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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 325 records · Page 18
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Towards automating structural discovery in scanning transmission electron microscopy *

Abstract Scanning transmission electron microscopy is now the primary tool for exploring functional materials on the atomic level. Often, features of interest are highly localized in specific regions in the material, such as ferroelectric domain walls, extended defects, or second phase inclusions. Selecting regions to image for structural and chemical discovery via atomically resolved imaging has traditionally proceeded via human operators making semi-informed judgements on sampling locations and parameters. Recent efforts at automation for structural and physical discovery have pointed towards the use of ‘active learning’ methods that utilize Bayesian optimization with surrogate models to quickly find relevant regions of interest. Yet despite the potential importance of this direction, there is a general lack of certainty in selecting relevant control algorithms and how to balance a priori knowledge of the material system with knowledge derived during experimentation. Here we address this gap by developing the automated experiment workflows with several combinations to both illustrate the effects of these choices and demonstrate the tradeoffs associated with each in terms of accuracy, robustness, and susceptibility to hyperparameters for structural discovery. We discuss possible methods to build descriptors using the raw image data and deep learning based semantic segmentation, as well as the implementation of variational autoencoder based representation. Furthermore, each workflow is applied to a range of feature sizes including NiO pillars within a La:SrMnO 3 matrix, ferroelectric domains in BiFeO 3 , and topological defects in graphene. The code developed in this manuscript is open sourced and will be released at github.com/nccreang/AE_Workflows .

47 OTHER INSTRUMENTATION↗
DOE OSTI2025

Controlling Oxidation of Nb in Oxygen Abundant Environments

Modern particle accelerators depend on Superconducting Radio Frequency (SRF) cavities made from high-purity niobium (Nb) to achieve optimal performance, including high quality factors and strong accelerating gradients. However, when exposed to air, niobium naturally forms a complex oxide layer that can introduce surface imperfections and carbon contamination. This work examines an alternative oxidation strategy under oxygen-rich conditions to better regulate the oxide formation process. The ultimate objective is to improve surface uniformity and cleanliness, thereby reducing defect density and enhancing performance. We used Confocal Microscopy, Scanning Electron Microscopy (SEM), and X-Ray Photoelectron Spectroscopy (XPS) to analyze surface changes. We used standard metrics, like Arithmetic Average Roughness (Ra) and Root Mean Square (Rq). Three oxidation methods were applied: short, extended, and a repeated HF and H₂O₂ oxidation process. Preliminary results show promising reductions in carbon contamination and surface defects.

Romero, Juan [Fermilab]↗
DOE OSTI2021

Dissecting the Quadruple Binary Hyad vA 351 Masses for Three M Dwarfs and a White Dwarf

We extend results first announced by Franz et al., that identified vA 351 = H346 in the Hyades as a multiple star system containing a white dwarf. With Hubble Space Telescope Fine Guidance Sensor fringe tracking and scanning, and more recent speckle observations, all spanning 20.7 years, we establish a parallax, relative orbit, and mass fraction for two components, with a period, P=2.70 yr and total mass 2.1 M{sub ⊙}. With ground-based radial velocities from the McDonald Observatory Otto Struve 2.1 m Telescope Sandiford Spectrograph, and Center for Astrophysics Digital Speedometers, spanning 37 years, we find that component B consists of BC, two M dwarf stars orbiting with a very short period (P{sub BC}=0.749 days), having a mass ratio M{sub C}/M{sub B} = 0.95. We confirm that the total mass of the system can only be reconciled with the distance and component photometry by including a fainter, higher-mass component. The quadruple system consists of three M dwarfs (A, B, C) and one white dwarf (D). We determine individual M dwarf masses M{sub A} = 0.53 ± 0.10 M{sub ⊙}, M{sub B} = 0.43 ± 0.04 M{sub ⊙}, and M{sub C} = 0.41 ± 0.04 M{sub ⊙}. The white dwarf mass, 0.54 ± 0.04 M{sub ⊙}, comes from cooling models, an assumed Hyades age of 670 Myr, and consistency with all previous and derived astrometric, photometric, and radial velocity results. Velocities from Hα and He i emission lines confirm the BC period derived from absorption lines, with similar (He i) and higher (Hα) velocity amplitudes. We ascribe the larger Hα amplitude to emission from a region each component shadows from the other, depending on the line of sight.

