Use of Modern Leak Detectors for the Calibration of Leak Standards.
Abstract not provided.
Forrest, Eric Christopher↗
SEARCH · Search NASA
Results for “CALIBRATION STANDARDS”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Photometer calibration error using extended standard sources
As part of a project to compare measurements of the night airglow made by the visible airglow experiment on the Atmospheric Explorer-C satellite, the standard light sources of several airglow observatories were compared with the standard source used in the absolute calibration of the satellite photometer. In the course of the comparison, it has been found that serious calibration errors (up to a factor of two) can arise when a calibration source with a reflecting surface is placed close to an interference filter. For reliable absolute calibration, the source should be located at a distance of at least five filter radii from the interference filter.
Torr, M. R.↗
Impact of lump characteristics on self-shielding corrections of active neutron interrogation on fissile material in waste - 15405
Non-destructive active neutron assay techniques such as active neutron coincidence counting, differential die away analysis or the californium shuffler method rely on the interrogation of fissile nuclear materials by an external neutron source. Whether it is a spontaneous fission or (α,n) neutron source, like {sup 252}Cf or AmLi; or a fusion neutron generator, all of these techniques rely on induced secondary fission events to provide prompt or delayed neutron signals that serve as the basis for the fissile material quantification. The accuracy of these fissile mass measurements is therefore dependent on the neutron interrogation efficiencies determined for calibration reference standards and whether the measured items are comparable to the calibration condition. In such favorable conditions, it is possible to establish a reliable empirical non-linear relationship between apparent (uncorrected) and real or true fissile mass. However, in waste measurements, this is unlikely to be the case; thus a calibration approach that takes account of the neutron self-shielding effect is required. By incorporating the Self-Shielding Factor (SSF) of the calibration reference standards, a linear mass calibration factor [s{sup -1}. {sup 239}Pu{sub eq} g{sup -1}] can be found; this calibration is accurate for waste in which the fissile material is 'infinitely dilute' i.e. the waste exhibits no self-shielding; this is assumed to be representative of dispersed material. The self-shielding correction and its systematic uncertainty are then left to be treated as part of the Total Measurement Uncertainty (TMU) evaluation associated with the assay result. The derivation of the TMU contribution associated with the self-shielding effect in nuclear waste is a complex problem for which a reliable evaluation has to be performed. This is usually based on assuming 'worst case scenarios' for the distribution of material that can arise in a particular waste stream. Such an approach is conservative, but often very penalizing, especially if one considers larger lumps (those containing grams of fissile material); for such lumps, the self-shielding correction becomes very significant, potentially altering the mass of {sup 239}Pu{sub eq} by over an order of magnitude. A worst case 'nuclear safety value' may not be the most appropriate choice for building a consignment best estimate or repository sentencing value for an item. In the present work the authors describe a numerical approach to study the variability of neutron self-shielding factors associated with distributions of a wide range of lump characteristics in terms of size, shape, chemical composition, density and isotopic composition. The described novel calculation tool is capable of accurately predicting the real impact of random distribution of lumps in a waste material, and allowed to show that given reasonable, defensible, assumptions on the composition of the lumps in waste stream, the systematic error component of the DDA TMU can be significantly reduced. (authors)
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
Calibration of the 11x11-Foot Transonic Wind Tunnel at NASA Ames Research Center
A static pipe calibration characterizing the streamwise static pressure distribution was conducted at the 11-By 11-Foot Transonic Wind Tunnel at NASA Ames Research Center. This data is used to determine the local Mach number within the test section and evaluate buoyancy corrections to axial force measurements. The 60 foot long, 6 inch diameter pipe contained 444 static pressure taps spanning the test section and nozzle regions of the tunnel. The forward end of the pipe extends into the settling chamber and is held by four cables mounting to the tunnel shell, and the aft end is fixed on the institutional model support system. A hydraulic cylinder at the aft end of the pipe provides tension on the system to reduce vibration and to keep the pipe as level as possible throughout the test section. The previous calibration was improved upon by using pressure scanners with greater accuracy, ensuring a uniform pressure tube length for each tap to control pneumatic lag, optically tracking any streamwise movement of the pipe, and more tightly controlling the tunnel condition set points. Typically this calibration is conducted with the pipe on tunnel centerline and 33 inches below centerline for sting-mounted models and semi-span (i.e. floor-mounted) models respectively, however schedule demands permitted only the centerline calibration. The semi-span calibration is planned to be completed in the summer of 2020. Immediately following the static pipe calibration, a shorter, 9 foot static pipe used as the calibration check standard was installed to obtain its first post-calibration pressure dataset. This short static pipe consists of 148 static pressure taps distributed along the pipe section and one total pressure tap at the end of an ogive nose. Performing the calibration test and its check standard back-to-back allows this dataset to establish a reliable baseline for future calibration check standard testing. Over time the use of a calibration check standard offers the ability to assess the stability of the calibration through statistical process control in an efficient and costeffective manner, thereby potentially increasing the time required between full tunnel calibrations.
