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NASA NTRS1993

Geomorphic evolution of the Martian highlands through ancient fluvial processes

The evolution of crater degradation in the Martian highlands based on variations in crater morphology is traced. The timing of this process related to geology, elevation, and latitude is examined, the nature of fluvial resurfacing is studied, and the approximate rate of denudation is determined. The obtained data make it possible to understand the early geologic history of Mars, the interaction between the atmosphere and surface processes through time, and the nature of highland surface materials. Degradation was found to begin with sheet-flooding and the formation of runoff channels in both the interior and exterior of the craters. Progressive stripping of the ejecta material led to craters with incised rims. Erosion and infilling led to flat doors. With time, continued erosion removed ejecta and rim materials completely. Timing of degradation based on cumulative size-frequency distribution curves of highland crater population indicates that the process ceased completely in the late Hesperian. Global average denudation rates were found to be between 0.0001 and 0.005 mm/yr.

Craddock, Robert A.↗

DOE OSTI2025

Predicting long-term stress relaxation on Alloy 709 using the crystal plasticity finite element method

This report summarizes the results of physics-based, crystal plasticity simulations for the long-term stress relaxation behavior of Alloy 709. The purpose of the study was to provide insight into five key questions related to long-term behavior in high temperatures materials which are difficult or impossible to answer experimentally: (1) is there a threshold stress for long-term relaxation? (2) is there strain threshold for relaxation damage, below which significant damage does not accumulate? (3) does damage continue to accumulate as the material relaxes or will damage accumulation plateau under some loading conditions? (4) does stress relaxation loading inevitably lead to failure? and (5) which, if any, engineering models for relaxation damage accumulation reasonably match the simulation results? The report summarizes the numerical simulations used to address these five questions and provides at least partial answers to each question.

36 MATERIALS SCIENCE↗

NASA NTRS2000

Minerologic and Petrologic Studies of Meteorites and Lunar Samples

In the past year this group continued essentially full time research on extraterrestrial materials, and the question of the origin of the solar system. The continuing scientific staff consists of the P.I. and Visiting Scientist Michael Petaev. Vitae for Wood and Petaev appear in Sec. 6. We benefit from the part time services of a Project Administrator (Judith Terry) and a Secretary (Muazzez Lohmiller). In January 1999 the P.I. assumed the Chairmanship of COMPLEX, the Committee on Planetary and Lunar Exploration of the Space Studies Board, National Research Council. Wood and Petaev were authors or coauthors of 21 publications, new manuscripts, and abstracts in the last year. These are listed above, and referenced by number [n] in the discussion below. Other references to the literature made in this Section are listed in Sec. 3.

Wood, John↗

NASA NTRS2010

Sample Return: What Happens to the Samples on Earth?

As space agencies throughout the world turn their attention toward human exploration of the Moon, Mars, and the solar system beyond, there has been an increase in the number of robotic sample return missions proposed as precursors to these human endeavors. In reality, however, we, as a global community, have very little experience with robotic sample return missions: 3 of the Russian Luna Missions successfully returned lunar material in the 1970s; 28 years later, in 2004, NASA s Genesis Mission returned material from the solar wind; and in 2006, NASA s Stardust Mission returned material from the Comet Wild2. [Note: The Japanese Hyabusa mission continues in space with the hope of returning material from the asteroid 25143 Itokawa.] We launch many spacecraft to LEO and return them to Earth. We also launch spacecraft beyond LEO to explore the planets, our solar system, and beyond. Some even land on these bodies. But these do not return. So as we begin to contemplate the sample return missions of the future, some common questions arise: "What really happens when the capsule returns?" "Where does it land?" "Who retrieves it and just how do they do that?" "Where does it go after that?" "How do the scientists get the samples?" "Do they keep them?" "Who is in charge?" The questions are nearly endless. The goal of this paper/presentation is to uncover many of the mysteries of the post-return phase of a mission - from the time the return body enters the atmosphere until the mission ends and the samples become part of a long term collection. The discussion will be based largely on the author s own experience with both the Genesis and Stardust missions. Of course, these two missions have a great deal in common, being funded by the same NASA Program (Discovery) and having similar team composition. The intent, however, is to use these missions as examples in order to highlight the general requirements and the challenges in defining and meeting those requirements for the final phase of sample return missions. The choices made by the Genesis and Stardust teams regarding recovery and sample handling will be discussed. These will be compared with the handling of returned lunar samples and the proposed handling of the Hyabusa samples as well. Finally, though none of these recent missions have been restricted within NASA s Planetary Protection Protocol, this is likely to change as missions venture farther from Earth. The implementation of Planetary Protection requirements will vary significantly based on mission scenario, however some of the potential implications of restricted Earth return will be considered.

