy Lithium Metal Batteries for Electric Vehicle Applications

Lithium metal batteries have great advantages over state-of-the-art lithium ion batteries in terms of energy density and cost, which present huge opportunities for long-range and low-cost electric vehicles in the future. However, the automotive industry has critical requirements on specific characteristics of battery cells, including but not limited to cycle life, working temperature range, fast discharge–charge capability, volume change, safety, and so on. In this Focus Review, we discuss both the cell- and system-level requirements and challenges of high-energy-density lithium metal batteries for future electrical vehicle applications and highlight some recent key progress in these aspects. Furthermore, our main objective is to identify key strategies on how to solve these challenges and inspire more research and development effort to accelerate the practical applications of lithium metal batteries.

25 ENERGY STORAGE↗

DOE OSTI2023

R -Nb 2 O 5 has an ‘idealized’ V 2 O 5 structure and Wadsley–Roth-like structural stability during Li-ion battery cycling

The adoption of batteries across diverse applications requires electrode materials with a wider range of performance metrics, such as cost, safety, and material availability. Along the path to discovering new commercially viable materials, a fundamental understanding of chemical and atomic structure features that provide structural stability and effective ion transport is essential. In support of new understanding, we report the cycling behavior of metastable R-Nb 2 O 5 . R-Nb 2 O 5 adopts an ‘idealized’ V 2 O 5 structure, in which [NbO 6 ] octahedra alternate in edge- and corner-sharing resulting in ReO 3 -like slabs, whereas Wadsley–Roth materials have ReO 3 -like blocks, linked through edge-sharing octahedra at intersecting crystallographic shear planes. We find that this slab structure is stable during cycling, with minor atomic structure changes and cycling curves that are symmetric on discharge and charge, resembling the behavior of Wadsley–Roth materials more than other related materials, such as ReO 3 , V 2 O 5 , or Nb 3 O 7 F. Based on our findings, R-Nb 2 O 5 can serve as a ‘structural bridge’ between Wadsley–Roth block structures and V 2 O 5 , through which we can relate inter- and intra-polyhedral structures to cycling behavior and structural stability during cycling.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2024

Monte Carlo Perturbation Analysis of Fuel Temperature Variations in the MCNP Model of the Annular Core Research Reactor

The Annular Core Research Reactor (ACRR) Monte Carlo N-Particle (MCNP) model is used by ACRR reactor operators and experiment designers at Sandia National Laboratories for a variety of computational calculations ranging from reactor kinetics parameter estimates and safety analyses to experimental planning. To understand the dominant source of uncertainty within the MCNP model, perturbations in temperature were applied to individual ACRR MCNP fuel rods. Fuel rod temperatures were randomly sampled from a uniform distribution from operational temperatures to quantify temperature-related uncertainty effects. Stochastic mixing was used to blend the cross sections of the desired temperatures using the MCNP continuous and Thermal Neutron Scattering Treatment [S(α,β)] libraries in ENDF/B-VII.1. Furthermore, this uncertainty analysis produced a 640 row × 640 column correlation and covariance matrix of the neutron energy spectra. Positive covariance was produced around the 1-MeV region and the 0.2-eV region. Correlation was found in the thermal and fast energy regions, but no correlation was observed in the slowing-down energy region because interactions in this region are not dominated by fuel.

ACRR↗

DOE OSTI2024

Defining blood hematology reference values in female pig-tailed macaques ( Macaca nemestrina ) using the Isolation Forest algorithm

Background: Pig-tailed macaques (PTMs) are commonly used as preclinical models to assess antiretroviral drugs for HIV prevention research. Drug toxicities and disease pathologies are often preceded by changes in blood hematology. To better assess the safety profile of pharmaceuticals, we defined normal ranges of hematological values in PTMs using an Isolation Forest (iForest) algorithm. Methods: Eighteen female PTMs were evaluated. Blood was collected 1–24 times per animal for a total of 159 samples. Complete blood counts were performed, and iForest was used to analyze the hematology data to detect outliers. Results: Median, IQR, and ranges were calculated for 13 hematology parameters. From all samples, 22 outliers were detected. These outliers were excluded from the reference index. Conclusions: Using iForest, we defined a normal range for hematology parameters in female PTMs. This reference index can be a valuable tool for future studies evaluating drug toxicities in PTMs.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2022