White, Bethany↗
A new calibration method for time delay standard and its application
A method which is used to measure time delay accurately by using a Type 900-LB slotted line is described. The accuracy for calibrating time delay of a precision coaxial air line Type 900-L is about + or - (0.4 to 0.6)ps, and for coaxial cables with VSWR less than 1.5 and time delay t less than 50ns is about + or - (3 to 5)ps. Theoretical analysis and mathematical derivation of microwave networks in cascade are given. Methods to eliminate the errors which are caused by the discontinuities and the error analysis of the measuring system are presented. Skin effect analysis of the transient characteristic of coaxial transmission line are discussed in detail. Methods to eliminate the errors which result from using the calibrated time delay standard to calibrate time interval measurement instruments are presented. The estimation of errors and formulae for correction of those errors are described.
Su, B. W.↗
Low-Activity Waste Glass Standards Preparation and Characterization for Calibration of Analytical Instruments
A matrix of seven low-activity waste (LAW) glasses was fabricated and characterized to be used by the Hanford Waste Treatment and Immobilization Plant (WTP) as analytical instrument calibration and matrix interference standards when measuring LAW glass compositions. The matrix of glasses was designed to represent the range of LAW glass compositions that will be generated by the WTP. Samples from each of the seven glasses were measured with electron probe microanalysis (EPMA), ion chromatography (IC), and bulk inductively coupled plasma mass spectroscopy (ICP-MS) to determine the variability and accuracy across batches and within individually poured glass bar samples. High relative percent differences and standard deviations were calculated for components with low concentrations due to instrument detection limits. IC and ICP-MS percent differences and standard deviations were higher at low component concentrations. Otherwise, variability in measured compositions from IC and ICP-MS was generally lower than measurements from EPMA, with the exclusion of Cl, F, Si, and B. Overall, the two methods proved comparable and complementary. From EPMA, IC, and ICP-MS data, volatile elements were underrepresented compared to batched compositions, which suggested loss of these elements during melting. EPMA data was statistically analyzed to evaluate homogeneity within single bars and whole compositions for each of the seven glasses. Most of the variability within glass compositions occurred at the bar-to-bar level; however, no clear systematic trends were observed. Based on these analyses, when using these glasses as reference material, it is recommended that the overall mean and variance of each composition be used for performing instrument calibrations and analytical corrections.
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
A new high accuracy spectroradiometer
High accuracy spectroradiometer for calibration of spectral radiance standards
RADIATION MEASUREMENT↗
Spectral Irradiance Calibration in the Infrared: Comparison of (alpha) Bootis and 1 Ceres with a Laboratory Standard - 11
Infrared spectra of two celestial objects frequently used as flux standards are calibrated against an absolute laboratory flux standard at a spectral resolving power of 100 to 200. The spectrum of the KI.5 III star alpha Boo is measured from 3 to 30 microns, and that of the C-type asteroid 1 Ceres from 5 to 30 microns. While these "standard" spectra do not have the apparent precision of those based on calculated models, they do not require the assumptions involved in theoretical models of stars and asteroids. Specifically, they provide a model-independent means of calibrating celestial flux in the spectral range from 12 to 30 microns, where accurate absolute photometry is not available. The agreement found between the spectral shapes of alpha Boo and Ceres based on laboratory standards and those based on observed ratios to alpha CMa (Sirius) and alpha Lyr (Vega), flux-calibrated by theoretical modeling of these hot stars, strengthens our confidence in the applicability of the stellar models as primary irradiance standards.
Witteborn, Fred C.↗
Evaluating the effect of accuracy ratios on the percent of calibrations which are out of tolerance
The standard practice in calibration laboratories across the country, including the Measurement Standards and Calibration Laboratory (MSCL) at the Johnson Space Center, is to use accuracy ratios to determine if instruments are in-tolerance rather than computing the actual uncertainty associated with the instruments. In the past, the accepted practice was to use an accuracy ratio of 10:1, but then state of the art advanced to the point where the 10:1 ratio could no longer be maintained, and the ratio was arbitrarily lowered to 4:1. It is now becoming increasingly difficult to maintain the 4:1 accuracy ratio, and in some cases 1:1 is the best that can be achieved. However, the effect of using these small accuracy ratios on the number of mistakes made in classifying instruments as in or out of tolerance is completely unknown. In order to assess the effect of using accuracy ratios in calibration, a simulation program was written to compute the proportion of instruments determined to be out of tolerance which were actually in, denoted by alpha, and the proportion of instruments determined to be in-tolerance which were actually out, denoted by beta. This was done for accuracy ratios of 1:1 and 10:1, for one to five progressive calibrations, under varying standard and instrument conditions. Selected results are presented and explained.