McNamara, Karen↗

DOE OSTI2024

Charge-lattice coupling and the dynamic structure of the U–O distribution in UO 2+x

The different structures and behaviors of UO 2+x observed in crystallographic and local structure measurements were examined by extended X-ray absorption fine structure (EXAFS) measurements of pristine UO 2.0 , p + and He 2+ irradiated UO 2.0 , and, at multiple temperatures, bulk U 4 O 9 and U 3 O 7 and thin film U 4 O 9-δ on an epitaxial substrate. The disorder caused by irradiation is mostly limited to increased widths of the existing U–O/U pair distributions, with any new neighbor shells being minor. As has been previously reported, the disorder caused by oxidative addition to U 4 O 9 and U 3 O 7 is much more extensive, resulting in multisite U–O distributions and greater reduction of the U–U amplitude with different distributions in bulk and thin-film U 4 O 9 . This includes the significant spectral feature near R = 1.2 Å for all U 4 O 9 and U 3 O 7 samples fit with a U-oxo type moiety with a U–O distance around 1.7 Å. In addition to indicating that these anomalies only occur in mixed valence materials, this work confirms the continuous rearrangement of the U–O distributions from 10 to 250 K. Although these variations of the structure are not observed in crystallography, their prominence in the EXAFS indicates that the dynamic structure underlying these effects is an essential factor of these materials.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS2004

Fighting Corrosion

Reinforced concrete structures such as bridges, parking decks, and balconies are designed to have a service life of over 50 years. All too often, however, many structures fall short of this goal, requiring expensive repairs and protection work earlier than anticipated. The corrosion of reinforced steel within the concrete infrastructure is a major cause for this premature deterioration. Such corrosion is a particularly dangerous problem for the facilities at NASA s Kennedy Space Center. Located near the Atlantic Ocean in Florida, Kennedy is based in one of the most corrosive-prone areas in the world. In order to protect its launch support structures, highways, pipelines, and other steel-reinforced concrete structures, Kennedy engineers developed the Galvanic Liquid Applied Coating System. The system utilizes an inorganic coating material that slows or stops the corrosion of reinforced steel members inside concrete structures. Early tests determined that the coating meets the criteria of the National Association of Corrosion Engineers for complete protection of steel rebar embedded in concrete. Testing is being continued at the Kennedy's Materials Science Beach Corrosion Test Site.

Source record↗

NASA NTRS1988

Search for the Tunguska event in the Antarctic snow

The Tunguska explosion in 1908 is supposed to have been produced by the impact of a small celestial body. The absence of any identifiable crater together with the huge energy released by the event suggest that the impactor exploded in midair and that its material was widely spread over the Earth. The short term contribution of such exceptional events to the total accretion rate of extraterrestrial material by the Earth could be significant. Samples were chosen in a core electromechanically drilled in 1984 near South Pole Station. There, the low temperatures, preventing melting all year long, and the nearly regular snow fall rate provide good conditions for a reliable continuous record of any infalling material. In many samples Ir was below the detection limit of the instrumentation. The iridium infall averaged over 45 samples is given. In a few samples the iridium content is significantly higher than the average: the frequency and amplitude of such fluctuations can be explained by the presence on some filters of finite size cosmic particles. No significant systematic increase above the average level is observed in the part of the core corresponding to the Tunguska event. The two major results of this study are: (1) The presence of Tunguska explosion debris in the Antarctic snow is not confirmed; and (2) The estimate of the average iridium infall, is an order of magnitude lower than the Ganapathy's background but is close to the values measured in Antarctic snow and atmospheric samples by Takahashi et al. The results are also consistent with the flux of micrometeoroids deduced from optical and radar observations or derived from the study of Greenland cosmic dust collection but are lower than the flux at mid-latitude measured in paleocene-oligocene sediments from the central part of the Pacific Ocean.