47 OTHER INSTRUMENTATION↗
NASA NTRS1980

The Infrared Astronomical Satellite /IRAS/ Scientific Data Analysis System /SDAS/ sky flux subsystem

The sky flux subsystem of the Infrared Astronomical Satellite Scientific Data Analysis System is described. Its major output capabilities are (1) the all-sky lune maps (8-arcminute pixel size), (2) galactic plane maps (2-arcminute pixel size) and (3) regional maps of small areas such as extended sources greater than 1-degree in extent. The major processing functions are to (1) merge the CRDD and pointing data, (2) phase the detector streams, (3) compress the detector streams in the in-scan and cross-scan directions, and (4) extract data. Functional diagrams of the various capabilities of the subsystem are given. Although this device is inherently nonimaging, various calibrated and geometrically controlled imaging products are created, suitable for quantitative and qualitative scientific interpretation.

Stagner, J. R.↗
NASA NTRS1992

Infrared observations and thermal models of the Beta Pictoris disk

Measurements of the flux from the central portion of the Beta Pic disk performed via photometry at 3.5-20 microns in 4- and 8-arcsec apertures are presented. The 10.1- and 20-micron measurements show an excess which is extended, with significant flux located in the annulus between 4- and 8-arcsec diameter centered on the star. Disk models are calculated to reproduce the ground-based IR data, IRAS fluxes, IRAS 60-micron scan profile widths, and optical scattered light distribution. The color temperature and angular scale of the disk are found to be inconsistent with emission from large ('blackbody') particles: most of the thermal emission originates from particles which are inefficient radiators, with sizes near 1 micron. A simple disk with a single power-law spatial distribution is inconsistent with the combined optical and IR data. The inner disk component represents a gross deficit of material relative to an inward extrapolation of the outer component.

Backman, D. E.↗
NASA NTRS1996

Clouds and the Earth's Radiant Energy System (CERES): An Earth Observing System Experiment

Clouds and the Earth's Radiant Energy System (CERES) is an investigation to examine the role of cloud/radiation feedback in the Earth's climate system. The CERES broadband scanning radiometers are an improved version of the Earth Radiation Budget Experiment (ERBE) radiometers. The CERES instruments will fly on several National Aeronautics and Space Administration Earth Observing System (EOS) satellites starting in 1998 and extending over at least 15 years. The CERES science investigations will provide data to extend the ERBE climate record of top-of-atmosphere shortwave (SW) and longwave (LW) radiative fluxes CERES will also combine simultaneous cloud property data derived using EOS narrowband imagers to provide a consistent set of cloud/radiation data, including SW and LW radiative fluxes at the surface and at several selected levels within the atmosphere. CERES data are expected to provide top-of-atmosphere radiative fluxes with a factor of 2 to 3 less error than the ERBE data Estimates of radiative fluxes at the surface and especially within the atmosphere will be a much greater challenge but should also show significant improvements over current capabilities.

Wielicki, Bruce A.↗
NASA NTRS2007

Hierarchical Segmentation Enhances Diagnostic Imaging

Bartron Medical Imaging LLC (BMI), of New Haven, Connecticut, gained a nonexclusive license from Goddard Space Flight Center to use the RHSEG software in medical imaging. To manage image data, BMI then licensed two pattern-matching software programs from NASA's Jet Propulsion Laboratory that were used in image analysis and three data-mining and edge-detection programs from Kennedy Space Center. More recently, BMI made NASA history by being the first company to partner with the Space Agency through a Cooperative Research and Development Agreement to develop a 3-D version of RHSEG. With U.S. Food and Drug Administration clearance, BMI will sell its Med-Seg imaging system with the 2-D version of the RHSEG software to analyze medical imagery from CAT and PET scans, MRI, ultrasound, digitized X-rays, digitized mammographies, dental X-rays, soft tissue analyses, moving object analyses, and soft-tissue slides such as Pap smears for the diagnoses and management of diseases. Extending the software's capabilities to three dimensions will eventually enable production of pixel-level views of a tumor or lesion, early identification of plaque build-up in arteries, and identification of density levels of microcalcification in mammographies.