Navard, Sharon E.↗
Spectral Irradiance Calibration in the Infrared 11: Comparison of (alpha) Boo and 1 Ceres with a Laboratory Standard
Infrared spectra of two celestial objects frequently used as flux standards are calibrated against an absolute laboratory flux standard at a spectral resolving power of 100 to 200. The spectrum of the K1.5III star, alpha Boo, is measured from 3 microns to 30 microns and that of the C-type asteroid, 1 Ceres, from 5 microns to 30 microns. While these 'standard' spectra do not have the apparent precision of those based on calculated models, they do not require the assumptions involved in theoretical models of stars and asteroids. Specifically they provide a model-independent means of calibrating celestial flux in the spectral range from 12 microns to 30 microns where accurate absolute photometry is not available. The agreement found between the spectral shapes of alpha Boo and Ceres based on laboratory standards, and those based on observed ratios to alpha CMa (Sirius) and alpha Lyr (Vega), flux calibrated by theoretical modeling of these hot stars strengthens our confidence in the applicability of the stellar models as primary irradiance standards.
Witteborn, Fred C.↗
Using an Absolute Cavity Pyrgeometer to Validate the Calibration of a Transfer Standard Pyrgeometer Outdoors, Independent from the Reference Value of the Atmospheric Longwave Irradiance
A unique method of pyrgeometer calibration has been developed to improve the measurement uncertainty [1]. The results of this method yielded irradiance values within ±3 W/m2 of those traceable to the World InfraRed Standard Group (WISG). The ACPs and pyrgeometer model PIR were deployed outdoors, and the irradiance measured by the PIR was compared against the irradiance measured by ACP95F3. Based on the results it is possible to achieve an uncertainty of ± 3.51 W/m2. These results suggest that the PIR calibration method might be useful in addressing the international need for a secondary standard pyrgeometer traceable to SI.
absolute cavity pyrgeometer↗
SeaWiFS Postlaunch Technical Report Series: The Fifth Sea-WiFS Intercalibration Round-Robin Experiment (SIRREX-5), July 1996 - Volume 7
This report documents the fifth Sea-viewing Wide Field-of-view Sensor (SeaWiFS) Intercalibration Round-Robin Experiment (SIRREX-5), which was held at the National Institute of Standards and Technology (NIST) on 23-30 July 1996. The agenda for SIRREX-5 was established based on recommendations made during SIRREX-4. For the first time in a SIRREX activity, instrument intercomparisons were performed at field sites, which were near NIST. The goals of SIRREX-5 were to continue the emphasis on training and the implementation of standard measurement practices, investigate the calibration methods and measurement chains in use by the oceanographic community, provide opportunities for discussion, and intercompare selected instruments. As at SIRREX-4, the day was divided between morning lectures and afternoon laboratory exercises. A set of core laboratory sessions were performed: 1) in-water radiant flux measurements; 2) in-air radiant flux measurements; 3) spectral radiance responsivity measurements using the plaque method; 4) device calibration or stability monitoring with portable field sources; and 5) various ancillary exercises designed to illustrate radiometric concepts. Before, during, and after SIRREX-5, NIST calibrated the SIRREX-5 participating radiometers for radiance and irradiance responsivity. The Facility for Automated Spectroradiometric Calibrations (FASCAL) was scheduled for spectral irradiance calibrations for standard lamps during SIRREX-5. Three lamps from the SeaWiFS community were submitted and two were calibrated.
Hooker, Stanford B.↗
Tables for calibrating altimeters and computing altitudes based on the standard atmosphere
During 1925 the assumption of an isothermal atmosphere which was in general use as the standard for the calibration of altimeters in the United States was replaced by a standard atmosphere which assumes an altitude-temperature relation closely corresponding to the average of upper air observations at latitude 40 degrees in this country. The same standard atmosphere had already been adopted somewhat earlier in the United States as the aircraft performance standard. National Advisory Committee for Aeronautics Technical Reports nos. 147 and 218 give necessary constants, tables, and information. However, neither of these reports includes all of the tables required for the computation of actual altitudes nor those readily suitable for use in calibrating altimeters, since the altitude intervals for which data are given are not sufficiently small. The present report has been prepared specifically for these purposes. The formulas which define the standard atmosphere are given in this report, together with other formulas giving the corrections to be applied to the standard altitude in order to obtain the actual altitude when the necessary observations of pressure and temperature are available. The tables necessary for the use of this standard atmosphere in calibrating altimeters and in computing altitudes form the principal part of this report. An example of the computation of actual altitudes from observed pressures and temperatures are given in table IV.
