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DOE OSTI2021

Geometry versus growth: Internal consistency of the flat ΛCDM model with KiDS-1000

Here, we carry out a multi-probe self-consistency test of the flat Lambda Cold Dark Matter (ΛCDM) model with the aim of exploring potential causes of the reported tensions between high- and low-redshift cosmological observations. We divide the model into two theory regimes determined by the smooth background (geometry) and the evolution of matter density fluctuations (growth), each governed by an independent set of ΛCDM cosmological parameters. This extended model is constrained by a combination of weak gravitational lensing measurements from the Kilo-Degree Survey, galaxy clustering signatures extracted from Sloan Digital Sky Survey campaigns and the Six-Degree Field Galaxy Survey, and the angular baryon acoustic scale and the primordial scalar fluctuation power spectrum measured in Planck cosmic microwave background (CMB) data. For both the weak lensing data set individually and the combined probes, we find strong consistency between the geometry and growth parameters, as well as with the posterior of standard ΛCDM analysis. In the non-split analysis, for which one single set of parameters was used, tension in the amplitude of matter density fluctuations as measured by the parameter S 8 persists at around 3σ, with a 1.5% constraint of S 8 = 0.776$_{–0.008}^{+0.016}$ for the combined probes. We also observe a less significant preference (at least 2σ) for higher values of the Hubble constant, H 0 = 70.5$_{–1.5}^{+0.7}$ km s –1 Mpc –1 , as well as for lower values of the total matter density parameter Ω m = 0.289$_{–0.005}^{+0.007}$ compared to the full Planck analysis. Including the subset of the CMB information in the probe combination enhances these differences rather than alleviate them, which we link to the discrepancy between low and high multipoles in Planck data. Our geometry versus growth analysis does not yet yield clear signs regarding whether the origin of the discrepancies lies in ΛCDM structure growth or expansion history but holds promise as an insightful test for forthcoming, more powerful data.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2021

Critical Interference Mechanisms for Marine Renewable Energy-powered Ocean Observing Platforms

Marine renewable energy devices, such as wave energy converters or tidal turbines, not only have the potential to provide clean, reliable power to the grid but may also offer new opportunities for ocean exploration by providing power for oceanographic sensors where other sources cannot. However, an important consideration in making this vision a reality is understanding whether the marine energy devices may interfere with oceanographic measurements. Interference may occur through several pathways, including sound produced by the device and the motion of the device itself. In this report, we provide an overview of interference pathways and their implications before exploring two use cases for marine energy-powered ocean observing platforms: a tidal-powered passive acoustic monitoring system and wave-powered wave measurement buoys. For each use case, we review the relevant literature and underlying physics of the systems as they are relevant to the desired measurements before making recommendations for design of such systems.

16 TIDAL AND WAVE POWER↗

DOE OSTI2020

Distributed Acoustic Sensing as a Distributed Hydraulic Sensor in Fractured Bedrock

Distributed acoustic sensing (DAS) was originally intended to measure oscillatory strain at frequencies of 1 Hz or more on a fiber optic cable. Recently, measurements at much lower frequencies have opened the possibility of using DAS as a dynamic strain sensor in boreholes. A fiber optic cable mechanically coupled to a geologic formation will strain in response to hydraulic stresses in pores and fractures. A DAS interrogator can measure dynamic strain in the borehole, which can be related to fluid pressure through the mechanical compliance properties of the formation. Because DAS makes distributed measurements, it is capable of both locating hydraulically active features and quantifying the fluid pressure in the formation. We present field experiments in which a fiber optic cable was mechanically coupled to two crystalline rock boreholes. The formation was stressed hydraulically at another well using alternating injection and pumping. The DAS instrument measured oscillating strain at the location of a fracture zone known to be hydraulically active. Rock displacements of less than 1 nm were measured. Laboratory experiments confirm that displacement is measured correctly. These results suggest that fiber optic cable embedded in geologic formations may be used to map hydraulic connections in three-dimensional fracture networks. A great advantage of this approach is that strain, an indirect measure of hydraulic stress, can be measured without beforehand knowledge of flowing fractures that intersect boreholes. The technology has obvious applications in water resources, geothermal energy, CO 2 sequestration, and remediation of groundwater in fractured bedrock.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Frequency–Magnitude Statistics of Laboratory Foreshocks Vary With Shear Velocity, Fault Slip Rate, and Shear Stress

