Analytical photoionization mass spectrometer with an argon gas filter between the light source and monochrometer Patent
Analytical photoionization mass spectrometer with argon gas filter between light source and monochrometer
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Analytical photoionization mass spectrometer with argon gas filter between light source and monochrometer
The development of flight suitable analyzer units for that part of the GIOTTO Ion Mass Spectrometer (IMS) experiment designated the High Energy Range Spectrometer (HERS) is discussed. Topics covered include: design of the total ion-optical system for the HERS analyzer; the preparation of the design of analyzing magnet; the evaluation of microchannel plate detectors and associated two-dimensional anode arrays; and the fabrication and evaluation of two flight-suitable units of the complete ion-optical analyzer system including two-dimensional imaging detectors and associated image encoding electronics.
The present invention provides an improved electron ionizer for use in a quadrupole mass spectrometer. The improved electron ionizer includes a repeller plate that ejects sample atoms or molecules, an ionizer chamber, a cathode that emits an electron beam into the ionizer chamber, an exit opening for excess electrons to escape, at least one shim plate to collimate said electron beam, extraction apertures, and a plurality of lens elements for focusing the extracted ions onto entrance apertures.
A miniature quadrupole mass spectrometer array has been designed and built for NASA flight missions.
Design, test evaluation, and performance failure analysis of ion mass spectrometer for OGO-F
Measurement of the neutral atmospheric composition above Fort Churchill, Canada (59 N, 94 W), by mass spectrometers in two rocket flights at 0835 CST on Feb. 4 and 6, 1969. A quantitative measure for the extent of agreement with static diffusive equilibrium is introduced, and substantial agreement with profiles predicted when static diffusive equilibrium was assumed is found for all constituents including helium. A sensitive search for atomic nitrogen yielded upper limits of a few per cent for one flight and of 0.2% for the other.
A method of analyzing soil samples with a mass spectrometer employing a spark-discharge ion source is described, and the effectiveness of the method is demonstrated by applying it to the determination of impurities, in amounts of less than 10 mg, in lunar samples. It is shown that four parts of the Luna-20 lunar highland sample differ in their chemical composition.
We present details of a miniature integrated time-of-flight mass spectrometer and sample handling system under development to address some of the needs for in situ sample analysis on landed missions. Additional information is contained in the original extended abstract.
The composition of the lower atmosphere of the planet Venus from 62 km to the surface was measured by a neutral gas mass spectrometer onboard of the Pioneer Venus Sounder Probe. Fifty-one mass spectra were obtained with an average altitude resolution of approximately 1 km. The instrument measured the composition of the gases relative to CO2, the dominant gas, that is sampled from the Venus atmosphere through a special leak. The mass range extended from 1 to 208 amu with a sensitivity of the order of 1 ppm relative to CO2, but for the noble gases it was nearly 100 times better. A description of the instrument and the initial results are reported.
Bacteria and other micro-organisms identified continously with aid of new technique for producing samples for mass spectrometer. Technique generates aerosol of organisms and feeds to spectrometer. Given species of organism produces characteristic set of peaks in mass spectrum and thereby identified. Technique useful for monitoring bacterial makeup in environmental studies and in places where cleanliness is essential, such as hospital operating rooms, breweries, and pharmaceutical plants.
Ablation products and high temperature boundary layer chemistry of polytetrafluoroethylene /Teflon/ in arc jet streams using mass spectrometer
A survey of mechanical vacuum pumps was completed. A small Roots blower for flight mass spectrometer applications was evaluated with respect to system operating parameters in a number of different modes of operation. The survey indicated that a metal bellows pump might be a viable alternative for the systems requirements. The results of the study are given, including current status of possible flight-type pumps, a systems analysis using available pumps, and recommendations for fabrication and tests of a potential flight-type pump.
The seasonal-latitudinal and the diurnal variations of composition observed by mass spectrometers on the Ogo 6 satellite are represented by two simple empirical formulas. The formulas are of a very general nature and predict the behavior of these variations at all heights and for all levels of solar activity; they yield a satisfactory representation of the corresponding variations in total density, as derived from satellite drag. It is suggested that a seasonal variation of hydrogen may explain the abnormally low hydrogen densities at high northern latitudes in July 1964.
The Mass Spectrometer Telescope (MAST) on SAMPEX is designed to provide high resolution measurements of the isotopic composition of energetic nuclei from He to Ni (Z = 2 to 28) over the energy range from about 10 to several hundred MeV/nuc. During large solar flares MAST will measure the isotopic abundances of solar energetic particles to determine directly the composition of the solar corona, while during solar quiet times MAST will study the isotopic composition of galactic cosmic rays. In addition, MAST will measure the isotopic composition of both interplanetary and trapped fluxes of anomalous cosmic rays, believed to be a sample of the nearby interstellar medium.
We present the first published method to convert data obtained by the Pioneer Venus Large Probe Neutral Mass Spectrometer (LNMS) into units of mixing ratio (ppm) and volume percent (v%) against CO 2 and N 2 , the dominant Venus atmospheric gases, including conversion to density (kg m −3 ). These unit conversions are key to unlocking the untapped potential of the data, which represents a significant challenge given the scant calibration data in the literature. Herein, we show that our data treatments and conversions yield mixing ratios and volume percent values for H 2 O, N 2 , and SO 2 that are within error to those reported for the gas chromatograph (LGC) on the Pioneer Venus Large Probe (PVLP). For the noble gases, we developed strategies to correct for instrument biases by treating the data as a relative scale and using PVLP and Venera-based measurements as calibration points. Together, these methods, conversions, calibrations, and comparisons afford novel unit conversions for the LNMS data and yield unified measures for Venus’ atmosphere from the LNMS and LGC on the PVLP. - Conversion into mixing ratio (ppm), volume percent (v%), and density (kg m −3 ). - Mixing ratios are expressed against CO 2 and N 2 . - LNMS and LGC measurements on the PVLP are consistent.
Construction of breadboard electronic system for cold cathode quadrupole mass spectrometer
Ion detection and monopole mass spectrometer performance tests with transverse magnetic field and titanium getter pump pumping capacity for D region ion composition analysis
The seasonal-latitudinal and the diurnal variations of composition observed by mass spectrometers on the OGO 6 satellite are represented by two simple empirical formulae, each of which uses only one numerical parameter. The formulae are of a very general nature and predict the behavior of these variations at all heights and for all levels of solar activity; they yield a satisfactory representation of the corresponding variations in total density as derived from satellite drag. It is suggested that a seasonal variation of hydrogen might explain the abnormally low hydrogen densities at high northern latitudes in July 1964.