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NASA NTRS2013

Properties of Cathodoluminescence for Cryogenic Applications of SiO2-based Space Observatory Optics and Coatings

Disordered thin film SiO2SiOx coatings undergoing electron-beam bombardment exhibit cathodoluminescence, which can produce deleterious stray background light in cryogenic space-based astronomical observatories exposed to high-energy electron fluxes from space plasmas. As future observatory missions push the envelope into more extreme environments and more complex and sensitive detection, a fundamental understanding of the dependencies of this cathodoluminescence becomes critical to meet performance objectives of these advanced space-based observatories. Measurements of absolute radiance and emission spectra as functions of incident electron energy, flux, and power typical of space environments are presented for thin (60-200 nm) SiO2SiOx optical coatings on reflective metal substrates over a range of sample temperatures (40-400 K) and emission wavelengths (260-5000 nm). Luminescent intensity and peak wavelengths of four distinct bands were observed in UVVISNIR emission spectra, ranging from 300 nm to 1000 nm. A simple model is proposed that describes the dependence of cathodoluminescence on irradiation time, incident flux and energy, sample thickness, and temperature.

electron-beam bombardment↗

NASA NTRS2014

Affordable Development and Optimization of CERMET Fuels for NTP Ground Testing

CERMET fuel materials for Nuclear Thermal Propulsion (NTP) are currently being developed at NASA's Marshall Space Flight Center. The work is part of NASA's Advanced Space Exploration Systems Nuclear Cryogenic Propulsion Stage (NCPS) Project. The goal of the FY12-14 project is to address critical NTP technology challenges and programmatic issues to establish confidence in the affordability and viability of an NTP system. A key enabling technology for an NCPS system is the fabrication of a stable high temperature nuclear fuel form. Although much of the technology was demonstrated during previous programs, there are currently no qualified fuel materials or processes. The work at MSFC is focused on developing critical materials and process technologies for manufacturing robust, full-scale CERMET fuels. Prototypical samples are being fabricated and tested in flowing hot hydrogen to understand processing and performance relationships. As part of this initial demonstration task, a final full scale element test will be performed to validate robust designs. The next phase of the project will focus on continued development and optimization of the fuel materials to enable future ground testing. The purpose of this paper is to provide a detailed overview of the CERMET fuel materials development plan. The overall CERMET fuel development path is shown in Figure 2. The activities begin prior to ATP for a ground reactor or engine system test and include materials and process optimization, hot hydrogen screening, material property testing, and irradiation testing. The goal of the development is to increase the maturity of the fuel form and reduce risk. One of the main accomplishmens of the current AES FY12-14 project was to develop dedicated laboratories at MSFC for the fabrication and testing of full length fuel elements. This capability will enable affordable, near term development and optimization of the CERMET fuels for future ground testing. Figure 2 provides a timeline of the development and optimization tasks for the AES FY15-17 follow on program.

Hickman, Robert R.↗

NASA NTRSDate not supplied

Computer Controlled High Vacuum Gas Purification and Analysis Line

Light stable isotope work requires the handling of gasses such a way that does not alter isotopic composition. To do this, there are a large number of analytical and experimental procedures which involve the use of a vacuum line, numerous “egg timers” and a human hand on a valve. Unfortunately, the human hand is inconsistent and inadvertent small, and commonly large, differences in timing can have a measurable effect on outcomes. We have constructed a computer controlled high-vacuum line to be used as an expandable platform for future experimental and analytical procedures. The vacuum line consists of an electropolished 316 stainless steel system of cryogenic u-traps partitioned by pneumatic valves. The code to operate the line has been developed using the LabView platform and will allow for automated timing, consistent valve opening speed and unattended operation of long analytical procedures. The aim of this project is to address a need in the light stable isotope laboratory for a general-purpose vacuum line for handling and manipulation of gasses. When combined with existing instrumentation it allows for a significant expansion of current analytical capabilities. The system allows for better handling of standards, gas conversion techniques and gas sample collection for interlaboratory comparisons. The basic structure of the line, automation hardware and software were chosen and designed to provide a base for future expansion of the system to incorporate new automated analytical techniques as laboratory instrumentation and analytical needs expand.

