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Development of CDZNTE Detectors for Low-Energy Gamma-Ray Astronomy

Under this grant the UC Berkeley PI, K. Hurley, joined a Goddard-led effort to develop large area, multi-pixel Cadmium-Zinc-Telluride (CdZnTe, or CZT) detectors for gamma-ray astronomy. His task was to advise the project of new developments in the area of cosmic gamma-ray bursts, in order to focus the detector development effort on the construction of an instrument which could be deployed on a spacecraft to localize and measure the energy spectra of bursts with good angular and energy resolution, respectively. UC Berkeley had no hardware role in this proposal. The result of this effort was the production, at Goddard, of five CZT prototype modules. A proposal was written for SWIFT, a MIDEX mission to study cosmic gamma-ray bursts. One experiment aboard SWIFT is the Burst Arcminute Telescope (BAT), which consists of a 5200 sq cm hard X-ray detector and a coded mask. The detector comprises 256 CZT modules, each containing 128 4 x 4 x 2 mm CZT detectors. Each detector is read out using an ASIC. The angular resolution achieved with this mask/array combination is 22 arcminutes, and a strong gamma-ray burst can be localized to an accuracy of 4 arcminutes in under 10 seconds. The energy resolution is typically 5 keV FWHM at 60 keV, and the energy range is 10 - 150 keV. The BAT views 2 steradians, and its sensitivity is such that the instrument can detect 350 gamma-ray burst/year, localizing 320 of them to better than 4 arcminute accuracy. The BAT concept therefore met the science goals for gamma-ray bursts. The UCB effort in the SWIFT proposal included the scientific objectives for gamma-ray bursts, and the assembly of a team of optical and radio observers who would use the BAT data to perform rapid multi-wavelength searches for the counterparts to bursts. This proposal was submitted to NASA and peer-reviewed. In January 1999 it was one of five such proposals selected for a Phase A study. This study was completed in June, and SWIFT was formally presented to NASA in September. It appeared that a final selection of two MIDEX missions for flight was imminent. However, the final selection was deferred at the last minute due to the uncertainty in NASA's OSS budget.

Gehrels, N.↗

Thermal Design to Meet Stringent Temperature Gradient/Stability Requirements of SWIFT BAT Detectors

The Burst Alert Telescope (BAT) is an instrument on the National Aeronautics and Space Administration (NASA) SWIFT spacecraft. It is designed to detect gamma ray burst over a broad region of the sky and quickly align the telescopes on the spacecraft to the gamma ray source. The thermal requirements for the BAT detector arrays are very stringent. The maximum allowable temperature gradient of the 256 cadmium zinc telluride (CZT) detectors is PC. Also, the maximum allowable rate of temperature change of the ASICs of the 256 Detector Modules (DMs) is PC on any time scale. The total power dissipation of the DMs and Block Command & Data Handling (BCDH) is 180 W. This paper presents a thermal design that uses constant conductance heat pipes (CCHPs) to minimize the temperature gradient of the DMs, and loop heat pipes (LHPs) to transport the waste heat to the radiator. The LHPs vary the effective thermal conductance from the DMs to the radiator to minimize heater power to meet the heater power budget, and to improve the temperature stability. The DMs are cold biased, and active heater control is used to meet the temperature gradient and stability requirements.

Choi, Michael K.↗

The Effect of Twin Boundaries on the Spectroscopic Performance of CdZnTe Detectors

Most single grains in cadmium zinc telluride (CdZnTe) grown by the high-pressure Bridgman (HPB) technique contain multiple twin boundaries. As a consequence, twin boundaries are one of the most common macroscopic material defects found in large area (400 to 700 sq mm) CdZnTe specimens obtained from HPB ingots. Due to the prevalence of twin boundaries, understanding their effect on detector performance is key to the material selection process. Twin boundaries in several 2 mm thick large area specimens were first, documented using infrared transmission imaging. These specimens were then fabricated into either 2 mm pixel or planar detectors in order to examine the effect of the twin boundaries on detector performance. Preliminary results show that twin boundaries, which are decorated with tellurium inclusions, produce a reduction in detector efficiency and a degradation in resolution. The extent of the degradation appears to be a function of the density of tellurium inclusions.