Understanding the nucleation phase of earthquakes is key for advancing earthquake hazard assessment and improving earthquake early warning systems. However, little progress has been made in this area due to a poor understanding of nucleation processes and incomplete seismic and fault zone measurements. The ability to integrate measured fault zone properties with seismic data could significantly improve our understanding of how earthquakes begin and whether there are systematic variations in seismic properties preceding failure. In this work, we use high-resolution laboratory measurements of fault zone properties along with acoustic emission data to document temporal variations of foreshock properties. Our data show that foreshock size increases with shear stress, loading rate, and fault slip rate. We propose that the preseismic fault slip rate and fault zone thickness (i.e., porosity) work in concert to modulate foreshock properties.

15 GEOTHERMAL ENERGY↗

DOE OSTI2022

Outsourced hearing in an orb-weaving spider that uses its web as an auditory sensor

Hearing is a fundamental sense of many animals, including all mammals, birds, some reptiles, amphibians, fish, and arthropods. The auditory organs of these animals are extremely diverse in anatomy after hundreds of millions of years of evolution, yet all are made up of cellular tissue and are morphologically part of the bodies of animals. Here, we show that hearing in the orb-weaving spider Larinioides sclopetarius is not constrained by the organism’s body but is extended through outsourcing hearing to its extended phenotype, the proteinaceous, self-manufactured orb web. We find that the wispy, wheel-shaped orb web acts as a hyperacute acoustic antenna to capture the sound-induced air particle movements that approach the maximum physical efficiency better than the acoustic responsivity of all previously known eardrums. By sensing the motion of web threads, the spider remotely detects and localizes the source of an incoming airborne acoustic wave, such as those emitted by approaching prey or predators. By outsourcing its acoustic sensors to its web, the spider is released from body size constraints and permits the araneid spider to increase its sound-sensitive surface area enormously, up to 10,000 times greater than the spider itself. The spider also enables the flexibility to functionally adjust and regularly regenerate its external "eardrum" according to its needs. The outsourcing and supersizing of auditory function in spiders provides unique features for studying extended and regenerative sensing and designing novel acoustic flow detectors for precise fluid dynamic measurement and manipulation.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2023

The DESI Bright Galaxy Survey: Final Target Selection, Design, and Validation

Over the next 5 yr, the Dark Energy Spectroscopic Instrument (DESI) will use 10 spectrographs with 5000 fibers on the 4 m Mayall Telescope at Kitt Peak National Observatory to conduct the first Stage IV dark energy galaxy survey. At z < 0.6, the DESI Bright Galaxy Survey (BGS) will produce the most detailed map of the universe during the dark-energy-dominated epoch with redshifts of >10 million galaxies spanning 14,000 deg 2 . In this work, we present and validate the final BGS target selection and survey design. From the Legacy Surveys, BGS will target an r < 19.5 mag limited sample (BGS Bright), a fainter 19.5 < r < 20.175 color-selected sample (BGS Faint), and a smaller low-z quasar sample. BGS will observe these targets using exposure times scaled to achieve homogeneous completeness and cover the footprint three times. We use observations from the Survey Validation programs conducted prior to the main survey along with simulations to show that BGS can complete its strategy and make optimal use of "bright" time. BGS targets have stellar contamination <1%, and their densities do not depend strongly on imaging properties. BGS Bright will achieve >80% fiber assignment efficiency. Finally, BGS Bright and BGS Faint will achieve >95% redshift success over any observing condition. BGS meets the requirements for an extensive range of scientific applications. BGS will yield the most precise baryon acoustic oscillation and redshift-space distortion measurements at z < 0.4. It presents opportunities for new methods that require highly complete and dense samples (e.g., N-point statistics, multitracers). BGS further provides a powerful tool to study galaxy populations and the relations between galaxies and dark matter.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2026

