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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 325 records · Page 18

Iridium Interfacial Stack - IrIS

Iridium Interfacial Stack (IrIS) is the sputter deposition of high-purity tantalum silicide (TaSi2-400 nm)/platinum (Pt-200 nm)/iridium (Ir-200 nm)/platinum (Pt-200 nm) in an ultra-high vacuum system followed by a 600 C anneal in nitrogen for 30 minutes. IrIS simultaneously acts as both a bond metal and a diffusion barrier. This bondable metallization that also acts as a diffusion barrier can prevent oxygen from air and gold from the wire-bond from infiltrating silicon carbide (SiC) monolithically integrated circuits (ICs) operating above 500 C in air for over 1,000 hours. This TaSi2/Pt/Ir/Pt metallization is easily bonded for electrical connection to off-chip circuitry and does not require extra anneals or masking steps. There are two ways that IrIS can be used in SiC ICs for applications above 500 C: it can be put directly on a SiC ohmic contact metal, such as Ti, or be used as a bond metal residing on top of an interconnect metal. For simplicity, only the use as a bond metal is discussed. The layer thickness ratio of TaSi2 to the first Pt layer deposited thereon should be 2:1. This will allow Si from the TaSi2 to react with the Pt to form Pt2Si during the 600 C anneal carried out after all layers have been deposited. The Ir layer does not readily form a silicide at 600 C, and thereby prevents the Si from migrating into the top-most Pt layer during future anneals and high-temperature IC operation. The second (i.e., top-most) deposited Pt layer needs to be about 200 nm to enable easy wire bonding. The thickness of 200 nm for Ir was chosen for initial experiments; further optimization of the Ir layer thickness may be possible via further experimentation. Ir itself is not easily wire-bonded because of its hardness and much higher melting point than Pt. Below the iridium layer, the TaSi2 and Pt react and form desired Pt2Si during the post-deposition anneal while above the iridium layer remains pure Pt as desired to facilitate easy and strong wire-bonding to the SiC chip circuitry.

Spry, David↗

Contamination Control Assessment of the World's Largest Space Environment Simulation Chamber

The Space Power Facility s thermal vacuum test chamber is the largest chamber in the world capable of providing an environment for space simulation. To improve performance and meet stringent requirements of a wide customer base, significant modifications were made to the vacuum chamber. These include major changes to the vacuum system and numerous enhancements to the chamber s unique polar crane, with a goal of providing high cleanliness levels. The significance of these changes and modifications are discussed in this paper. In addition, the composition and arrangement of the pumping system and its impact on molecular back-streaming are discussed in detail. Molecular contamination measurements obtained with a TQCM and witness wafers during two recent integrated system tests of the chamber are presented and discussed. Finally, a concluding remarks section is presented.

Snyder, Aaron↗

Bismuth Passivation Technique for High-Resolution X-Ray Detectors

The Athena-plus team requires X-ray sensors with energy resolution of better than one part in 3,000 at 6 keV X-rays. While bismuth is an excellent material for high X-ray stopping power and low heat capacity (for large signal when an X-ray is stopped by the absorber), oxidation of the bismuth surface can lead to electron traps and other effects that degrade the energy resolution. Bismuth oxide reduction and nitride passivation techniques analogous to those used in indium passivation are being applied in a new technique. The technique will enable improved energy resolution and resistance to aging in bismuth-absorber-coupled X-ray sensors. Elemental bismuth is lithographically integrated into X-ray detector circuits. It encounters several steps where the Bi oxidizes. The technology discussed here will remove oxide from the surface of the Bi and replace it with nitridized surface. Removal of the native oxide and passivating to prevent the growth of the oxide will improve detector performance and insulate the detector against future degradation from oxide growth. Placing the Bi coated sensor in a vacuum system, a reduction chemistry in a plasma (nitrogen/hydrogen (N2/H2) + argon) is used to remove the oxide and promote nitridization of the cleaned Bi surface. Once passivated, the Bi will perform as a better X-ray thermalizer since energy will not be trapped in the bismuth oxides on the surface. A simple additional step, which can be added at various stages of the current fabrication process, can then be applied to encapsulate the Bi film. After plasma passivation, the Bi can be capped with a non-diffusive layer of metal or dielectric. A non-superconducting layer is required such as tungsten or tungsten nitride (WNx).

