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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 325 records · Page 18

The effects of space radiation on thin films of YBa2Cu3O(sub 7-x)

This investigation had two objectives: (1) to determine the effects of space radiation on superconductor parameters that are most important in space applications; and (2) to determine whether this effect can be simulated with Co-60 gamma rays, the standard test method for space materials. Thin films of yttrium barium copper oxide (YBCO) were formed by coevaporation of Y, BaF2, and Cu and post-annealing in wet oxygen at 850 C for 3.5 h. The substrate used was (100) silicon with an evaporated zirconia buffer layer. The samples were characterized by four point probe electrical measurements as a function of temperature. The parameters measured were the zero resistance transition temperature (T sub c) and the room temperature resistance. The samples were then exposed to Co-60 gamma-rays in air and in pure nitrogen, and to 780 keV electrons, in air. The parameters were then remeasured. The results are summarized. The results indicate little or no degradation in the parameters measured for samples exposed up to 10 Mrads of gamma-rays in nitrogen. However, complete degradation of samples exposed to 10-Mrad in air was observed. This degradation is preliminarily attributed to the high level of ozone generated in the chamber by the gamma-ray interaction with air. It can be concluded that: (1) the electron component of space radiation does not degrade the critical temperature of the YBCO films described, at least for energies around 800 keV and doses similar to those received by surface materials on spacecraft in typical remote sensing missions; and (2) for qualifying this and other superconducting materials against the space-radiation threat the standard test method in the aerospace industry, namely, exposure to Co-60 gamma-rays in air, may require some further investigation. As a minimum, the sample must be either in vacuum or in positive nitrogen pressure.

Herschitz, R.↗

Lightning flashes triggered in altitude by the rocket and wire technique

Electrical measurements were conducted in 1987 and 1988 on streamer and leader discharges occurring during the first stages of a triggered flash. This paper describes the pulsing phenomenon observed at positive leader onset (typical pulsing rate 25 microns), and it is shown that the same process happened in the case of the ignition of a flash triggered in altitude; with a wire several hundred meters long, positive leader propagates alone for several ms before the ignition of the downward negative stepped leader.

Laroche, P.↗

Electrical characterization of chemically modified YBa2Cu3O(7-x) surfaces

Results on electrical characterization of YBa2Cu3O(7-x) thin-film surfaces treated with a Br/ethanol chemical etch are presented. Electrical measurements of YBa2Cu3O(7-x)/Au/Nb device structures fabricated using polycrystalline, post-annelaed YBa2Cu3O(7-x) films with Br-etched surfaces, show improvements of approximately one or two orders of magnitude in current densities and resistivities (resistance-area products) relative to unetched devices. The existence of supercurrents in these structures has been confirmed by observation of the ac Josephson effect, and by magnetic field and temperature studies of the critical currents. The Br-etch process has produced 10 x 10 sq micron devices with critical current densities greater than 400 A/sq cm and resistivities as low as 4 x 10 to the -7th ohm/sq cm.

Hunt, B. D.↗

Cross-Quint-Bridge Resistor

Integrated-circuit conductive test pattern intended to provide data on effects of design widths and design spacings upon actual widths of conductive lines. Provides for electrical measurements both on lines of unknown width and on features having known dimensions. Data from measurements on five bridges used to determine four parameters of mathematical model describing system. In principle, pattern determines effects of width and spacing and interaction between them.

Hannaman, David J.↗

RSRM top hat cover simulator lightning test, volume 1

The test sequence was to measure electric and magnetic fields induced inside a redesigned solid rocket motor case when a simulated lightning discharge strikes an exposed top hat cover simulator. The test sequence was conducted between 21 June and 17 July 1990. Thirty-six high rate-of-rise Marx generator discharges and eight high current bank discharges were injected onto three different test article configurations. Attach points included three locations on the top hat cover simulator and two locations on the mounting bolts. Top hat cover simulator and mounting bolt damage and grain cover damage was observed. Overall electric field levels were well below 30 kilowatts/meter. Electric field levels ranged from 184.7 to 345.9 volts/meter and magnetic field levels were calculated from 6.921 to 39.73 amperes/meter. It is recommended that the redesigned solid rocket motor top hat cover be used in Configuration 1 or Configuration 2 as an interim lightning protection device until a lightweight cover can be designed.