Dynamical Dark Energy Imprints in the Lyman-Alpha Forest

The nature of dark energy (DE) remains elusive, even though it constitutes the dominant energy-density component of the Universe and drives the late-time acceleration of cosmic expansion. By combining measurements of the expansion history from baryon acoustic oscillations, supernova surveys, and cosmic microwave background data, the Dark Energy Spectroscopic Instrument (DESI) Collaboration has inferred that the DE equation of state may evolve over time. The profound implications of a time-variable, ``dynamical" DE (DDE) that departs from a cosmological constant motivate the need for independent observational tests. In this work, we use cosmological hydrodynamical simulations of structure formation to investigate how DDE affects the properties of the Lyman-Alpha ``forest'' of absorption features produced by neutral hydrogen in the cosmic web. We find that DDE models consistent with the DESI constraints induce a spectral tilt in the forest transmitted flux power spectrum, imprinting a scale- and redshift-dependent signature relative to standard Lambda-CDM cosmologies. These models also yield higher intergalactic medium temperatures and reduced Lyman-Alpha opacity compared to Lambda-CDM. We discuss the observational implications of these trends as potential avenues for independent confirmation of DDE.

Garza, Diego [UC, Santa Cruz, Inst. Part. Phys.] (↗

DOE OSTI2025

Prototype acoustic positioning system for the Pacific Ocean Neutrino Experiment

We present the design and initial performance characterization of the prototype acoustic positioning system intended for the Pacific Ocean Neutrino Experiment. It comprises novel piezo-acoustic receivers with dedicated filtering- and amplification electronics installed in P-ONE instruments and is complemented by a commercial system comprised of cabled and autonomous acoustic pingers for sub-sea installation manufactured by Sonardyne Ltd. We performed an in-depth characterization of the acoustic receiver electronics and their acoustic sensitivity when integrated into P-ONE pressure housings. These show absolute sensitivities of up to -125 dB re V2/μPa2 in a frequency range of 10–40 kHz. We furthermore conducted a positioning measurement campaign in the ocean by deploying three autonomous acoustic pingers on the seafloor, as well as a cabled acoustic interrogator and a P-ONE prototype module deployed from a ship. Using a simple peak-finding detection algorithm, we observe high accuracy in the tracking of relative ranging times at approximately 230–280 μs at distances of up to 1600 m, which is sufficient for positioning detectors in a cubic-kilometer detector and which can be further improved with more involved detection algorithms. The tracking accuracy is further confirmed by independent ranging of the Sonardyne system and closely follows the ship's drift in the wind measured by GPS. The absolute positioning shows the same tracking accuracy with its absolute precision only limited by the large uncertainties of the deployed pinger positions on the seafloor.

Data analysis↗

DOE OSTI2020

Mapping of Benthic Habitats at Marine Renewable Energy Sites Using Multibeam Echosounder and Sediment Profile Imaging Technologies