Parker, Bradford H.↗

Development of High Resolution Mirrors and Cd-Zn-Te Detectors for Hard X-ray Astronomy

We describe the fabrication and implementation of a high-resolution conical, grazing- incidence, hard X-ray (20-70 keV) telescope. When flown aboard stratospheric balloons, these mirrors are used to image cosmic sources such as supernovae, neutron stars, and quasars. The fabrication process involves generating super-polished mandrels, mirror shell electroforming, and mirror testing. The cylindrical mandrels consist of two conical segments; each segment is approximately 305 mm long. These mandrels are first, precision ground to within approx. 1.0 micron straightness along each conical segment and then lapped and polished to less than 0.5 micron straightness. Each mandrel segment is the super-polished to an average surface roughness of approx. 3.25 angstrom rms. By mirror shell replication, this combination of good figure and low surface roughness has enabled us to achieve 15 arcsec, confirmed by X-ray measurements in the Marshall Space Flight Center 102 meter test facility. To image the focused X-rays requires a focal plane detector with appropriate spatial resolution. For 15 arcsec optics of 6 meter focal length, this resolution must be around 200 microns. In addition, the detector must have a high efficiency, relatively high energy resolution, and low background. We are currently developing Cadmium-Zinc-Telluride fine-pixel detectors for this purpose. The detectors under study consist of a 16x16 pixel array with a pixel pitch of 300 microns and are 1 mm and 2 mm thick. At 60 keV, the measured energy resolution is around 2%.

Ramsey, Brian D.↗

Building A New Kind of Graded-Z Shield for Swift's Burst Alert Telescope

The Burst Alert Telescope (BAT) on Swift has a graded-Z Shield that closes out the volume between the coded aperture mask and the Cadmium-Zinc-Telluride (CZT) detector array. The purpose of the 37 kilogram shield is to attenuate gamma rays that have not penetrated the coded aperture mask of the BAT instrument and are therefore a major source of noise on the detector array. Unlike previous shields made from plates and panels, this shield consists of multiple layers of thin metal foils (lead, tantalum, tin, and copper) that are stitched together much like standard multi-layer insulation blankets. The shield sections are fastened around BAT, forming a curtain around the instrument aperture. Strength tests were performed to validate and improve the design, and the shield will be vibration tested along with BAT in late 2002. Practical aspects such as the layup design, methods of manufacture, and testing of this new kind of graded-Z Shield are presented.

Robinson, David W.↗

EXIST: The Next Large GRB Observatory

Studies have begun on the EXIST (Energetic X-ray Imaging Survey Telescope) Mission as a Black Hole Survey 'Einstein Probe', a major element in the new NASA Beyond Einstein Program in the Office of Space Science. This program was approved by the US Congress, in February 2003 as part of the NASA FY2004 NASA budget. EXIST is planned as a very wide-field coded aperture telescope and a positional accuracy for GRBs better than one arc-minute. The baseline detectors are Cadmium-Zinc-Telluride (CZT), with a total sensitive area of approximately 8 m2. EXIST will use SWIFT as a pathfinder mission; the findings of SWIFT will refine the scientific objectives of EXIST and will help to determine many of its design parameters. EXIST will study early star and galaxy formation at high redshifts through observations of thousands of GRBs, their afterglows and host galaxies. It is intended that the international GRB community will play a large role in EXIST through direct participation as well as with complementary observational programs, both space-based and ground-based. Some preliminary design features and capabilities of the EXIST Mission will be presented.