Chervenak, James↗

VUV Testing of Science Cameras at MSFC: QE Measurement of the CLASP Flight Cameras

The NASA Marshall Space Flight Center (MSFC) has developed a science camera suitable for sub-orbital missions for observations in the UV, EUV and soft X-ray. Six cameras were built and tested for the Chromospheric Lyman-Alpha Spectro-Polarimeter (CLASP), a joint National Astronomical Observatory of Japan (NAOJ) and MSFC sounding rocket mission. The CLASP camera design includes a frame-transfer e2v CCD57-10 512x512 detector, dual channel analog readout electronics and an internally mounted cold block. At the flight operating temperature of -20 C, the CLASP cameras achieved the low-noise performance requirements (less than or equal to 25 e- read noise and greater than or equal to 10 e-/sec/pix dark current), in addition to maintaining a stable gain of approximately equal to 2.0 e-/DN. The e2v CCD57-10 detectors were coated with Lumogen-E to improve quantum efficiency (QE) at the Lyman- wavelength. A vacuum ultra-violet (VUV) monochromator and a NIST calibrated photodiode were employed to measure the QE of each camera. Four flight-like cameras were tested in a high-vacuum chamber, which was configured to operate several tests intended to verify the QE, gain, read noise, dark current and residual non-linearity of the CCD. We present and discuss the QE measurements performed on the CLASP cameras. We also discuss the high-vacuum system outfitted for testing of UV and EUV science cameras at MSFC.

Champey, Patrick↗

VUV Testing of Science Cameras at MSFC: QE Measurement of the CLASP Flight Cameras

The NASA Marshall Space Flight Center (MSFC) has developed a science camera suitable for sub-orbital missions for observations in the UV, EUV and soft X-ray. Six cameras were built and tested for the Chromospheric Lyman-Alpha Spectro-Polarimeter (CLASP), a joint National Astronomical Observatory of Japan (NAOJ) and MSFC sounding rocket mission. The CLASP camera design includes a frame-transfer e2v CCD57-10 512x512 detector, dual channel analog readout electronics and an internally mounted cold block. At the flight operating temperature of -20 C, the CLASP cameras achieved the low-noise performance requirements (less than or equal to 25 e- read noise and greater than or equal to 10 e-/sec/pix dark current), in addition to maintaining a stable gain of approximately equal to 2.0 e-/DN. The e2v CCD57-10 detectors were coated with Lumogen-E to improve quantum efficiency (QE) at the Lyman- wavelength. A vacuum ultra-violet (VUV) monochromator and a NIST calibrated photodiode were employed to measure the QE of each camera. Four flight-like cameras were tested in a high-vacuum chamber, which was configured to operate several tests intended to verify the QE, gain, read noise, dark current and residual non-linearity of the CCD. We present and discuss the QE measurements performed on the CLASP cameras. We also discuss the high-vacuum system outfitted for testing of UV and EUV science cameras at MSFC.

Camera↗

The Realuminizing of the 7-Meter Diameter Solar Simulator Collimating Mirror

This paper describes the modification of a three-electron-beam (EB) gun system for vacuum depositing a highly reflective aluminum coating on a 7.01-m (23-ft) -diam nickel-plated aluminum collimating mirror. The mirror is part of the JPL 7.62-m space simulator that was recently modernized with a new high vacuum pumping system, solar lamp power supplies, solar optic lens system, and refurbished collimating mirror. The mirror is the primary reflector for the solar simulation system and the aluminized reflective surface is its most critical performance element. The uniformity of thickness and high reflectivity of the coating is visible and near-ultraviolet (UV) light governs the accuracy of the beam for solar testing. The uniformity of the thin-film thickness also controls the durability of the mirror over time.

solar↗

Expanding the Measurement Capabilities of the mARC II Arc-Jet to Map the Operating Envelope for High-Enthalpy Air Flows

The mARC II is a 30 kW arc-jet facility at NASA Ames Research Center developed to produce high-enthalpy flows for low-cost technology development purposes. In this work, we introduce new measurement capabilities following the latest facility upgrades and begin characterizing the operating envelope for the two-disk arc-heater configuration with air as the working gas. The lower bound of the envelope corresponds to the lowest set current and the farthest sensor distance from the nozzle (𝐼set = 40 A, 𝑧 = 69 mm), while the upper bound corresponds to the highest current and closest sensor distance (𝐼set = 200 A, 𝑧 = 2 mm). Stagnation point heat flux was measured using a water-cooled Gardon gauge (⌀4.76 mm, 3/16" hemispherical), with values ranging from 15 ≤ q̇₀ ≤ 900 W/cm2. Stagnation pressure was measured using a water-cooled Pitot probe (⌀4.76 mm, 3/16" hemispherical), with values ranging from 18 ≤ p₀ ≤ 1100 Pa. The upgraded vacuum system is demonstrated to significantly extend the lower end of the operating envelope of the mARC II. Additionally, measurements of bulk enthalpy (3 ≤ h ≤ 13 MJ/kg) and stagnation enthalpy (4 ≤ h₀ ≤ 34 MJ/kg) demonstrate the mARC II facility's high-enthalpy capabilities. Completion of the operating envelope characterization is ongoing in tandem with the development of complementary diagnostic capabilities and numerical simulations.