Source record↗
DOE OSTI2025

Nanoscale Phase Identification Using Two-Dimensional Pair Correlation Functions: A Case Study on Hafnium Oxide

Accurate identification of local phases in nanocrystalline materials is essential for understanding their functional properties, but it remains a significant challenge for polymorphic materials to locally differentiate them at nanoscale. This challenge is further compounded in polycrystalline materials with randomly oriented grains and the coexistence of multiple phases. In this report, we present a methodology for phase and orientation identification at the nanoscale by leveraging vector pair correlation functions extracted from atomically resolved scanning transmission electron microscopy (STEM) images. We demonstrate the accuracy of the methodology on both simulated and experimental data from HfO 2 -based films, a material that exhibits multiple coexisting phases in films with thicknesses ranging from 5 to 20 nm. While demonstrated on HfO 2 films, the methodology can be extended to other polymorphic nanocrystalline systems with complex phase coexistence.

36 MATERIALS SCIENCE↗
NASA NTRS1976

A photon counting array photometer using an intensified charge coupled device

An array photometer which uses an intensified charge coupled device was developed. This system, the University of Maryland Array Photometer (UMAP), has the ability to discriminate single photoelectron events in real time at a 4 Megahertz rate. The photosensor uses an S-20 photocathode and a Fairchild CCD202 with a 100 by 100 array of separate individual channels. The overall system has demonstrated a noise level which permits single photoelectron discrimination, a scan rate of 400 frames per second, a very linear response, and very low lag. The UMAP system has a very large dynamic range exceeding 10,000 in the photon counting mode. A special technique to extend the dynamic range to 1,000,000 was described. The performance parameters of this system, both in the laboratory and on the telescope were cited. Data from these observations were discussed to illustrate the system sensitivity, which is basically limited by the pixel size in the array, rather than the electrooptics.

Currie, D. G.↗
NASA NTRS2001

Large Scale Diffuse X-ray Emission from Abell 3571

Observations of the Luman alpha forest suggest that there are many more baryons at high redshift than we can find in the Universe nearby. The largest known concentration of baryons in the nearby Universe is the Shapley supercluster. We scanned the Shapley supercluster to search for large scale diffuse emission with the Rossi X-ray Timing Explorer (RXTE), and found some evidence for such emission. Large scale diffuse emission may be associated to the supercluster, or the clusters of galaxies within the supercluster. In this paper we present results of scans near Abell 3571. We found that the sum of a cooling flow and an isothermal beta model adequately describes the X-ray emission from the cluster. Our results suggest that diffuse emission from A3571 extends out to about two virial radii. We briefly discuss the importance of the determination of the cut off radius of the beta model.

Molnar, Sandor M.↗
NASA NTRS2016

Estimating Terra MODIS Polarization Effect Using Ocean Data

Terra MODIS has been known since pre-launch to have polarization sensitivity, particularly in shortest-wavelength bands 8 and 9. On-orbit reflectance trending of pseudo-invariant sites show a variation in reflectance as a function of band and scan mirror angle of incidence consistent with time-dependent polarization effects from the rotating double-sided scan mirror. The MODIS Characterization Support Team [MCST] estimates the Mueller matrix trending from this variation as observed from a single desert site, but this effect is not included in Collection 6 [C6] calibration. Here we extend the MCSTs current polarization sensitivity monitoring to two ocean sites distributed over latitude to helpestimate the uncertainties in the derived Mueller matrix. The Mueller matrix elements derived for polarization-sensitive Band 8 for a given site are found to be fairly insensitive to surface brdf modeling. The site-to-site variation is a measure of the uncertainty in the Mueller estimation.Results for band 8 show that the polarization correction reduces mirror-side striping by up to 50% and reduces the instrument polarization effect on reflectance time series of an ocean target.

Wald, Andrew E.↗
NASA NTRS1980

Saturn's E ring revisited

Images of the E ring of Saturn obtained by the image processing of photographs of the 1966 edge-on presentation of the planet's ring plane are presented. Two methods of image enhancement were used: scanning with an image quantizer operated in the derivative mode to enhance contrast and computerized subtraction of a circularly symmetric image of the overexposed Saturn disk. Further photographic and CCD observation confirming the existence of the ring extending to twice the diameter of the A ring, which was not detected by the Pioneer 11 imaging photopolarimeter, is indicated.