Fishman, Gerald J.↗

X-Ray Testing Constellation-X Optics at MSFC's 100-m Facility

In addition to the 530-m-long X-Ray Calibration Facility (XRCF), NASA's Marshall Space Flight Center (MSFC) operates a 104-m-long (source-to-detector) X-ray-test facility. Originally developed and still occasionally used for stray-light testing of visible-fight optical systems, the so-called "Stray-Light Facility" now serves primarily as a convenient and inexpensive facility for performance evaluation and calibration of X-ray optics and detectors. The facility can accommodate X-ray optics up to about 1-m diameter and 12-m focal length. Currently available electron-impact sources at the facility span the approximate energy range 0.2 to 100 keV, thus supporting testing of soft- and hard-X-ray optics and detectors. Available MSFC detectors are a front-illuminated CCD (charge-coupled device) and a scanning CZT (cadmium--zinc--telluride) detector, with low-energy cut-offs of about 0.8 and 3 keV, respectively. In order to test developmental optics for the Constellation-X Project, led by NASA's Goddard Space Flight Center (GSFC), MSFC undertook several enhancements to the facility. Foremost among these was development and fabrication of a five-degree-of-freedom (5-DoF) optics mount and control system, which translates and tilts the user-provided mirror assembly suspended from its interface plate. Initial Constellation-X tests characterize the performance of the Optical Alignment Pathfinder Two (OAP2) for the large Spectroscopy X-ray Telescope (SXT) and of demonstration mirror assemblies for the Hard X-ray Telescope (HXT). With the Centroid Detector Assembly (CDA), used for precision alignment of the Chandra (nee AXAF) mirrors, the Constellation-X SXT Team optically aligned the individual mirrors of the OAPZ at GSFC. The team then developed set-up and alignment procedures, including transfer of the alignment from the optical alignment facility at GSFC to the X-ray test facility at MSFC, using a reference flat and fiducials. The OAPZ incorporates additional ancillary features --- fixed aperture mask and movable sub-aperture mask --- to facilitate X-ray characterization of the optics. Although the OAPZ was designed to- have low sensitivity to temperature offsets and gradients, analyses showed the necessity of active temperature control for the X-ray performance testing. Thus, the Smithsonian Astrophysical Observatory (SAO) implemented a thermal control and monitoring system, designed to hold the OAP2 close to its assembly.

O'Dell, Stephen↗

Crime scene investigations using portable, non-destructive space exploration technology

The National Institute of Justice (NIJ) and the National Aeronautics and Space Administration's (NASAs) Goddard Space Flight Center (GSFC) have teamed up to explore the use of NASA developed technologies to help criminal justice agencies and professionals solve crimes. The objective of the program is to produce instruments and communication networks that have application within both NASA's space program and NIJ programs with state and local forensic laboratories. A working group of NASA scientists and law enforcement professionals has been established to develop and implement a feasibility demonstration program. Specifically, the group has focused its efforts on identifying gunpowder and primer residue, blood, and semen at crime scenes. Non-destructive elemental composition identification methods are carried out using portable X-ray fluorescence (XRF) systems. These systems are similar to those being developed for planetary exploration programs. A breadboard model of a portable XRF system has been constructed for these tests using room temperature silicon and cadmium-zinc telluride (CZT) detectors. Preliminary tests have been completed with gunshot residue (GSR), blood-spatter and semen samples. Many of the element composition lines have been identified. Studies to determine the minimum detectable limits needed for the analyses of GSR, blood and semen in the crime scene environment have been initiated and preliminary results obtained. Furthermore, a database made up of the inorganic composition of GSR is being developed. Using data obtained from the open literature of the elemental composition of barium (Ba) and antimony (Sb) in handswipes of GSR, we believe that there may be a unique GSR signature based on the Sb to Ba ratio.