Deterministic modelling of the SPERT IV reactor transients using the multi-physics capability of WIMS

The ANSWERS WIMS reactor physics code is being developed for whole core multi-physics modelling. The established neutronics capability for lattice calculations has recently been extended to be suitable for whole core modelling of Small Modular Reactors (SMRs). A whole core transport, SP3 or diffusion flux solution is combined with fuel assembly resonance shielding. An integrated thermal hydraulic solver permits temperature and density variations to feedback to the neutronics calculation. This capability can be applied to both steady state and time dependent transient problems. Nuclear reactor design and safety case development requires assessment of a range of reactor transients, to inform both normal operation limitations and accident scenario analysis. This paper presents new methodology developed in WIMS to couple the core neutronics to the integrated core thermal hydraulics solver for the simulation of reactor transients in whole core models. To support the validation of the multi-physics capability of WIMS, this capability has been applied to the reactivity insertion transient experiments performed in the plate fuelled SPERT-IV reactor. This study employs WIMS using the whole core solver MERLIN, which calculates the time-dependent flux distribution and magnitude, coupled to ARTHUR, which solves for the time-dependent thermal hydraulics solution, and provides thermal feedback via the cross sections generated by GEOM, which performs resonance shielding calculations and generates cross section data for the plate geometry. This spatial kinetics model, with dynamic cross section generation, allows for variations in the temperature and neutron flux profile with time.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

NASA NTRS1988

Post-Challenger evaluation of space shuttle risk assessment and management

As the shock of the Space Shuttle Challenger accident began to subside, NASA initiated a wide range of actions designed to ensure greater safety in various aspects of the Shuttle system and an improved focus on safety throughout the National Space Transportation System (NSTS) Program. Certain specific features of the NASA safety process are examined: the Critical Items List (CIL) and the NASA review of the Shuttle primary and backup units whose failure might result in the loss of life, the Shuttle vehicle, or the mission; the failure modes and effects analyses (FMEA); and the hazard analysis and their review. The conception of modern risk management, including the essential element of objective risk assessment is described and it is contrasted with NASA's safety process in general terms. The discussion, findings, and recommendations regarding particular aspects of the NASA STS safety assurance process are reported. The 11 subsections each deal with a different aspect of the process. The main lessons learned by SCRHAAC in the course of the audit are summarized.

Source record↗

NASA NTRS1993

Lunar science strategy: Exploring the Moon with humans and machines

Important scientific questions that can be addressed from the lunar surface are reviewed for a number of scientific disciplines. A successful strategy for human exploration of the Moon is outlined. It consists of several elements: thorough preparation; a means of extending the human reach; measurement of the mobility of both human and robotic components; and flexible technologies so as to be able to take the most effective path as successive decision points occur. Part of thorough preparation involves concurrent development of a set of science goals and objectives as well as a supporting information base; neither can evolve independently of the other. This matched set will drive the definition of missions and technologies used to satisfy the requirements of various science disciplines. No single site on the Moon will satisfy all requirements. Thus, global accessibility is a goal of the current Lunar and Mars Exploration Program science strategy. Human mobility on the surface is limited to a few kilometers without the use of vehicles. Unpressurized crew carrying rovers could take explorers to distances tens of kilometers from an outpost; the distance is primarily limited by health and safety concerns. Pressurized rovers could extend the range to hundreds of kilometers, but size, mass, and costs limit such vehicles to missions beyond current planning horizons. The establishment of several outposts instead of one would provide opportunities for effective use of the unique capabilities of humans. Extending the human reach to global dimensions may be accomplished through teleoperation or telepresence. The most effective mix of these techniques is a decision that will evolve as experience is gained on the surface. Planning and technology must be flexible enough to allow a variety of options to be selected.