TPS↗

Expanding the Measurement Capabilities of the mARC II Arc-Jet to Map the Operating Envelope for High-Enthalpy Air Flows

The mARC II is a 30 kW arc-jet facility at NASA Ames Research Center developed to produce high-enthalpy flows for low-cost technology development purposes. In this work, we introduce new measurement capabilities following the latest facility upgrades and begin characterizing the operating envelope for the two-disk arc-heater configuration with air as the working gas. The lower bound of the envelope corresponds to the lowest set current and the farthest sensor distance from the nozzle (𝐼set = 40 A, 𝑧 = 69 mm), while the upper bound corresponds to the highest current and closest sensor distance (𝐼set = 200 A, 𝑧 = 2 mm). Stagnation point heat flux was measured using a water-cooled Gardon gauge (⌀4.76 mm, 3/16" hemispherical), with values ranging from 15 ≤ q̇₀ ≤ 900 W/cm 2 . Stagnation pressure was measured using a water-cooled Pitot probe (⌀4.76 mm, 3/16" hemispherical), with values ranging from 18 ≤ p₀ ≤ 1100 Pa. The upgraded vacuum system is demonstrated to significantly extend the lower end of the operating envelope of the mARC II. Additionally, measurements of bulk enthalpy (3 ≤ h ≤ 13 MJ/kg) and stagnation enthalpy (4 ≤ h₀ ≤ 34 MJ/kg) demonstrate the mARC II facility's high-enthalpy capabilities. Completion of the operating envelope characterization is ongoing in tandem with the development of complementary diagnostic capabilities and numerical simulations.

instrumentation↗

Vibration-Isolation Bench for Testing in Vacuum

Precise optical systems tested without contamination. Vibration isolator is one of three such units supporting cast-iron table. Table used to test optical systems in vacuum. Isolator made from commercially available components. Scaled-down version finds wider application in electron optics or electron-beam lithography.

Dankowski, J. C.↗

Thermal Vacuum Facility for Testing Thermal Protection Systems

A thermal vacuum facility for testing launch vehicle thermal protection systems by subjecting them to transient thermal conditions simulating re-entry aerodynamic heating is described. Re-entry heating is simulated by controlling the test specimen surface temperature and the environmental pressure in the chamber. Design requirements for simulating re-entry conditions are briefly described. A description of the thermal vacuum facility, the quartz lamp array and the control system is provided. The facility was evaluated by subjecting an 18 by 36 in. Inconel honeycomb panel to a typical re-entry pressure and surface temperature profile. For most of the test duration, the average difference between the measured and desired pressures was 1.6% of reading with a standard deviation of +/- 7.4%, while the average difference between measured and desired temperatures was 7.6% of reading with a standard deviation of +/- 6.5%. The temperature non-uniformity across the panel was 12% during the initial heating phase (t less than 500 sec.), and less than 2% during the remainder of the test.

Daryabeigi, Kamran↗

Review of Current State of the Art and Key Design Issues With Potential Solutions for Liquid Hydrogen Cryogenic Storage Tank Structures for Aircraft Applications

Due to its high specific energy content, liquid hydrogen (LH2) is emerging as an alternative fuel for future aircraft. As a result, there is a need for hydrogen tank storage systems, for these aircraft applications, that are expected to provide sufficient capacity for flight durations ranging from a few minutes to several days. It is understood that the development of a large, lightweight, reusable cryogenic liquid storage tank is crucial to meet the goals of and supply power to hydrogen-fueled aircraft, especially for long flight durations. This report provides an annotated review (including the results of an extensive literature review) of the current state of the art of cryogenic tank materials, structural designs, and insulation systems along with the identification of key challenges with the intent of developing a lightweight and long-term storage system for LH2. The broad classes of insulation systems reviewed include foams (including advanced aerogels) and multilayer insulation (MLI) systems with vacuum. The MLI systems show promise for long-term applications. Structural configurations evaluated include single- and double-wall constructions, including sandwich construction. Potential wall material candidates are monolithic metals as well as polymer matrix composites and discontinuously reinforced metal matrix composites. For short-duration flight applications, simple tank designs may suffice. Alternatively, for longer duration flight applications, a double-wall construction with a vacuum-based insulation system appears to be the most optimum design. The current trends in liner material development are reviewed in the case that a liner is required to minimize or eliminate the loss of hydrogen fuel through permeation.