Objectives/Scope: The goal of this work was to develop a consistent and semi-automated seafloor survey method for generating high-resolution, benthic habitat maps for environmental assessments and monitoring of marine renewable energy sites. Sediment profile and plan view imaging (SPI/PV) technology was combined with multibeam bathymetry and acoustic backscatter methods to demonstrate a rapid, cost-effective benthic mapping protocol. A key technical innovation of this project was the development of an image processing platform that automatically measures key features from the images. Methods: Multibeam echosounder (MBES) acoustic and SPI/PV surveys were conducted at three coastal areas off the U.S. west coast, including the PacWave South energy test site off of Newport, Oregon. Point data on physical and biological sediment conditions obtained from the SPI/PV imagery were used to efficiently ground-truth the high-resolution MBES bathymetry and backscatter mosaics. The SPI camera is an optical corer that obtains an undisturbed 21 by 15 cm, high-resolution, cross-sectional image of the sediment–water interface and upper sediment column. The plan view camera attached to the SPI camera frame captures a downward looking view of the seabed immediately before the SPI image is obtained. As part of this project, we developed a computer vision image processing platform (iSPI) that uses deep convolutional neural networks and other approaches to automatically identify and measure key features in the images, such as grain size and surface relief. Results: Detailed benthic habitat maps were generated using this mapping approach for three different marine settings. The sites mapped included a silt-dominated embayment; a sloping, nearshore, transitional very fine to coarse sand bottom; and a medium, sand-dominated continental shelf marine energy test site. In each case, acoustic and imaging surveys were completed in less than week, and detailed benthic habitat maps were generated within 60 days. The results were placed within the Coastal and Marine Ecological Classification Standard (CMECS) habitat mapping framework, and various combinations of the bathymetry, backscatter, and SPI and PV data were used to generate CMECS component maps. Novel Information: This project developed and demonstrated a repeatable and cost-effective approach for efficiently mapping benthic habitat conditions over broad areas of the seafloor by combining state-of-the-art acoustic and imaging techniques. The primary survey tools used in this project have been used previously in both the offshore renewable (wind) and oil and gas sectors to map and monitor benthic environments. This project’s innovations include 1) the focused use of high-resolution SPI/PV imagery to ground-truth acoustic mosaics, and 2) the development of a computer automated image analysis processing tool that both streamlines and standardizes the generation of data from the imagery and makes the data extraction process more cost-effective and repeatable.

13 HYDRO ENERGY↗

DOE OSTI2026

Online Alpha Monitoring of High Cs-137 Hanford and SRS High Level Waste with Tensioned Metastable Fluid Detectors

The Department of Energy’s Hanford and Savannah River Sites maintain millions of gallons of caustic supernate and salt high activity waste in their high-level waste (HLW) tank farm inventories. The Savannah River Site is currently treating this waste with a calixarene-based solvent extraction of Cs-137 to reduce these inventories. Hanford is employing an at-tank crystalline silico titanate (CST) based solid phase extraction methodology to reduce their liquid HLW inventories. Due to the high solubility of Cs-137 and the relative insolubility of the actinides in these caustic waste forms, the beta to alpha radioactivity ratio can often exceed six orders of magnitude in the feed solutions to these treatment processes. This unique characteristic leads to significant technical challenges in making rapid gross alpha measurements in the presence of the overwhelming beta, gamma, as well as dissolved sodium salt in these HLW matrices. Conventional radioanalytical techniques, such as liquid scintillation analysis or gas flow proportional counting require significant radiochemistry preparation prior to the radiometric measurements for gross alpha activity. These required pretreatments render these technologies untenable for rapid quantification of gross alpha activity that could be required to support on or at-line measurements ensuring a waste stream will meet regulatory requirements. The radiation measurement properties of Tensioned Metastable Fluid Detectors (TMFDs) have been studied by Purdue University’s Taleyarkhan research group for well over a decade. Fluids tensioned to the appropriate degree will rupture when struck by radiation, resulting in a measurable cavitation event. The negative pressure generating this tension can be adjusted by centrifugal rotation or by acoustic means in such a way that these cavitation events can be generated from alpha radiation but will not be generated by beta or gamma radiation. Purdue University and the Savannah River National Laboratory are currently collaborating to develop a gamma/beta blind, spectroscopic alpha measurement system based on the Tensioned Metastable Fluid Detector technology to provide a potential solution for performing rapid gross alpha measurements on these high gamma/beta sample matrices. Measurements using the Indirect Drive Acoustically Tensioned Metastable Fluid Detectors developed as part of this collaboration were performed with an alpha emitting radionuclide. Successful determination of gross alpha activity was observed, indicating a potential pathway for rapid gross alpha measurements in remote-handled shielded cells or in process situations requiring online alpha monitoring. Measurements using this system have been conducted on high beta activity solutions, demonstrating the beta blind capability of this system. Measurements are currently underway to test the system’s capability to measure gross alpha activity on Savannah River Site high level waste high Cs-137 samples that have been measured by the SRNL radiochemistry team. This work was supported by the DOE EM Technology Development program.