Morrison, Donald A.↗

NASA NTRS1994

Environmental, Safety, and Health Considerations: Composite Materials in the Aerospace Industry

The Aerospace Industries Association, Suppliers of Advanced Composite Materials Association, and the National Aeronautics and Space Administration co-sponsored a conference on 'Environmental, Safety, and Health Considerations--Composite Materials in the Aerospace Industry.' The conference was held in Mesa, Arizona, on October 20-21, 1994. Seventeen papers were presented in four sessions including general information, safety, waste, and emissions from composites. Topics range from product stewardship, best work practice, biotransformation of uncured composite materials, to hazardous waste determination and offgassing of composite materials.

Chu, Huai-Pu↗

NASA NTRS1997

Existing and Required Modeling Capabilities for Evaluating ATM Systems and Concepts

ATM systems throughout the world are entering a period of major transition and change. The combination of important technological developments and of the globalization of the air transportation industry has necessitated a reexamination of some of the fundamental premises of existing Air Traffic Management (ATM) concepts. New ATM concepts have to be examined, concepts that may place more emphasis on: strategic traffic management; planning and control; partial decentralization of decision-making; and added reliance on the aircraft to carry out strategic ATM plans, with ground controllers confined primarily to a monitoring and supervisory role. 'Free Flight' is a case in point. In order to study, evaluate and validate such new concepts, the ATM community will have to rely heavily on models and computer-based tools/utilities, covering a wide range of issues and metrics related to safety, capacity and efficiency. The state of the art in such modeling support is adequate in some respects, but clearly deficient in others. It is the objective of this study to assist in: (1) assessing the strengths and weaknesses of existing fast-time models and tools for the study of ATM systems and concepts and (2) identifying and prioritizing the requirements for the development of additional modeling capabilities in the near future. A three-stage process has been followed to this purpose: 1. Through the analysis of two case studies involving future ATM system scenarios, as well as through expert assessment, modeling capabilities and supporting tools needed for testing and validating future ATM systems and concepts were identified and described. 2. Existing fast-time ATM models and support tools were reviewed and assessed with regard to the degree to which they offer the capabilities identified under Step 1. 3 . The findings of 1 and 2 were combined to draw conclusions about (1) the best capabilities currently existing, (2) the types of concept testing and validation that can be carried out reliably with such existing capabilities and (3) the currently unavailable modeling capabilities that should receive high priority for near-term research and development. It should be emphasized that the study is concerned only with the class of 'fast time' analytical and simulation models. 'Real time' models, that typically involve humans-in-the-loop, comprise another extensive class which is not addressed in this report. However, the relationship between some of the fast-time models reviewed and a few well-known real-time models is identified in several parts of this report and the potential benefits from the combined use of these two classes of models-a very important subject-are discussed in chapters 4 and 7.

Odoni, Amedeo R.↗

NASA NTRS2001

Keeping Cool in Extreme Heat

Through a partnership with Unitika Ltd., NASA's Langley Research Center created a foam based on high temperature resistant polyimide chemistry. Licensed non-exclusively to SORDAL, Inc., the low-density foam, named TEEK, can be processed into forms or used to fill structures such as honeycomb. TEEK offers superior insulation and support qualities, with heat and flame resistance abilities.TEEK is a practical selection for hull insulation in the shipbuilding industry, with numerous potential applications in aerospace applications, fire-resistant construction materials, and a wide range of consumer products that will improve safety and energy efficiency. Other opportunities are available in the areas of automotive coatings and sealants, electrical components, and recreational equipment. SORDAL has introduced its new product in several different forms, under the name "SOLREX". The company is developing a new product called SORDAL Paper(TM) that will be used in conjunction with the polyimide foam to offer thermal protection in various products, such as fire resistant garments and prosthetics.

Source record↗

NASA NTRS2007

NASA Dryden's UAS Service Capabilities

The vision of NASA s Dryden Flight Research Center is to "fly what others only imagine." Its mission is to advance technology and science through flight. Objectives supporting the mission include performing flight research and technology integration to revolutionize aviation and pioneer aerospace technology, validating space exploration concepts, conducting airborne remote sensing and science missions, and supporting operations of the Space Shuttle and the International Space Station. A significant focus of effort in recent years has been on Unmanned Aircraft Systems (UAS), both in support of the Airborne Science Program and as research vehicles to advance the state of the art in UAS. Additionally, the Center has used its piloted aircraft in support of UAS technology development. In order to facilitate greater access to the UAS expertise that exists at the Center, that expertise has been organized around three major capabilities. The first is access to high-altitude, long-endurance UAS. The second is the establishment of a test range for small UAS. The third is safety case assessment support.