High vacuum↗

NASA NTRS1978

Variable-temperature cryogenic trap for the separation of gas mixtures

The paper describes a continuous variable-temperature U-shaped cold trap which can both purify vacuum-line combustion products for subsequent stable isotopic analysis and isolate the methane and ethane constituents of natural gases. The canister containing the trap is submerged in liquid nitrogen, and, as the gas cools, the gas mixture components condense sequentially according to their relative vapor pressures. After the about 12 min required for the bottom of the trap to reach the liquid-nitrogen temperature, passage of electric current through the resistance wire wrapped around the tubing covering the U-trap permits distillation of successive gas components at optimal temperatures. Data on the separation achieved for two mixtures, the first being typical vacuum-line combustion products of geochemical samples such as rocks and the second being natural gas, are presented, and the thermal behavior and power consumption are reported.

Des Marais, D. J.↗

NASA NTRS1990

Scattered-light scanner measurements of cryogenic liquid-jet breakup

The effect of highly turbulent Mach 1 gas flow and high thermal gradients on drop size measurements was investigated with a scattered light scanner. The instrument, developed at NASA-Lewis, was used to measure characteristic drop diameters or cyrogenic liquid sprays. By correcting for gas turbulence and thermal gradient affects, it was possible to obtain good reproducible data with the scattered light scanner. Tests were conducted primarily in the aerodynamic-stripping regime of liquid atomization and it was found that the loss of small droplets due to vaporization and dispersion had a marketed effect on drop size measurements. The nitrogen gas flow rate exponent of 1.33 is the same as that predicted by atomization theory for liquid jet breakup in high velocity gas flow. However, when the sprays were sampled farther downstream of the atomizer, at axial distances of 2.5 and 4.5 cm, the exponent for W sub n decreased 1.2 and 0.9, respectively. This was attributed to the loss of small droplets due to vaporization when values of downstream axial distances exceeded 1.3 cm.

Ingebo, Robert D.↗

NASA NTRS2011

Design of Multilayer Insulation for the Multipurpose Hydrogen Test Bed

Multilayer insulation (MLI) is a critical component for future, long term space missions. These missions will require the storage of cryogenic fuels for extended periods of time with little to no boil-off and MLI is vital due to its exceptional radiation shielding properties. Several MLI test articles were designed and fabricated which explored methods of assembling and connecting blankets, yielding results for evaluation. Insight gained, along with previous design experience, will be used in the design of the replacement blanket for the Multipurpose Hydrogen Test Bed (MHTB), which is slated for upcoming tests. Future design considerations are discussed which include mechanical testing to determine robustness of such a system, as well as cryostat testing of samples to give insight to the loss of thermal performance of sewn panels in comparison to the highly efficient, albeit laborious application of the original MHTB blanket.