Source record↗

Sputtered Ta-Si-N diffusion barriers in Cu metallizations for Si

Electrical measurements on shallow Si n+-p junction diodes with a 30-nm TiSi2 contacting layer demonstrate that an 80-nm-thick amorphous Ta36Si14N50 film prepared by reactive RF sputtering of a Ta5Si3 target in an Ar/N2 plasma very effectively prevents the interaction between the Si substrate with the TiSi2 contacting layer and a 500-nm Cu overlayer. The Ta36Si14N50 diffusion barrier maintains the integrity of the I-V characteristics up to 900 C for 30-min annealing in vacuum. It is concluded that the amorphous Ta36Si14N50 alloy is not only a material with a very low reactivity for copper, titanium, and silicon, but must have a small diffusivity for copper as well.

Kolawa, E.↗

The effects of space radiation on thin films of YBa2Cu3O(7-x)

This investigation had two objectives: (1) to determine the effects of space radiation on superconductor parameters that are most important in space applications; and (2) to determine whether this effect can be simulated with Co-60 gamma rays, the standard test method for space materials. Thin films of yttrium barium copper oxide (YBCO) were formed by coevaporation of Y, BaF2, and Cu and post-annealing in wet oxygen at 850 C for 3.5 h. The substrate used was (100) silicon with an evaporated zirconia buffer layer. The samples were characterized by four point probe electrical measurements as a function of temperature. The parameters measured were the zero resistance transition temperature T(sub c) and the room temperature resistance. The samples were then exposed to Co-60 gamma-rays in air and in pure nitrogen, and to 780 keV electrons, in air. The parameters were then remeasured. The results are summarized. The results indicate little or no degradation in the parameters measured for samples exposed up to 10 Mrads of gamma-rays in nitrogen. However, complete degradation is preliminarily attributed to the high level of ozone generated in the chamber by the gamma-ray interaction with air. It can be concluded that: (1) the electron component of space radiation does not degrade the critical temperature of the YBCO films described, at least for energies around 800 keV and doses similar to those received by surface materials on spacecraft in typical remote sensing missions; and (2) for qualifying this and other superconducting materials against the space-radiation threat the standard test method used in the aerospace industry, namely, exposure to Co-60 gamma-rays in air, may require some further investigation. As a minimum, the sample must be either in vacuum or in positive nitrogen pressure.

Herschitz, R.↗

LEO effects on candidate solar cell cover materials

The Long Duration Exposure Facility (LDEF) test samples discussed within are part of the Solar Array Materials Passive (SAMPLE) LDEF experiment, which included contributions from NASA and Jet Propulsion Lab (JPL). Only the JPL portion is described in this paper. The JPL test plate contains 30 individual thin silicon solar cell/cover samples. It was the intent of the experiment to evaluate the stability and protective capability of various cover materials such as conventional fused silica and potential alternative materials such as Teflon, silicone RTV's, glass resins, polyimides, and a copolymer encapsulate. Examination of the recovered experiment shows extensive physical changes have occurred. Approximately 150 micrometeoroid/debris impact were noted, some directly on the solar cells. Of particular interest are the results of ultraviolet and atomic oxygen interactions with the various cover materials. Initial results show that the fused silica cover is the most stable and protective, with performance of other materials varying widely. Electrical measurements of the cell/cover samples are presented as part of the evaluation of cover materials to protect cells in low earth orbit environments.