Bauer, Jeff↗

NASA NTRS2008

Surface Landing Site Weather Analysis for NASA's Constellation Program

Altino, Karen M.↗

NASA NTRS2008

Surface Landing Site Weather Analysis for Constellation Program

Weather information is an important asset for NASA's Constellation Program in developing the next generation space transportation system to fly to the International Space Station, the Moon and, eventually, to Mars. Weather conditions can affect vehicle safety and performance during multiple mission phases ranging from pre-launch ground processing to landing and recovery operations, including all potential abort scenarios. Meteorological analysis is an important contributor, not only to the development and verification of system design requirements but also to mission planning and active ground operations. Of particular interest are the surface atmospheric conditions at both nominal and abort landing sites for the manned Orion capsule. Weather parameters such as wind, rain, and fog all play critical roles in the safe landing of the vehicle and subsequent crew and vehicle recovery. The Marshall Space Flight Center Natural Environments Branch has been tasked by the Constellation Program with defining the natural environments at potential landing zones. Climatological time series of operational surface weather observations are used to calculate probabilities of occurrence of various sets of hypothetical vehicle constraint thresholds, Data are available for numerous geographical locations such that statistical analysis can be performed for single sites as well as multiple-site network configurations. Results provide statistical descriptions of how often certain weather conditions are observed at the site(s) and the percentage that specified criteria thresholds are matched or exceeded. Outputs are tabulated by month and hour of day to show both seasonal and diurnal variation. This paper will describe the methodology used for data collection and quality control, detail the types of analyses performed, and provide a sample of the results that can be obtained,

Altino, Karen M.↗

NASA NTRS2010

A Comparison of Tropical Storm (TS) and Non-TS Gust Factors for Assessing Peak Wind Probabilities at the Eastern Range

Knowledge of peak wind speeds is important to the safety of personnel and flight hardware at Kennedy Space Center (KSC) and the Cape Canaveral Air Force Station (CCAFS), but they are more difficult to forecast than mean wind speeds. Development of a reliable model for the gust factor (GF) relating the peak to the mean wind speed motivated a previous study of GF in tropical storms. The same motivation inspired a climatological study of non-TS peak wind speed statistics without the use of GF. Both studies presented their respective statistics as functions of mean wind speed and height. The few comparisons of IS and non-TS GF in the literature suggest that the non-TS GF at a given height and mean wind speed are smaller than the corresponding TS GF. The investigation reported here converted the non-TS peak wind statistics mentioned above to the equivalent GF statistics and compared the results with the previous TS GF results. The advantage of this effort over all previously reported studies of its kind is that the TS and non-TS data are taken from the same towers in the same locations. That eliminates differing surface attributes, including roughness length and thermal properties, as a major source of variance in the comparison. The results are consistent with the literature, but include much more detailed, quantitative information on the nature of the relationship between TS and non-TS GF as a function of height and mean wind speed. In addition, the data suggest the possibility of providing an operational model for non-TS GF as a function of height and wind speed in a manner similar to the one previously developed for TS GF.

Merceret, Francis J.↗

NASA NTRS2014

Analyzing the Impacts of Natural Environments on Launch and Landing Availability for NASA's Exploration Systems Development Programs