Marlow, Weston A.↗

NASA NTRS2001

Detection and Characterization of Imperfections in Composite Pressure Vessels

The thermographic evaluation of composite structures for delaminations, disbonds, inclusions, porosity and microcracking has proven to be a valuable asset in the field of nondestructive testing. Coupling large area coverage, variable sensitivity and minimal surface contact with a photographic type image representation of structural anomalies; thermography has become a primary inspection method for composite structures. Thermography works well for locating both surface and subsurface defects in most composite systems ranging in thickness of up to 0.25 inch (0.64 cm) or more. The thermographic method for inspection of composite structures typically involves applying an external source of heat to the structure and then recording the changes in the surface heat profile manifested by embedded defects or by material property variations. If these temperature variations are large enough and an infrared camera with sufficient sensitivity is used, then the material or structural abnormality can be detected and referred back to its source. Interpreting the information given in a thermogram, can be a difficult task under ideal circumstances and extremely challenging in a real world setting. Variables including depth, thermal conductivity, orientation and size of the abnormality can all have a great influence on how its heat pattern will be seen by the imager. The work discussed in this paper illustrates how the microstructure of several commonly found defects in composite structures relate to their thermographic image counterpart. Two test cases are studied herein, including a large graphite/epoxy RP-1 fuel tank and a graphite composite cryogenic fuel feedline. The structures used in this study were designed to serve as manufacturing proof of concept specimens and to undergo hydroburst testing to verify manufacturing practices and structural design. Prior to hydrostatic testing the structures underwent 100% thermographic evaluation to ensure that no manufacturing or handling damage was present. Due to a large inclusion found in the feedline, it was pulled from service and dissected without performing the hydroproof The thermographic indications found in the RP-1 tank were below critical limits so it underwent a complete hydroproof loading series and finally a hydroburst. Following the hydroburst samples were cut from the tank in regions where thermography had located damage before the test. These regions were thermographically and then were cross-sectioned and photomicrographed.

Walker, James L.↗

NASA NTRS2009

Covariant C and O Isotope Trends in Arctic Carbonate Crusts and ALH 84001: Potential Biomarker or Indicator of Cryogenic Formation Environment?

This work seeks to use the chemical, isotopic, and mineralogical characteristics of secondary carbonate minerals produced during brief aqueous events to identify the conditions of the aqueous environment in which they formed. Liquid water near the surface of Mars is subject to either rapid freezing and/or evaporation. These processes are also active on Earth, and produce secondary minerals that have complex chemical, mineralogical, and isotopic textures and compositions that can include covariant relationships between Delta C-13 (sub VPDB) and delta O-18 (sub VSMOW). The extremely well studied four billion year old carbonates preserved in martian meteorite ALH 84001 also show covariant delta C-13 and delta O-18 compositions, but these variations are manifested on a micro-scale in a single thin section while the variation observed so far in terrestrial carbonates is seen between different hand samples.

Socki, Richard A.↗

NASA NTRS2011

Helium-Cooled Black Shroud for Subscale Cryogenic Testing

This shroud provides a deep-space simulating environment for testing scaled-down models of passively cooling systems for spaceflight optics and instruments. It is used inside a liquid-nitrogen- cooled vacuum chamber, and it is cooled by liquid helium to 5 K. It has an inside geometry of approximately 1.6 m diameter by 0.45 m tall. The inside surfaces of its top and sidewalls have a thermal absorptivity greater than 0.96. The bottom wall has a large central opening that is easily customized to allow a specific test item to extend through it. This enables testing of scale models of realistic passive cooling configurations that feature a very large temperature drop between the deepspace-facing cooled side and the Sun/Earth-facing warm side. This shroud has an innovative thermal closeout of the bottom wall, so that a test sample can have a hot (room temperature) side outside of the shroud, and a cold side inside the shroud. The combination of this closeout and the very black walls keeps radiated heat from the sample s warm end from entering the shroud, reflecting off the walls and heating the sample s cold end. The shroud includes 12 vertical rectangular sheet-copper side panels that are oriented in a circular pattern. Using tabs bent off from their edges, these side panels are bolted to each other and to a steel support ring on which they rest. The removable shroud top is a large copper sheet that rests on, and is bolted to, the support ring when the shroud is closed. The support ring stands on four fiberglass tube legs, which isolate it thermally from the vacuum chamber bottom. The insides of the cooper top and side panels are completely covered with 25- mm-thick aluminum honeycomb panels. This honeycomb is painted black before it is epoxied to the copper surfaces. A spiral-shaped copper tube, clamped at many different locations to the outside of the top copper plate, serves as part of the liquid helium cooling loop. Another copper tube, plumbed in a series to the top plate s tube, is clamped to the sidewall tabs where they are bolted to the support ring. Flowing liquid helium through these tubes cools the entire shroud to 5 K. The entire shroud is wrapped loosely in a layer of double-aluminized Kapton. The support ring s inner diameter is the largest possible hole through which the test item can extend into the shroud. Twelve custom-sized trapezoidal copper sheets extend inward from the support ring to within a few millimeters of the test item. Attached to the inner edge of each of these sheets is a custom-shaped strip of Kapton, which is aluminum- coated on the warm-facing (outer) side, and has thin Dacron netting attached to its cold-facing side. This Kapton rests against the test item, but the Dacron keeps it from making significant thermal contact. The result is a non-contact, radiatively reflective thermal closeout with essentially no gap through which radiation can pass. In this way, the part of the test item outside the shroud can be heated to relatively high temperatures without any radiative heat leaking to the inside.