Rocchia, R.↗

NASA NTRS1992

Selected results for LDEF thermal control coatings

The investigation of space environmental effects on LDEF thermal control coatings by the Materials Special Investigation Group is continuing. Analyses of chromic acid anodize, A276 white paint, and Z306 black paint were conducted, assessing performance as functions of environmental exposure. Test results from additional coatings, such as on scuff plates, M003, and the black chromium plate solar absorber, were obtained. Guidelines for the use of these materials and comparisons to ground based test data will be presented.

Golden, Johnny L.↗

NASA NTRS2002

Microgravity: Molecular Dynamics Simulations at the NCCS Probe the Behavior of Liquids in Low Gravity

The life of the very small, whether in something as complicated as a human cell or as simple as a drop of water, is of fundamental scientific interest: By knowing how a tiny amount of material reacts to changes in its environment, scientists maybe able to answer questions about how a bulk of material would react to comparable changes. NASA is in the forefront of computational research into a broad range of basic scientific questions about fluid dynamics and the nature of liquid boundary instability. For example, one important issue for the space program is how drops of water and other materials will behave in the low-gravity environment of space and how the low gravity will affect the transport and containment of these materials. Accurate prediction of this behavior is among the aims of a set of molecular dynamics experiments carried out on the NCCSs Cray supercomputers. In conventional computational studies of materials, matter is treated as continuous - a macroscopic whole without regard to its molecular parts - and the behavior patterns of the matter in various physical environments are studied using well-established differential equations and mathematical parameters based on physical properties such as compressibility density, heat capacity, and vapor pressure of the bulk material.

Source record↗

NASA NTRS2007

One-Dimensional Ablation with Pyrolysis Gas Flow Using a Full Newton's Method and Finite Control Volume Procedure

The development and verification of a one-dimensional material thermal response code with ablation is presented. The implicit time integrator, control volume finite element spatial discretization, and Newton's method for nonlinear iteration on the entire system of residual equations have been implemented and verified for the thermochemical ablation of internally decomposing materials. This study is a continuation of the work presented in "One-Dimensional Ablation with Pyrolysis Gas Flow Using a Full Newton's Method and Finite Control Volume Procedure" (AIAA-2006-2910), which described the derivation, implementation, and verification of the constant density solid energy equation terms and boundary conditions. The present study extends the model to decomposing materials including decomposition kinetics, pyrolysis gas flow through the porous char layer, and a mixture (solid and gas) energy equation. Verification results are presented for the thermochemical ablation of a carbon-phenolic ablator which involves the solution of the entire system of governing equations.

Amar, Adam J.↗

NASA NTRS2026

Artemis Suit Material Effects of Calendaring Woven Fabrics on Dust Resistance

This paper presents one element of an ongoing NASA technology-infusion effort to design, fabricate, and test a new outer shell fabric for a lunar Extravehicular Activity (EVA) space suit, a critical component of sustained lunar exploration. A primary challenge for suit textiles is preventing lunar dust, which is highly abrasive, electrostatically charged, and capable of infiltrating even tightly woven fabrics from penetrating the Environment Protection Garment (EPG) and compromising suit durability and astronaut safety. To enhance dust-blocking performance, the Artemis Suit Materials Team investigated calendaring, a continuous roll to roll mechanical finishing process in which fabric passes through heated rollers under high pressure to compress and flatten the weave, thereby reducing pore size and modifying surface texture without significantly affecting other properties. Targeted testing of calendared Teflon™ T-162 and Ortho Fabric samples provides new insight into how calendaring influences dust resistance, informing future material development and advancing EVA suit technology for long-duration lunar missions.

Dust↗

NASA NTRS2026

Artemis Suit Material Effects of Calendaring Woven Fabrics on Dust Resistance

Dust↗

DOE OSTI2024

Measuring the Moisture Content of Wood Sheathing with Continuous Wave Radars

Radars were studied for measuring the moisture content of wood-based materials because of their non-destructive nature and their ability to measure the moisture content of several layers at once. These convenient characteristics enable a quick and non-invasive method to find areas of high moisture content in building envelopes so that problems can be fixed before the structure degrades. The need to operate the radar at millimeter ranges required the development of new techniques and methods for analyzing and calculating the moisture content of individual layers of building material. The techniques are providing accurate results for oriented strand board, and efforts are continuing for investigating other construction materials, meeting FCC requirements, and building a system that will be easy to deploy.