Firearms↗

X-Ray Detector Research at MSFC for Space Applications

NASA's Vision for Space Exploration has specific goals aimed at exploring the Solar System. This vision, under presidential mandate includes landing humans on the moon before the end of the next decade, paving the way for eventual journeys to Mars and beyond. The first missions to the moon will be in the form of both Orbiters and Landers, with the goal of paving the way for human return. One of the instruments we are currently working on,in collaboration with Brookhaven National Laboratory, is a lunar orbiter fluorescent x-ray spectrometer to finely map the light elements (down to Carbon) on surface of the moon. Funded NASA s Planetary Instrument Definition and Development Program the instrument is based on silicon drift detector arrays read out by custom ASICs. These offer the promise of high spectral resolution, necessary for resolving weak lines against a strong background continuum, and very low power requirements, necessary for large areas (greater than 500 square centimeters) required for future lunar missions. Further, the inherent radiation hardness of these detectors makes them ideal candidates for exploring the Jovian system, where the harsh radiation environment from Jupiter s radiation belts creates unfavorable detector conditions. Looking beyond our solar system, in the hard x-ray regime (20-80keV.), we are studying Cadmium-Zinc-Telluride pixilated detectors as feasible candidates for focal plane detectors of a hard x-ray telescope. This energy region bridges the gap between thermal and non-thermal x-ray emission from astronomical sources, will allow us to better understand supernovae nucleosynthesis (such as through the Ti-44 lines at 68keV and 78keV), Active Galactic Nuclei and other compact objects, more completely. The detectors that we are characterizing are 2mm in thickness and are pixilated with a 16x16 array of 300 micrometer pitch pixels (50micometer gap). These detectors are designed at Rutherford Appleton Laboratory, material is from eV Products, and polymer flip-chip assembly was performed by a commercial vendor. An energy resolution of 2.0% at 60keV (or better) should allow us to sufficiently distinguish lines of interest from background continuum, and the detector spatial resolution should be fine enough to over-sample the focal spot from the x-ray focusing optics by about a factor of two. Full technical details of these developments will be presented.

Gaskin, Jessica↗

A Hard-X-Ray Telescope Science Enhancement Package for the Constellation-X Mission

We present a science enhancement package (SEP) for NASA's planned Constellation-X mission submitted in response to a call for white papers. The call solicited proposals for either extending the bandwidth of Con-X to higher energies or enhancing the low-energy spectral resolution. The ground rules were that enhancement package should cost no more than $100M and weigh no more than 100 kg. The nickel-replicated-optics team responded with a stand-alone hard-x-ray telescope SEP concept. This consisted of two mirror modules, each with approximately 70 multilayer and iridium-coated shells, and two corresponding cadmium-zinc-telluride-based focal plane detectors. Addition of this package permits measurement of the hard-x-ray continuum up to 30-40 keV, which is essential for a quantitative measurement of the spectrum of gravitationally broadened iron lines that appear in the spectra of many black hole candidates. Full details of the instrument will be presented showing trades in energy bandwidth and effective area together with the full science justification for the enhancement package.

Ramsey, Brian↗

Characterization of Single-Sided Charge-Sharing CZT Strip Detectors for Gamma-Ray Astronomy

We report progress in the study of thick single-sided charge-sharing cadmium zinc telluride (CZT) strip detector modules designed to perform spectroscopy and 3-D imaging of gamma-rays. We report laboratory measurements including spectroscopy, efficiency and 3-D imaging capability of prototype detectors (15 15 7.5 cu mm) with 11x11 unit cells. We also report on Monte Carlo simulations (GEANT4 v7.1) to investigate the effect of multihits on detector performance in both spectroscopy and imaging. We compare simulation results with data obtained from laboratory measurements and discuss the implications for future strip detector designs. Keywords: CZT, strip detectors, gamma-ray

Donmez, Burcin↗

HX-POL-A Balloon-Borne Hard X-Ray Polarimeter

We report on the design and estimated performance of a balloon-borne hard X-ray polarimeter called HX-POL. The experiment uses a combination of Si and Cadmium Zinc Telluride detectors to measure the polarization of 50 keV-400 keV X-rays from cosmic sources through the dependence of the angular distribution of Compton scattered photons on the polarization direction. On a one-day balloon flight, HX-POL would allow us to measure the polarization of bright Crab-like sources for polarization degrees well below 10%. On a longer (15-30 day) flight from Australia or Antarctica, HX-POL would be be able to measure the polarization of bright galactic X-ray sources down to polarization degrees of a few percent. Hard X-ray polarization measurements provide unique venues for the study of particle acceleration processes by compact objects and relativistic outflows. In this paper, we discuss the overall instrument design and performance. Furthermore, we present results from laboratory tests of the Si and CZT detectors. Index Terms Gamma-ray astronomy, gamma-ray astronomy detectors, polarization, semiconductor radiation detectors, X-ray astronomy, X-ray astronomy detectors.