Tuttle, James↗

NASA NTRS2005

Nonflammable, Hydrophobic Aerogel Composites for Insulation

Aerogel composites that are both nonflammable and hydrophobic have been developed for use as lightweight thermal- insulation materials for cryogenic systems. Aerogels are well known in the industry for their effectiveness as thermal insulators under cryogenic conditions, but the treatments used heretofore to render them hydrophobic also make them flammable. Nonflammability would make it safer to use aerogel insulation, especially in oxygen-rich environments and on cryogenic systems that contain liquid oxygen. A composite of this type is a silica aerogel reinforced with fibers. In comparison with unreinforced aerogels, the aerogel composite is about ten times as stiff and strong, better able to withstand handling, and more amenable to machining to required shapes. The composite can be made hydrophobic and nonflammable by appropriate design of a sol-gel process used to synthesize the aerogel component. In addition to very low thermal conductivity needed for insulation, aerogel composites of this type have been found to exhibit high resistance to moisture and nonflammability in oxygen-rich atmospheres: Samples floating on water for months gained no weight and showed no signs of deterioration. Samples were found to be nonflammable, even in pure oxygen at atmospheric pressure [14.7 psia (0.10 MPa)]

Redouane, Begag↗

NASA NTRS2013

Induction Heating Model of Cermet Fuel Element Environmental Test (CFEET)

Deep space missions with large payloads require high specific impulse and relatively high thrust to achieve mission goals in reasonable time frames. Nuclear Thermal Rockets (NTR) are capable of producing a high specific impulse by employing heat produced by a fission reactor to heat and therefore accelerate hydrogen through a rocket nozzle providing thrust. Fuel element temperatures are very high (up to 3000 K) and hydrogen is highly reactive with most materials at high temperatures. Data covering the effects of high‐temperature hydrogen exposure on fuel elements are limited. The primary concern is the mechanical failure of fuel elements due to large thermal gradients; therefore, high‐melting‐point ceramics‐metallic matrix composites (cermets) are one of the fuels under consideration as part of the Nuclear Cryogenic Propulsion Stage (NCPS) Advance Exploration System (AES) technology project at the Marshall Space Flight Center. The purpose of testing and analytical modeling is to determine their ability to survive and maintain thermal performance in a prototypical NTR reactor environment of exposure to hydrogen at very high temperatures and obtain data to assess the properties of the non‐nuclear support materials. The fission process and the resulting heating performance are well known and do not require that active fissile material to be integrated in this testing. A small‐scale test bed; Compact Fuel Element Environmental Tester (CFEET), designed to heat fuel element samples via induction heating and expose samples to hydrogen is being developed at MSFC to assist in optimal material and manufacturing process selection without utilizing fissile material. This paper details the analytical approach to help design and optimize the test bed using COMSOL Multiphysics for predicting thermal gradients induced by electromagnetic heating (Induction heating) and Thermal Desktop for radiation calculations.