DiPrete, David [Savannah River National Laboratory↗

DOE OSTI2022

Standardizing reverberation-measured C iv time-lag quasars, and using them with standardized Mg ii quasars to constrain cosmological parameters

ABSTRACT We use 38 C iv quasar (QSO) reverberation-mapped observations, which span eight orders of magnitude in luminosity and the redshift range 0.001064 ≤ z ≤ 3.368, to simultaneously constrain cosmological-model and QSO radius–luminosity (R–L) relation parameters in six cosmological models, using an improved technique that more correctly accounts for the asymmetric errors bars of the time-lag measurements. We find that R–L relation parameters are independent of the cosmological models used in the analysis and so the R–L relation can be used to standardize the C iv QSOs. The C iv QSO cosmological constraints are consistent with those from Mg ii QSOs, allowing us to derive joint C iv + Mg ii QSO cosmological constraints which are consistent with currently accelerated cosmological expansion, as well as consistent with cosmological constraints derived using better-established baryon acoustic oscillation (BAO) and Hubble parameter [H(z)] measurements. When jointly analysed with H(z) + BAO data, current C iv + Mg ii QSO data mildly tighten current H(z) + BAO data cosmological constraints.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2020

Soft elastic constants from phonon spectroscopy in hole-doped Ba 1-x (K,Na) x Fe 2 As 2 and Sr 1-x Na x Fe 2 As 2

We report inelastic x-ray scattering measurements of the in-plane polarized transverse acoustic phonon mode propagating along q ∥ [ 100 ] in various hole-doped compounds belonging to the 122 family of iron-based superconductors. Additionally, the slope of the dispersion of this phonon mode is proportional to the square root of the shear modulus C 66 in the q → 0 limit and, hence, sensitive to the tetragonal to orthorhombic structural phase transition occurring in these compounds. In contrast to a recent report for Ba ( Fe 0.94 Co 0.06 ) 2 As 2 [Weber et al. , Phys. Rev. B 98 , 014516 (2018) ], we find qualitative agreement between values of C 66 deduced from our experiments and those derived from measurements of the Young modulus in Ba 1 - x ( K , Na ) x Fe 2 As 2 at optimal doping. These results provide an upper limit of about 50 Å for the nematic correlation length for the investigated optimally hole-doped compounds. Furthermore, we also studied compounds at lower doping levels exhibiting the orthorhombic magnetic phase, where C 66 is not accessible by volume probes, as well as the C 4 tetragonal magnetic phase.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2024

Effects of irradiation damage on the hardness and elastic properties of quaternary and high entropy transition metal diborides

Multi-principal component transition metal (TM) diborides represent a class of high-entropy ceramics (HECs) that have received considerable interest in recent years owing to their promising properties for extreme environment applications that include thermal/ environmental barriers, hypersonic vehicles, turbine engines, and next-generation nuclear reactors. While the addition of chemical disorder through the random distribution of TM elements on the cation sublattice has offered opportunities to tailor elastic stiffness and hardness, the effects of irradiation-induced structural damage on the physical properties of these complex materials have remained largely unexplored. To this end, changes in the hardness and elastic moduli of a high-entropy TM diboride (Hf 0.2 Nb 0.2 Ta 0.2 Ti 0.2 Zr 0.2 )B 2 and three of its quaternary subsets following irradiation with 10 MeV gold (Au) ions to fluences of up to 6 × 10 15 Au cm -2 are investigated at the micrometer and sub-micrometer length-scales via the dispersion of laser-generated surface acoustic waves (SAW) and nanoindentation, respectively. The nanoindentation measurements show that the TM diborides exhibit an initial increase in hardness following irradiation with energetic Au ions, with a subsequent decrease in hardness following further irradiation. One quaternary composition, (Hf 1/3 Ta 1/3 Ti 1/3 )B 2 , exhibits a notable exception to the trend and continues to exhibit an increase in hardness with ion irradiation fluence. Although differences in the absolute values of the effective elastic moduli obtained from the measured SAW dispersion and nanoindentation are observed (and attributed to microstructural variations at the measurement length-scale), both techniques yield similar trends in the form of an initial reduction and subsequent saturation in the elastic modulus with increasing ion irradiation fluence. The quaternary TM diboride (Hf 1/3 Ta 1/3 Ti 1/3 )B 2 again exhibits a departure from this trend. The high-entropy TM diboride (Hf 0.2 Nb 0.2 Ta 0.2 Ti 0.2 Zr 0.2 )B 2 exhibits the greatest recovery in hardness and modulus when irradiated to high ion fluences following initial changes at low fluence, indicating superior resistance to radiation-induced damage over its quaternary counterparts. Opportunities for designing HECs with superior hardness and modulus for enhanced radiation resistance (compared to their single constituent counterparts) by tailoring chemical disorder and bond character in the lattice are discussed.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Cross-Beam Energy Transfer Saturation by Ion Heating