Krawczynski, H.↗

Detailed Studies of Pixelated CZT Detectors Grown with the Modified Horizontal Bridgman Method

The detector material Cadmium Zinc Telluride (CZT) achieves excellent spatial resolution and good energy resolution over a broad energy range, several keV up to some MeV. Presently, there are two main methods to grow CZT crystals, the Modified High-Pressure Bridgman (MHB) and the High-Pressure Bridgman (HPB) process. The study presented in this paper is based on MHB CZT substrates from the company Orbotech Medical Solutions Ltd. [Orbotech Medical Solutions Ltd., 10 Plaut St., Park Rabin, P.O. Box 2489, Rehovot, Israel, 76124]. Former studies have shown that high-work-function materials on the cathode side reduce the leakage current and, therefore, improve the energy resolution at lower energies. None of the studies have emphasized on the anode contact material. Therefore, we present in this paper the result of a detailed study in which for the first time the cathode material was kept constant and the anode material was varied. We used four different anode materials: Indium, Titanium, Chromium and Gold, metals with work-functions between 4.1 eV and 5.1 eV. The detector size was 2.0 x 2.0 x 0.5 cu cm with 8 x 8 pixels and a pitch of 2.46 mm. The best performance was achieved with the low-work-function materials Indium and Titanium with energy resolutions of 2.0 keV (at 59 keV) and 1.9 keV (at 122 keV) for Titanium and 2.1 keV (at 59 keV) and 2.9 keV (at 122 keV) for Indium. Taking into account the large pixel pitch of 2.46 mm, these resolutions are very competitive in comparison to those achieved with detectors made of material produced with the more expensive conventional HPB method. We present a detailed comparison of our detector response with 3D simulations. The latter comparisons allow us to determine the mobility-lifetime-products (mu tau-products) for electrons and holes. Finally, we evaluated the temperature dependency of the detector performance and ls-products. For many applications temperature dependence is important, therefore, we extended the scope of our study to temperatures as low as -30 C. There are two important results. The breakdown voltage increases with decreasing temperature, and electron mobility-lifetime-product decreases by about 30% over a range from 20 C to -30 C. The latter effect causes the energy resolution to deteriorate, but the concomitantly increasing breakdown voltage makes it possible to increase the applied bias voltage and restore the full performance

Jung, I.↗

Growth of CdZnTe Crystals for Radiation Detector Applications by Directional Solidification

Advances in Cadmium Zinc Telluride (Cd(sub 1-x)Zn(sub x)Te) growth techniques are needed for the production of large-scale arrays of gamma and x-ray astronomy. The research objective is to develop crystal growth recipes and techniques to obtain large, high quality CdZnTe single crystal with reduced defects, such as charge trapping, twinning, and tellurium precipitates, which degrade the performance of CdZnTe and, at the same time, to increase the yield of usable material from the CdZnTe ingot. A low gravity material experiment, "Crystal Growth of Ternary Compound Semiconductors in Low Gravity Environment", will be performed in the Material Science Research Rack (MSRR) on International Space Station (ISS). One section of the flight experiment is the melt growth of CdZnTe ternary compounds. This talk will focus on the ground-based studies on the growth of Cd(sub 0.80)Zn(sub 0.20)Te crystals for radiation detector applications by directional solidification. In this investigation, we have improved the properties that are most critical for the detector applications (electrical properties and crystalline quality): a) Electrical resistivity: use high purity starting materials (with reproducible impurity levels) and controlled Cd over pressure during growth to reproducibly balance the impurity levels and Cd vacancy concentration b) Crystalline quality: use ultra-clean growth ampoule (no wetting after growth), optimized thermal profile and ampoule design, as well as a technique for supercool reduction to growth large single crystal with high crystalline quality

Su, Ching-Hua↗

Development of a Silicon Tracker for the All-Sky Medium Energy Gamma-ray Observatory Prototype