Gomez, C. F.↗

NASA NTRS2013

Induction Heating Model of Cermet Fuel Element Environmental Test (CFEET)

Gomez, Carlos F.↗

NASA NTRS2019

A thin-ply composite with embedded metallic mesh for a spaceborne antenna

This study presents a technique developed for embedding a conductive metallic mesh into the layup of thin-ply carbon fiber reinforced polymer (CFRP) composite material. Thermal cycling and subsequent mechanical testing on fabricated samples has been used to evaluate thin-ply composites as a crack mitigation technique. Furthermore, the construction of thin-ply CFRP composite tubes has been demonstrated for both straight segments and curved segments utilizing a novel sacrificial ceramic molding method. These prototypes represent the building blocks for a 1 m scale radiating element and are the first test articles for the evaluation of thin-ply CFRP composites with an embedded metallic mesh. The successful implementation of a CFRP composite with an embedded metallic mesh would enable ultra-lightweight conductive structures for future applications, such as antennas, requiring survival in cryogenic temperatures.

Sakovsky, Maria↗

NASA NTRS1988

Design, development, and test of Shuttle/Centaur G-prime cryogenic tankage thermal protection systems

The thermal protection systems (TPS) for the Shuttle/Centaur were designed to provide fail-safe thermal protection during prelaunch, launch ascent, and on-orbit operations as well as during potential abort, where the Shuttle and Centaur would return to earth. The TPS selected used a helium-purged polyimide foam beneath three radiation shields for the liquid-hydrogen (LH2) tank and radiation shields only for the liquid-oxygen (LO2) tank. A double-walled vacuum bulkhead separated the two tanks. The LH2 tank had one 1.9 cm-thick layer of foam on the forward bulkhead and two layers on the larger-area sidewall. Full scale tests of the flight vehicle in a simulated Shuttle cargo bay gave total prelaunch heating rates of 29.5 and 12.9 kW for the LH2 and LO2 tanks, respectively. Calorimeter tests on a representative sample of the LH2 tank sidewall TPS indicated that the measured unit heating one would rapidly decrease from the prelaunch rate of about 300 W/sq m to a desired rate less than 4 W/sq m once on-orbit.

Macneil, Peter N.↗

NASA NTRS2017

Thermally-Conductive Metallic Coatings and Applications for Heat Removal on In-Space Cryogenic Vehicles

For large in-space cryogenic upper stages, substantial axial heat removal from a forward skirt by vapor-based heat interception may not be achieved by simple attachment methods unless sufficient thermal conductance from the skirt to the cooling fluid can be achieved. Preferable methods would allow for the addition of the cooling system to existing structure with minimal impact on the structure. Otherwise, significant modification to the basic structural design andor novel and complex attachment mechanisms with high effective thermal conductance are likely to be required. The approach being pursued by evolvable Cryogenics (eCryo) is to increase the thermal performance of a relatively simple attachment system by applying metallic or other thermally conductive material coatings to the mating surface area of the fluid channel where it is attached the skirt wall. The expectation of candidate materials is that the dramatic increase in conductivity of pure metals at temperatures close to liquid hydrogen vapor temperature will compensate for the reduced actual contact area typical of mechanical joints. Basic contact conductance data at low temperatures for candidate interface materials is required to enable the test approach. A test rig was designed at NASA Glenn Research Center to provide thermal contact resistance testing between small sample coupons coated with conductive material via electron beam evaporation, a low-temperature option that will not affect physical properties of base materials. Average coating thicknesses were 10 k. The test fixture was designed to mount directly to a cryocooler cold head within a vacuum test chamber. The purpose of this test was to determine qualitative contact conductance between various test samples. Results from this effort will be implemented in a sub-scale vapor-based heat interception test, where the applicability for increased heat removal on large structural skirts will be considered.