Cross-beam energy transfer (CBET) saturation by ion heating was measured in a gas-jet plasma characterized using Thomson scattering. Here, a wavelength-tunable ultraviolet (UV) probe laser beam was interacted with four intense UV pump beams to drive large-amplitude ion-acoustic waves. For the highest-intensity interactions, the power transferred to the probe laser dropped, demonstrating ion-acoustic wave saturation. Over this time, the ion temperature was measured to increase by a factor of 7 during the 500-ps interaction. Particle-in-cell simulations show ion trapping and a subsequent ion heating consistent with measurements. Linear kinetic CBET models were found to agree well with the observed energy transfer when the measured plasma conditions were used.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2026

Correlation of Surface Acoustic Wave (SAW) force myography sensor output with elbow joint torque

Accurate assessment of skeletal muscle forces and net joint torque is essential for preventing fatigue-related injuries, optimizing physical training, and monitoring disease progression in neuromuscular conditions. However, existing joint torque evaluation techniques are hindered by limited portability and high operational costs, confining their use to controlled laboratory or clinical settings. Despite substantial advances in wearable joint torque estimation systems, ongoing challenges such as power constraints, bulky wired setups, and susceptibility to environmental or motion artifacts underscore the urgent need for truly batteryless, wireless solutions deployable in real-world settings. This paper proposes a novel surface acoustic wave (SAW)-based force myography (FMG) system for noninvasive measurement of joint torque, validated against a gold-standard electromechanical dynamometer. The approach uses a single SAW sensor embedded in an armband to detect volumetric biceps brachii changes, with a second-order polynomial mapping sensor output and elbow angle to torque. Seven participants were tested in both isometric (15°–90°) and isokinetic (10°/s and 20°/s) supinated elbow flexion tasks. Under isometric conditions, subject-specific calibration achieved a normalized root-mean-square error (NRMSE) of 13.6% ± 6.0% and R 2 = 0.834 ± 0.180, while a group-level model yielded 14.4% ± 6.8% and 0.808 ± 0.208, respectively. For isokinetic trials, the group model produced an NRMSE of 24.1% ± 6.6% at 10°/s and 24.9% ± 08.9% at 20°/s, highlighting the feasibility of using a single-sensor SAW-FMG setup across different speeds. Because SAW devices support wireless, battery-free operation, the proposed system offers a pathway to portable, real-time monitoring for sports medicine, rehabilitation, and clinical diagnostics.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Observing fish interactions with marine energy turbines using acoustic cameras