Brombacher, W G↗
Calibration source maintenance, characterization and development
The Standards and Calibration Office maintains visible and near infrared calibration sources for the use of various GSFC organizations instrument calibration needs and related field activities. These are large aperture spherical and hemispherical integrating sources designed to provide a spatially uniform absolute spectral radiance with a well-defined angular uniformity characteristic. In essence, the calibration and characterization efforts involve monitoring and documenting the stability and the absolute radiance of these calibration sources. These sources are recalibrated on a regular basis to both document any changes that might occur in the output of the sources and to provide the most up-to-date calibration data for the source users. Efforts included comparing the calibration numbers with those of a commercial calibration laboratory that was engaged to do independent calibrations. However, the most recent calibrations done by the independent laboratory and those done by GSFC personnel show a rather large discrepancy (10 to 15 percent). Efforts are underway to resolve these differences.
Mclean, J. T.↗
Using an Absolute Cavity Pyrgeometer to Validate the Calibration of a Secondary Standard Pyrgeometer Outdoors, Independent from the Reference Value of the Atmospheric Longwave Irradiance
Accurate measurements of broadband outdoor longwave irradiance are important for renewable energy applications and the study of the atmosphere and climate change. A unique method of pyrgeometer calibration has been developed to improve the measurement uncertainty [1]. The results of this method yielded irradiance values within ±3 W/m 2 of those traceable to the World InfraRed Standard Group (WISG). This article describes a technique for validating this pyrgeometer calibration method using two Absolute Cavity Pyrgeometers (ACPs). The ACPs and pyrgeometer model PIR were deployed outdoors and the irradiance measured by the PIR was compared against the average irradiance measured by the two ACPs. The irradiance measured by the PIR was calculated using two equations, NREL equation and the Physikalisch Meteorologisches Observatorium Davos (PMOD) equation. The uncertainty with 95% confidence level ( U 95 ) of the irradiance measured by the PIR using NREL equation equaled ±3.51 W/m 2 with respect to SI and using PMOD equation U 95 equaled ±2.99 W/m 2 with respect to SI. These results suggest that the PIR calibration method might be useful in addressing the international need for a secondary standard pyrgeometer traceable to SI.
54 ENVIRONMENTAL SCIENCES↗
On Calibrations Using the Crab Nebula as a Standard Candle
Inspired by a recent paper (Kirsch et al. 2005) on possible use of the Crab Nebula as a standard candle for calibrating X-ray response func tions, we examine possible consequences of intrinsic departures from a single (absorbed) power law upon such calibrations. We limited our analyses to three more modern X-ray instruments -- the ROSAT/PSPC, th e RXTE/PCA, and the XMM-Newton/EPIC-pn. The results are unexpected an d indicate a need to refine two of the three response functions studi ed. The implications for Chandra will be discussed.
Weisskopf, Martin↗
Apollo experience report: Flight instrumentation calibration
Three types of instrumentation-calibration data were used in the Apollo Program to provide the correct engineering data for tests and mission support. The command and service module instrumentation-component procurement specifications required individual-component calibration, and calibration data for these individual components (conventional-calibration data) were always used for mission data support. A mean standard type of calibration data derived from a statistical sampling of conventional-calibration data was used for test and checkout during the latter part of the Apollo Program. The lunar module instrumentation procurement specification permitted the use of standard-calibration data. These data were applicable to similarly instrumented measurements. The definition, merit, and application of each type of data are discussed.
Demoss, J. F.↗
Evaluating Statistical Process Control (SPC) techniques and computing the uncertainty of force calibrations
In recent years there has been a push within NASA to use statistical techniques to improve the quality of production. Two areas where statistics are used are in establishing product and process quality control of flight hardware and in evaluating the uncertainty of calibration of instruments. The Flight Systems Quality Engineering branch is responsible for developing and assuring the quality of all flight hardware; the statistical process control methods employed are reviewed and evaluated. The Measurement Standards and Calibration Laboratory performs the calibration of all instruments used on-site at JSC as well as those used by all off-site contractors. These calibrations must be performed in such a way as to be traceable to national standards maintained by the National Institute of Standards and Technology, and they must meet a four-to-one ratio of the instrument specifications to calibrating standard uncertainty. In some instances this ratio is not met, and in these cases it is desirable to compute the exact uncertainty of the calibration and determine ways of reducing it. A particular example where this problem is encountered is with a machine which does automatic calibrations of force. The process of force calibration using the United Force Machine is described in detail. The sources of error are identified and quantified when possible. Suggestions for improvement are made.
Navard, Sharon E.↗