small scale testing↗

NASA NTRS1987

Support of the eight-foot high-temperature tunnel modifications project

An ultrasonic level sensor was developed to measure the liquid level in a storage vessel under high pressures, namely up to 6000 psi. The sensor is described. A prototype sensor was installed in the cooling-water storage vessel of the Eight-Foot High-Temperature Tunnel. Plans are being made to install the readout instrument in the control room, so that tunnel operators can monitor the water level during the course of a tunnel run. It was discovered that the sensor will operate at cryogenic temperatures. Consequently, a sensor will be installed in the modified Eight-Foot High-Temperature Tunnel to measure the sound speed of liquid oxygen (LOX) as it is transferred from a storage vessel to the tunnel combustor at pressure of about 3000 psi. The sound speed is known to be a reliable indicator of contamination of LOX by pressurized gaseous nitrogen, which will be used to effect the transfer. Subjecting the sensor to a temperature cycle from room temperature to liquid nitrogen temperature and back again several times revealed no deterioration in sensor performance. The method using this sensor is superior to the original method, which was to bleed samples of LOX from the storage vessel to an independent chamber for measurement of the sound speed.

Hodges, Donald Y.↗

NASA NTRS2016

Spectral Monitoring of Volatiles During Drilling into Frozen Lunar Simulant

NASA's Resource Prospector (RP) project intends to characterize the 3D distribution of volatiles in permanently shadowed regions at the lunar poles. One RP remote sensing instrument is a near-infrared spectrometer with an associated camera and radiometer, called the Near-InfraRed Volatile Spectrometer System (NIRVSS). In May 2016, NIRVSS, a Honeybee Robotics drill, and an Inficon mass spectrometer were placed in a vacuum chamber at Glenn Research Center. Also inside was a tube (1.2 m high x 25 cm diameter) filled with lunar simulant NU-LHT-3M, initially doped with a homogeneous water abundance of ~5%, chilled to cryogenic temperatures and exposed to a vacuum (~10e-6 Torr). During drilling, the NIRVSS instruments observed the cuttings pile as subsurface materials were emplaced on the surface. Spectral features associated with water ice, near 2000 and 3000 nm, were measured by the spectrometer during drilling. The spectral data documents development of a desiccated soil layer in the tube down to ~25-30 cm (confirmed by post-test soil analyses), formed during the initial pump down to vacuum. Drilling occurred in 10 cm segments, with the drill stem extracted and flutes brushed after each 10 cm depth. One exception to this was the 40 cm depth segment where the soil was delivered to a sample capture mechanism, and sealed for post-test analyses. To ~30 cm depth the greatest 2000 and 3000 nm signatures were associated with brushing of the drill flutes above the surface. At depths >40 cm the strongest ice signatures were associated with the drill clearing soil from the existing hole, or beginning to encounter new material. For these greater depths, brushing the flutes after extraction produced much weaker ice signatures than for shallower depths. This suggests that the soil may remain trapped in the exit funnel and is not emplaced on the surface. After each event creating strong ice signatures, these signatures decreased to near background levels in 5 minutes or less, due to surface exposure to vacuum.

lunar poles↗

NASA NTRS1987

Design, development and test of shuttle/Centaur G-prime cryogenic tankage thermal protection systems

The thermal protection systems for the shuttle/Centaur would have had to provide fail-safe thermal protection during prelaunch, launch ascent, and on-orbit operations as well as during potential abort. The thermal protection systems selected used a helium-purged polyimide foam beneath three rediation shields for the liquid-hydrogen tank and radiation shields only for the liquid-oxygen tank (three shields on the tank sidewall and four on the aft bulkhead). A double-walled vacuum bulkhead separated the two tanks. The liquid-hydrogen tank had one 0.75-in-thick layer of foam on the forward bulkhead and two layers on the larger area sidewall. Full scale tests of the flight vehicle in a simulated shuttle cargo bay that was purged with gaseous nitrogen gave total prelaunch heating rates of 88,500 Btu/hr and 44,000 Btu/hr for the liquid-hydrogen and -oxygen tanks, respectively. Calorimeter tests on a representative sample of the liquid-hydrogen tank sidewall thermal protection system indicated that the measured unit heating rate would rapidly decrease from the prelaunch rate of approx 100 Btu/hr/sq ft to a desired rate of less than 1.3 Btu/hr/sq ft once on orbit.

Knoll, Richard H.↗