Abstract Marine current energy converters such as tidal and riverine turbines have the potential to provide reliable, clean power. The risk of collision of fishes with marine energy turbines is not yet well understood, in part due to the challenges associated with observing fish at turbine sites. Turbidity and light availability can limit the effectiveness of optical sensors like video cameras, motivating the use of acoustic cameras for this task. However, challenges persist in collecting and interpreting data acquired from acoustic cameras. Given the limited number of turbine deployments to date, it is prudent to draw on the application of acoustic cameras to monitor fish in other scenarios. This article synthesizes their use for other fisheries applications to inform best practices and set realistic expectations for the results of acoustic camera monitoring at turbine sites. We discuss six key tasks performed with acoustic cameras: detecting objects, identifying objects as fish, counting fish, measuring fish, classifying fish taxonomically and analysing fish behavior. Specific challenges to monitoring fish at turbine sites are discussed. This article is intended to serve as a reference for researchers, regulators and marine energy developers on effective use of acoustic cameras to monitor fish at turbine sites. The studies detailed in this article provide evidence that, in some scenarios, acoustic cameras can be used to inform the risk of fish collision with marine energy turbines but doing so requires careful study design and data processing.

Cotter, Emma↗

DOE OSTI2023

Energy Budget of Brittle Fracturing in Granite Under Stress Relaxation and Creep

Creep and relaxation are the two major time-dependent fracturing processes in rocks. While a considerable amount of research has been done in understanding these two mechanisms, critical gaps remain regarding how different energy components evolve during time-dependent fracturing processes in rocks. In this study, a series of relaxation and creep experiments were conducted on prismatic Barre granite specimens in the laboratory to estimate the energy budget of brittle fracturing in granite. For the input energy, the work done by the machine (W) is calculated and for the output energy the radiated seismic energy (E R ), released in the form of acoustic emissions (AEs), is calculated as the only measurable output energy component in the conducted experiments. The low-frequency plateau (Ω 0 ) and corner frequency (f 0 ) for each AE waveform was estimated by fitting the observed AE spectra with the theoretical spectra using the Omega model. These parameters were used to estimate the seismic moments (M 0 ) based on the radiation pattern for the double couple (shear) and non-double-couple (non-shear) events. The range of f 0 and M 0 varied from 150 to 750 kHz and 10 –4 to 10 –1 N m, respectively. Moment magnitude (M w ) varied in a wider range from –9 to –6 in creep and –8.5 to –7 in relaxation. Stress drops (Δ σ ) and source radius (r) were estimated for the AEs using Brune’s model. Here, the results report on three primary observations: (1) the effects of different source mechanisms on the estimated source parameters showed that M 0 and Δ σ were higher for DC events as compared to NDC in both relaxation and creep. (2) The radiation efficiency in the case of creep is 70% higher as compared to relaxation and, (3) the stress drop estimated in relaxation and creep demonstrated a breakdown in scaling with the seismic moment.

58 GEOSCIENCES↗

DOE OSTI2024

High-temperature structure, elasticity, and thermal expansion of ε-ZrH 1.8

Zirconium hydride is a promising candidate material for nuclear microreactor applications as a solid-state moderator component, owing to its favorable neutronics properties and good thermal stability over other metal hydrides. Here, in the present work, the crystal structure, thermal expansion, and elastic properties of the hydrogen-rich ε phase hydride were measured at elevated temperatures in the range 300–900 K. Samples were prepared by direct hydriding Zircaloy-4 metal – a nuclear-grade zirconium alloy. Room-temperature lattice parameters agree well with those reported from literature for unalloyed zirconium hydride and fall within an observed quadratic H-content dependence. The coefficients of thermal expansion, determined from lattice expansion and dilatometry, agree well within our work but were about 30 % lower than those reported by others for unalloyed hydrides. Density functional theory-based molecular dynamics simulations were used to compare with thermal expansion and elasticity measurements. Results showed lattice parameter temperature dependence and slope of thermal expansion align with those from measurements. Based on diffraction scans at select temperatures, ε phase remained stable in air up to at least 770 K. Likewise, dilatometry showed smooth thermal expansion up to the thermal decomposition temperature around 950 K. The precise decomposition temperature was not determined via diffraction due to sparse scanning. The complete elastic property measurements were gathered for ε-phase Ziracloy-4 hydride for the first time. Young's modulus was lower compared to the metal and δ hydride phases. High-temperature elasticity measurements were limited to <350 K due to acoustic dissipation effects.

36 MATERIALS SCIENCE↗