Killough, Stephen M↗

NASA NTRS2000

Solid Freeform Fabrication of Continuous Fiber Reinforced Composites for Propulsion Applications

For propulsion related applications, materials must be able to demonstrate excellent ablation and oxidation resistance at temperature approaching 3500'C, adequate load bearing capabilities, non-catastrophic failure modes, and ability to withstand transient thermal shock. A potential list of propulsion-material property requirements includes, low density, high elastic modulus, low thermal-expansion coefficient, high thermal conductivity, excellent erosion and oxidation/corrosion resistance, and flaw-insensitivity. In many cases, they will also need to be able to be joined, survive thermal cycling and multi-axial stress states, and for reusable applications, the materials must maintain the above attributes after prolonged exposure to extremely harsh chemical environments. The final and possibly most important attribute for these materials are the need to be lower cost and readily available in large quantities. Recently, Advanced Ceramics Research, Inc. (ACR) has developed low cost, flexible- manufacturing processes for Zr & Hf-based carbon fiber reinforced composites, materials with good oxidation and ablation resistance up to 3500 C. This process, called Continuous Composite Co-extrusion (C(sup 3)), incorporates carbon fibers to fabricate 'in-situ' carbide and boride-matrix/carbon fiber composites. This is a variation of ACR's manufacturing process for low-cost structural ceramic materials called Fibrous Monoliths With carbon fiber reinforcements. Fibrous Monolithic materials have a distinct fibrous texture, consist of intertwined cells of a primary phase, separated by cell boundaries of a tailored secondary phase and show very high fracture energies, damage tolerance, and graceful failure. Since they are monolithic powder based composites-, they can be manufactured by conventional powder processing techniques using inexpensive raw materials. This combination of high performance and low cost is a breakthrough that could enable wider application of ceramics in high temperature applications. Typical volume fractions of the two phases are 80 to 95% for the cell phase and 5 to 20% for the interpenetrating cell boundary phase. ACR is currently developing an innovative solid freeform form fabrication (SFF) approach to produce Hf and Zr based ceramic composite components reinforced with continuous carbon fiber tows for critical structural components such as tubes and blisks. The process is simple, robust and will be widely applicable to a number of material systems. This technique was originally developed at the University of Delaware Center for Composite Materials (UD-CCM) for rapid fabrication of polymer matrix composites by a technique called automated tow placement or ATP. The current process is being developed in collaboration with UD-CCM. The paper will detail the freeform fabrication process to create low-cost ceramic fiber reinforced composites for high-temperature applications. The results of mechanical properties and microstructural characterization will be presented, together with examples of complex shapes and parts. It is believed that the process will be able to create complex shaped parts for propulsion applications at an order of magnitude lower cost than current CVI and PIP process.

Vaidyanathan, R.↗

NASA NTRS2001

Solid Free-Form Fabrication of Continuous Fiber Reinforced Composites for Propulsion Application

For propulsion related applications, materials must be able to demonstrate excellent ablation and oxidation resistance at temperature approaching 3500 C, adequate load bearing capabilities, non-catastrophic failure modes, and ability to withstand transient thermal shock. A potential list of propulsion-material property requirements includes, low density, high elastic modulus, low thermal-expansion coefficient, high thermal conductivity, excellent erosion and oxidation/corrosion resistance, and flaw-insensitivity. In many cases, they will also need to be able to be joined, survive thermal cycling and multi-axial stress states, and for reusable applications, the materials must maintain the above attributes after prolonged exposure to extremely harsh chemical environments. The final and possibly most important attribute for these materials are the need to be lower cost and readily available in large quantities. Recently, Advanced Ceramics Research, Inc. (ACR) has developed low cost, flexible-manufacturing processes for Zr & Hf-based carbon fiber reinforced composites, materials with good oxidation and ablation resistance up to 3500 C. This process, called Continuous Composite Co-extrusion (C(sup 3)), incorporates carbon fibers to fabricate 'in-situ' carbide and boride-matrix/carbon fiber composites. M is a variation of ACR's manufacturing process for low-cost structural ceramic materials called Fibrous Monoliths with carbon fiber reinforcements. Fibrous Monolithic materials have a distinct fibrous texture, consist of intertwined cells of a primary phase, separated by cell boundaries of a tailored secondary phase and show very high fracture energies, damage tolerance, and graceful failure. Since they are monolithic powder based composites; they can be manufactured by conventional powder processing techniques using inexpensive raw materials. This combination of high performance and low cost is a breakthrough that could enable wider application of ceramics in high temperature applications. Typical volume fractions of the two phases are 80 to 95% for the cell phase and 5 to 20% for the interpenetrating cell boundary phase. ACR is currently developing an innovative solid freeform form fabrication (SFF) approach to produce Hf and Zr based ceramic composite components reinforced with continuous carbon fiber tows for critical structural components such as tubes and blisks. The process is simple, robust and will be widely applicable to a number of material systems. This technique was originally developed at the University of Delaware Center for Composite Materials (UD-CCM) for rapid fabrication of polymer matrix composites by a technique called automated tow placement or ATP. The current process is being developed in collaboration with UD-CCM. The paper will detail the freeform fabrication process to create low-cost ceramic fiber reinforced composites for high-temperature applications. The results of mechanical properties and microstructural characterization will be presented, together with examples of complex shapes and parts. It is believed that the process will be able to create complex shaped parts for propulsion applications at an order of magnitude lower cost than current CVI and PIP processes.