Mital, Subodh K.↗

A low cost imaging displacement measurement system for spacecraft thermal vacuum testing

A low cost imaging displacement technique suitable for use in thermal vacuum testing was built and tested during thermal vacuum testing of the space infrared telescope facility (SIRTF, later renamed Spitzer infrared telescope facility). The problem was to measure the relative displacement of different portions of the spacecraft due to thermal expansion or contraction. Standard displacement measuring instrumentation could not be used because of the widely varying temperatures on the spacecraft and for fear of invalidating the thermal vacuum testing. The imaging system was conceived, designed, purchased, and installed in approximately 2 months at very low cost. The system performed beyond expectations proving that sub millimeter displacements could be measured from over 2 meters away. Using commercial optics it was possible to make displacement measurements down to 10 (mu)m. An automated image processing tool was used to process the data, which not only speeded up data reduction, but showed that velocities and accelerations could also be measured. Details of the design and capabilities of the system are discussed along with the results of the test on the observatory. Several images from the actual test are presented.

thermal vacuum↗

Vacuum gage calibration system for 10 to the minus 8th power to 10 torr

Calibration system consists of a gas source, a source pressure gage, source volume, transfer volume and test chamber, plus appropriate piping, valves and vacuum source. It has been modified to cover as broad a range as possible while still providing accuracy and convenience.

Holanda, R.↗

Liquefaction of Cryogenic Fluids for Production and Storage of Commodities on Extra-Terrestrial Surfaces

The Cryogenic Fluid In-situ Liquefaction for Landers (CryoFILL) activity has been investigating concepts for the liquefaction of cryogenic fluids produced on the surface of the Moon and Mars. CryoFILL consists of four activities: liquid nitrogen liquefaction testing that was completed in 2019, liquid oxygen liquefaction testing planned to begin in early 2022, fiber-optic sensor temperature measurement system development, and lightweight vacuum jacketed systems designed for the atmosphere of Mars. Additional activities include the development and validation of numerical modeling systems at three stages: thermodynamic models of the liquefaction process for basic energy/mass estimates, nodal models to predict liquefaction tank system level performance, and computational fluid dynamics to assess fluid phenomena occurring within the tank, specifically condensation and stratification within the ullage. These developments form a combined liquefaction and storage solution to support Lunar and Martian exploration. Key testing results from liquid nitrogen testing as well as plans for liquid oxygen testing will be discussed including key sensitivities from analytical evaluation of completed test results. Progress on the development and improvements on fiber optic sensor testing and developments will also be provided. Finally, work on the progress of the lightweight vacuum jacketed systems being co-developed by NASA and industry will be summarized.

Liquefaction↗

Molecular branching ratio method for intensity calibration of optical systems in the vacuum ultraviolet

A state-of-the-art review is given of the molecular branching ratio method for intensity calibration in the vacuum ultraviolet. Ways are described for determining both relative and quantitative responses in the wavelength range 1000 A to 3000 A. The molecular band systems which are discussed are the following: H2(B 1 Sigma u +)-(X 1 Sigma g +), H2(C 1 Pi u)-(X 1 Sigma g +), N2(A 1 Pi g)-(X 1 Sigma g +), CO(A 1 Pi)-(X 1 Sigma +), NO(A 2 Sigma +)-(X 2 Pi r), and NO(+) (A 1 Pi)-(X 1 Sigma +).

Mumma, M. J.↗

Cross sections and band strengths for the N2O/+/ /A 2Sigma+ to X 2Pi/ system produced by vacuum ultraviolet radiation

Analysis of cross sections that have been obtained for the production of the N2O(+) (A 2Sigma+ to X 2Pi) fluorescence, using vacuum ultraviolet radiation between 462 and 755 A. The fluorescence spectra produced using incident photons of 715.6- and 754.9-A wavelengths are presented, as well as the relative fluorescence cross sections for the individual observed bands of the above-mentioned N2O(+) system. Finally, absolute cross sections for the production of the N2O(+) (A 2Sigma+ to X 2Pi) system are presented, as well as band strengths for the A 2Sigma+(0,0,0) to X 2Pi(n1,n2,0) fluorescence.

Lee, L. C.↗