Stella, Paul M.↗

Neutron, gamma ray, and temperature effects on the electrical characteristics of thyristors

Experimental data showing the effects of neutrons, gamma rays, and temperature on the electrical and switching characteristics of phase-control and inverter-type SCR's are presented. The special test fixture built for mounting, heating, and instrumenting the test devices is described. Four SCR's were neutron irradiated at 300 K and four at 365 K for fluences up to 3.2 x 10 exp 13 n/sq. cm, and eight were gamma irradiated at 300 K only for gamma doses up to 5.1 Mrads. The electrical measurements were made during irradiation and the switching measurements were made only before and after irradiation. Radiation induced crystal defects, resulting primarily from fast neutrons, caused the reduction of minority carrier lifetime through the generation of R-G centers. The reduction in lifetime caused increases in the on-state voltage drop and in the reverse and forward leakage currents, and decreases in the turn-off time.

Frasca, A. J.↗

Growth and electrical properties of ultrafine fibers

This paper reports on free-standing ultrafine fibers formed using the gas-evaporation method in the presence of electric fields. Materials up to 10 cm in length have been prepared in this way. Electrical measurements on Pd fibers 3 mm in length and about 200-300 A in diameter are given.

Webb, G. W.↗

Neutron, gamma ray, and temperature effects on the electrical characteristics of thyristors

Experimental data showing the effects of neutrons, gamma rays, and temperature on the electrical and switching characteristics of phase-control and inverter-type SCR's are presented. The special test fixture built for mounting, heating, and instrumenting the test devices is described. Four SCR's were neutron irradiated at 300 K and four at 365 K for fluences up to 3.2 x 10 exp 13 pn/sq. cm, and eight were gamma irradiated at 300 K only for gamma doses up to 5.1 Mrads. The electrical measurements were made during irradiation and the switching measurements were made only before and after irradiation. Radiation induced crystal defects, resulting primarily from fast neutrons, caused the reduction of minority carrier lifetime through the generation of R-G centers. The reduction in lifetime caused increases in the on-state voltage drop and in the reverse and forward leakage currents, and decreases in the turn-off time.

Frasca, A. J.↗

Search for new high temperature thermoelectric materials

Although important efforts are actually devoted to improve Si-Ge materials, their thermoelectric energy conversion efficiency remains relatively low and the nondimensional ZT value does not exceed 1. Higher values can be obtained by investigating new materials. A search for new high temperature thermoelectric materials identified a certain number of compounds between transition metals and bismuth, antimony and germanium as potential candidates. Results of the preliminary synthesis of samples by a variety of techniques (Bridgman, mechanical alloying) are presented as well as some electrical measurements. Some compounds showed interesting properties and need to be investigated in more details.

Caillat, Thierry↗

Near-equilibrium growth of thick, high quality beta-SiC by sublimation

A close spaced near-equilibrium growth technique was used to produce thick, high quality epitaxial layers of beta-silicon carbide. The process utilized a sublimation method to grow morphologically smooth layers. The beta silicon carbide growth layers varied from about 200 to 750 microns in thickness. Chemical vapor deposition grown, 2-10 microns, beta silicon carbide films were used as seeds at 1860 and 1910 C growth temperatures. The respective average growth rates were 20 and 30 microns per hour. The layers are p-type with a 3.1 x 10 exp 17/cu cm carrier concentration. Electrical measurements indicate considerable improvement in the breakdown voltage of Schottky barriers on growth samples. Breakdown values ranged from 25 to 60 V. These measurements represent the highest values reported for 3C-SiC.

Shields, Virgil B.↗

FNAS/solar flare energetics

We have performed an extensive study of solar flare energy buildup and release, concentrating in two aspects: (1) relationship with 3D field topology and measured electric currents; and (2) flare onset characteristics as determined from combined x ray and ultraviolet observations. We extended our previous studies on the characteristic topology of flaring regions, by following the evolution of an active region over three consecutive days. From comparison with flare observations in x rays and h alpha, we found further support for the hypothesis that flares were triggered by taking place at the separators (3D generalization of and x-type neutral point). Furthermore, we found that emerging in flux at a site within the active regions where no (or little) activity was previously observed, caused the appearance of a secondary separator and thereon continuous triggering of activity at such site. Our topology arguments were then applied to a study of sympathetic activity between two regions within an active complex. Here again we found that interacting field structures along separators and separatrices, which act as pathways for recurrent flaring to spread between the regions, could be used to understand how activity spread to potentially explosive sites with the complex. We also finished our study of flare onset characteristics as determined from combined x ray and ultraviolet observations. Using a quasi-static modeling approach, we find that this phase is characterized by a relatively low level of energy release, 10 exp 26-27 erg/s, which is sufficient to produce 'gentle' evaporation, a shift in the location of the transition zone as compared to pre-flare conditions, and an increase in the temperature and density of coronal loops. All these changes have profound implications on the observed signatures of impulsive phase phenomena, which had been neglected in the past. As a follow-up of this investigation, we now plan to apply our results to the interpretation of high-sensitivity spectroscopic and hard x-ray data currently being gathered by the Yohkoh and Compton Gamma Ray Observatory satellites.