The gamma-ray sky from several hundred keV to a hundred MeV has remained largely unexplored due to the challenging nature of detecting gamma rays in this regime. At lower energies, Compton scattering is the dominant interaction process whereas at higher energies pair production dominates, with a crossover at a few MeV. Thus, an instrument designed to work in this energy range must be optimized for both Compton and pair-production events. AMEGO, the All-sky Medium Energy Gamma-ray Observatory, a Probe-class mission in consideration for the 2020 decadal survey, is designed to operate at energies from 200 keV to > 10 GeV with over an order of magnitude increase in sensitivity and with superior angular and energy resolution compared to previous instruments. AMEGO comprises four major subsystems: a plastic anticoincidence detector for rejecting cosmic-ray events, a silicon tracker for tracking pair-production products and tracking and measuring the energies of Compton-scattered electrons, a cadmium-zinc-telluride (CZT) calorimeter for measuring the energy and location of Compton scattered photons, and a CsI calorimeter for measuring the energy of the pair-production products at high energies. A prototype instrument, known as ComPair, is under development at NASA’s Goddard Space Flight Center and the US Naval Research Laboratory. In this contribution, we provide details on the development of the silicon tracker subsystem.

Griffin, Sean↗

XL-Calibur - a second-generation balloon-borne hard X-ray polarimetry mission

XL-Calibur is a hard X-ray (15-80 keV) polarimetry mission operating from a stabilised balloon-borne platform in the stratosphere. It builds on heritage from the X-Calibur mission, which observed the accreting neutron star GX 301−2 from Antarctica, between December 29th 2018 and January 1st 2019. The XL-Calibur design incorporates an X-ray mirror, which focusses X-rays onto a polarimeter comprising a beryllium rod surrounded by Cadmium Zinc Telluride (CZT) detectors. The polarimeter is housed in an anticoincidence shield to mitigate background from particles present in the stratosphere. The mirror and polarimeter-shield assembly are mounted at opposite ends of a12 m long lightweight truss, which is pointed with arcsecond precision by WASP – the Wallops Arc Second Pointer. TheXL-Calibur mission will achieve a substantially improved sensitivity over X-Caliburby using a larger effective area X-ray mirror, reducing background through thinner CZT detectors, and improved anticoincidence shielding. When observing a 1 Crab source for t(day) days, the Minimum Detectable Polarisation (at 99% confidence level) is∼2%·t−1/2day. The energy resolution at 40 keV is∼5.9 keV. The aim of this paper is to describe the design and performance of the XL-Calibur mission, as well as the foreseen science programme.

Q Abarr↗

Radiation Effects in CdZnTe Gamma-Ray Detectors Produced by 199 MeV Protons

Many future space missions will use Cadmium Sinc Telluride (CdZnTe) gamma-ray detectors because their operation at room temperature makes compact, lightweight detector systems possible. Even though instruments for space using CdZnTe detectors have already been built, the effect of the high-energy particle space environment on these detectors has not been measured. To determine the effect of energetic charged particles on these detectors, we have bombarded seveal CdZnTe detectors with 199 MeV protons at the Indiana University Cyclotron Facility.

radiation↗

Semiconductor to Metal Transition in the Solids/Melts of Te and Pseudo-Binary of Hg1-xCdxTe for x = 0, 0.1 and 0.2

This paper reports the experimentally measured thermal and electrical conductivities from which the Lorenz numbers as functions of temperature were derived for the solids and melts of elemental Te and samples of Hg1-xCdxTe of x = 0, 0.1 and 0.2. The structural changes in the vicinity of the solid-liquid phase transition of elemental Te and various Hg1-xCdxTe solid solutions were assessed by closely examining these experimental properties and the derived Lorenz numbers. The values of Lorenz numbers for the solids of these samples were higher than the value of L0, i.e., the Lorenz number for the free electron gas derived by Sommerfeld, implying the characteristics of non-degenerate semiconductor. With the increasing value of x, or the larger bandgap, the materials become more non-degenerate with larger deviation from L0. As the solids started to melt, the measured values of Lorenz number for all samples started to decrease and eventually reached and maintained at values close to L0 at higher temperatures. The trend of the Lorenz number indicates that the transition from non-degenerate semiconductor of the solid samples to metal or degenerate semiconductor when the samples temperature reached above their liquidus temperatures.

thermal conductivity↗