Vaidyanathan, R.↗

DOE OSTI2024

Nuclear Structural Component Relevant Properties of Nickel-Based Alloys Produced via Additive Manufacturing

Idaho National Laboratory initiated examination of nickel-based alloys manufactured via three different additive manufacturing methods for potential applications in nuclear, high temperature structural components. The three methods analyzed included laser powder bed fusion, blown powder laser directed energy deposition, and wire-fed gas metal arc directed energy deposition. With the rapid push towards additive manufacturing, codes do not exist that definitively define what is or is not tolerable for each process and application, such as with conventional, wrought products. This report contains the initial work to understand possible manufacturing methods for high temperature alloys, and specifically, void formation, microstructure evolution, corrosion, and mechanical properties. To generate mechanical test data, specimens were tested irrespective of voids and microstructures were analyzed to better understand how to negate/improve these issues. The preliminary results showed major decreases in mechanical performance for material tested. Test specimens will continue to be produced to further improve each additive manufacturing processes, quantify void acceptance, and better understand the most suitable high temperature alloys receptive to additive manufacturing and high temperature nuclear applications.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Characterizing Electrode Materials and Interfaces in Solid-State Batteries

Solid-state batteries (SSBs) could offer improved energy density and safety, but the evolution and degradation of electrode materials and interfaces within SSBs are distinct from conventional batteries with liquid electrolytes and represent a barrier to performance improvement. Over the past decade, a variety of imaging, scattering, and spectroscopic characterization methods has been developed or used for characterizing the unique aspects of materials in SSBs. These characterization efforts have yielded new understanding of the behavior of lithium metal anodes, alloy anodes, composite cathodes, and the interfaces of these various electrode materials with solid-state electrolytes (SSEs). This review provides a comprehensive overview of the characterization methods and strategies applied to SSBs, and it presents the mechanistic understanding of SSB materials and interfaces that has been derived from these methods. This knowledge has been critical for advancing SSB technology and will continue to guide the engineering of materials and interfaces toward practical performance.

25 ENERGY STORAGE↗

NASA NTRSDate not supplied

Carbonate Mineralogy of the C1 Clasts in Kaidun Meteorite

The Kaidun meteorite is a polymict microbreccia weighing approximately 850 g that fell in the People's Republic of South Yemen on December 3, 1980. Although the host material is CR chondrite, it is unique in that it contains many clasts of various chondritic and achondritic materials. Chondritic clasts include EH3-5, EL3, C1, C2, CM1, CM2, CV3, and ordinary chondrite-related materials. Achondrites include a high-Ca primitive achondrite, fragments of alkali-rich differentiated materials, and an aubrite-like clasts [1]. In this study, we focused on C1 materials. There is plenty of evidence that aqueous alteration in the carbonaceous chondrite clasts in Kaidun occurred primarily on their parent bodies before accumulation to a Kaidun body/ Therefore, observations of the C1 materials, which are highly aqueously altered, can provide quantitative constraints on the geologic history of their asteroid parent bodies. In addition, although the lack of petrological features can make the classification of C1 material more difficult, recent studies and analysis of new meteorite fall and returned samples continue to emphasize the diversity of C1 materials.

K Ogiya↗