The National Aeronautics and Space Administration (NASA) is developing new capabilities for human and scientific exploration beyond Earth orbit. Natural environments information is an important asset for NASA's development of the next generation space transportation system as part of the Exploration Systems Development (ESD) Programs, which includes the Space Launch System (SLS) and Multi-Purpose Crew Vehicle (MPCV) Programs. Natural terrestrial environment conditions - such as wind, lightning and sea states - can affect vehicle safety and performance during multiple mission phases ranging from pre-launch ground processing to landing and recovery operations, including all potential abort scenarios. Space vehicles are particularly sensitive to these environments during the launch/ascent and the entry/landing phases of mission operations. The Marshall Space Flight Center (MSFC) Natural Environments Branch provides engineering design support for NASA space vehicle projects and programs by providing design engineers and mission planners with natural environments definitions as well as performing custom analyses to help characterize the impacts the natural environment may have on vehicle performance. One such analysis involves assessing the impact of natural environments to operational availability. Climatological time series of operational surface weather observations are used to calculate probabilities of meeting/exceeding various sets of hypothetical vehicle-specific parametric constraint thresholds. Outputs are tabulated by month and hour of day to show both seasonal and diurnal variation. This paper will discuss how climate analyses are performed by the MSFC Natural Environments Branch to support the ESD Launch Availability (LA) Technical Performance Measure (TPM), the SLS Launch Availability due to Natural Environments TPM, and several MPCV (Orion) launch and landing availability analyses - including the 2014 Orion Exploration Flight Test 1 (EFT-1) mission.

Altino, Karen M.↗

NASA NTRS2014

Analyzing the Impacts of Natural Environments on Launch and Landing Availability for NASA's Eploration Systems Development Programs

NASA is developing new capabilities for human and scientific exploration beyond Earth orbit. Natural environments information is an important asset for NASA's development of the next generation space transportation system as part of the Exploration Systems Development Program, which includes the Space Launch System (SLS) and MultiPurpose Crew Vehicle (MPCV) Programs. Natural terrestrial environment conditions - such as wind, lightning and sea states - can affect vehicle safety and performance during multiple mission phases ranging from prelaunch ground processing to landing and recovery operations, including all potential abort scenarios. Space vehicles are particularly sensitive to these environments during the launch/ascent and the entry/landing phases of mission operations. The Marshall Space Flight Center (MSFC) Natural Environments Branch provides engineering design support for NASA space vehicle projects and programs by providing design engineers and mission planners with natural environments definitions as well as performing custom analyses to help characterize the impacts the natural environment may have on vehicle performance. One such analysis involves assessing the impact of natural environments to operational availability. Climatological time series of operational surface weather observations are used to calculate probabilities of meeting or exceeding various sets of hypothetical vehicle-specific parametric constraint thresholds.

Altino, Karen M.↗

NASA NTRS2014

Optical Multi-Gas Monitor Technology Demonstration on the International Space Station

The International Space Station (ISS) employs a suite of portable and permanently located gas monitors to insure crew health and safety. These sensors are tasked with functions ranging from fixed mass spectrometer based major constituents analysis to portable electrochemical sensor based combustion product monitoring. An all optical multigas sensor is being developed that can provide the specificity of a mass spectrometer with the portability of an electrochemical cell. The technology, developed under the Small Business Innovation Research program, allows for an architecture that is rugged, compact and low power. A four gas version called the Multi-Gas Monitor was launched to ISS in November 2013 aboard Soyuz and activated in February 2014. The portable instrument is comprised of a major constituents analyzer (water vapor, carbon dioxide, oxygen) and high dynamic range real-time ammonia sensor. All species are sensed inside the same enhanced path length optical cell with a separate vertical cavity surface emitting laser (VCSEL) targeted at each species. The prototype is controlled digitally with a field-programmable gate array/microcontroller architecture. The optical and electronic approaches are designed for scalability and future versions could add three important acid gases and carbon monoxide combustion product gases to the four species already sensed. Results obtained to date from the technology demonstration on ISS are presented and discussed.

Pilgrim, Jeffrey S.↗

DOE OSTI2021

DESIGN AND PROTOYPING OF A FISSILE-BEARING CHLORIDE SALT IRRADIATION EXPERIMENT

Limited data exists on the properties of irradiated fueled chloride-based salts for use in advanced nuclear reactors. The design and prototyping of a salt irradiation experiment is underway. Mechanical design will integrate the experiment into existing assemblies in TRIGA type cores. Neutronics modeling demonstrated how targeted power densities can be reached and provide insight on radionuclide source term generation within the experiment. Thermal-hydraulic and computational fluid dynamics (CFD) analysis indicated that temperature ranges in the salt can satisfy both safety and programmatic requirements. Initial prototyping tests provided confidence in the ability to extract the salt post-irradiation, and in the heater performance. Future planned prototyping will provide an integral assessment of the proposed design prior to insertion in the reactor.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