Machado, M. E.↗

Experiments in diamond film fabrication in table-top plasma apparatus

The objectives of this experiment are to illustrate the process of plasma assisted chemical vapor deposition and to show devices which can be made simply in the laboratory. These devices illustrate clearly the concepts of bandgap, junctions, and photoelectronic processes. Films and devices are measured electrically, optically, and thermally.

Masi, James V.↗

Field and data analysis studies related to the atmospheric environment

This report summarizes work on a broad array of projects including: (1) applications of meteorological and/or oceanographic satellites; (2) improvement of the current set of NASA/USAF lightning related launch commit criteria rules; (3) the design, building, testing and deployment of a set of cylindrical field mills for aircraft use; (4) the study of marginal electrification storm conditions in relationship to the current launch commit rules for the space shuttle and various other launch vehicles using an instrumented aircraft; (5) support of the DC-8 and ER-2 lightning instrument package as part of both the Tropical Ocean - Global Atmospheric/Coupled Ocean-Atmospheric Response Experiment and the Convection and Moisture Experiment; (6) design of electronic circuitry and microprocessor firmware for the NASA Advanced Ground Based Field Mill; (7) design and testing of electronic and computer instrumentation for atmospheric electricity measurements; (8) simulating observations from a lightning imaging sensor on the Tropical Rainfall Measuring satellite; and (9) supporting scientific visualization and the development of computer software tools.

Kidder, Stanley↗

Seeded Physical Vapor Transport of Cadmium-Zinc Telluride Crystals: Growth and Characterization

Crystals of Cd(1-x)Zn(x)Te with x = 0.2 and 40 g in weight were grown on monocrystalline cadmium-zinc telluride seeds by closed-ampoule physical vapor transport with or without excess (Cd + Zn) in the vapor phase. Two post-growth cool-down rates were used. The crystals were characterized using low temperature photoluminescence, atomic force microscopy, chemical etching, X-ray diffraction and electrical measurements. No formation of a second, ZnTe-rich phase was observed.

Palosz, W.↗

Morphology and Structure of ZnO Films Synthesized by Off-Axis Sputtering Deposition

ZnO is a wide-band-gap oxide material that has many applications. A new potential application of ZnO material is for light emitting devices since its structure and electrical properties are similar to that of the GaN material (a blue laser candidate). It also is a good substrate for fabricating GaN-based devices. Off-axis sputtering technique has revealed great potential in synthesizing excellent oxide materials because the negative ion bombardment is greatly reduced when adatoms condense on substrates. The surface of films grown by off-axis sputtering will be much smoother than that produced in a regular sputtering configuration. A growth mechanism is studied by investigating the morphology and structure of ZnO films under different growth conditions and orientations. ZnO films are deposited on (0001) sapphire and quartz substrates by off- axis sputtering deposition at various oxygen/argon mixture ratios and pressures and at different temperatures. All films reveal highly textured structures on quartz substrates and epitaxial growth on sapphire substrates. Two off-axis configurations, vertical and horizontal orientations are conducted to study the process of film growth, surface morphology, and film structure. X-ray diffraction, scanning probe microscopy, and electrical measurements are used to characterize these films. Detailed results will be discussed in the presentation. Keywords: ZnO, Photonic material, Off-axis sputtering, Growth mechanism

Zhu, Shen↗