Feibelman, W. A.↗
NASA NTRS1992

The chromosphere of VV cephei and the distribution of circumstellar dust around red giants and supergiants

The work on this project has followed two separate paths of inquiry. The first project was entitled 'the Chromosphere of VV Cephei.' The examination of the archival spectra revealed significant changes in the spectra. Therefore, we obtained additional observing time with IUE to monitor the system during the summer of 1991. Short-term changes continue to be seen in both the overall spectrum and individual line profiles. Work continues on this object. The second project was entitled 'the Distribution of Circumstellar Dust around Red Giants and Supergiants.' A number of cool evolved stars are surrounded by dust shells of sufficient angular size as to appear extended in the IRAS survey data. The aim of this project has been to convolve the predictions of the flux distribution from model dust shells with the IRAS beam profiles in order to reproduce the observed IRAS scans. At the time of the last status report, the cross-scan profiles of the IRAS detectors had just been added to the modeling procedure. For scans in which the star passed near the detector center, there was no significant variation in predicted scan profile for different detectors. Scans in which the detector did not pass over the bright central star had been anticipated to be particularly useful in determining the dust distribution; however, significant differences in the predicted scan profiles were seen for different detector profiles. For this reason, and due to the cross-talk effects discussed in the previous status report, further work on the scans not including a central star has been postponed in favor of further analysis of scans passing over the central star.

Bauer, Wendy Hagen↗
NASA NTRS1996

Electronic and Interfacial Properties of PD/6H-SiC Schottky Diode Gas Sensors

Pd/SiC Schottky diodes detect hydrogen and hydrocarbons with high sensitivity. Variation of the diode temperature from 100 C to 200 C shows that the diode sensitivity to propylene is temperature dependent. Long-term heat treating at 425 C up to 140 hours is carried out to determine the effect of extended heat treating on the diode properties and gas sensitivity. The heat treating significantly affects the diode's capacitive characteristics, but the diode's current carrying characteristics are much more stable with a large response to hydrogen. Scanning Electron Microscopy and X-ray Spectrometry studies of the Pd surface after the heating show cluster formation and background regions with grain structure observed in both regions. The Pd and Si concentrations vary between grains. Auger Electron Spectroscopy depth profiles revealed that the heat treating promoted interdiffusion and reaction between the Pd and SiC dw broadened the interface region. This work shows that Pd/SiC Schottky diodes have significant potential as high temperature gas sensors, but stabilization of the structure is necessary to insure their repeatability in long-term, high temperature applications.

Chen, Liang-Yu↗
NASA NTRS2016

Pluto's Global Surface Composition Through Pixel-by-Pixel Hapke Modeling of New Horizons Ralph LEISA Data

On July 14th 2015, NASA's New Horizons mission gave us an unprecedented detailed view of the Pluto system. The complex compositional diversity of Pluto's encounter hemisphere was revealed by the Ralph/LEISA infrared spectrometer on board of New Horizons. We present compositional maps of Pluto defining the spatial distribution of the abundance and textural properties of the volatiles methane and nitrogen ices and non-volatiles water ice and tholin. These results are obtained by applying a pixel-by-pixel Hapke radiative transfer model to the LEISA scans. Our analysis focuses mainly on the large scale latitudinal variations of methane and nitrogen ices and aims at setting observational constraints to volatile transport models. Specifically, we find three latitudinal bands: the first, enriched in methane, extends from the pole to 55degN, the second dominated by nitrogen, continues south to 35 degN, and the third, com- posed again mainly of methane, reaches 20 degN. We demonstrate that the distribution of volatiles across these surface units can be explained by differences in insolation over the past few decades. The latitudinal pattern is broken by Sputnik Planitia, a large reservoir of volatiles, with nitrogen playing the most important role. The physical properties of methane and nitrogen in this region are suggestive of the presence of a cold trap or possible volatile stratification. Furthermore our modeling results point to a possible sublimation transport of nitrogen from the northwest edge of Sputnik Planitia toward the south.

Protopapa, S.↗
NASA NTRSDate not supplied

Statistical Descriptors of Composite Fiber Aggregation

This study introduces a method of characterizing fiber aggregation and resin rich regions in composite microstructures. Microscale models of representative elements (RVE) need to be indicative of the extend of clustering (i.e. close fiber-to-fiber interaction) and resin rich “pools” which may impact the overall strength and performance of a composite structure. This algorithm was used to evaluate different unidirectional 2-D microstructure scans, which will be compared to their manufacturing method or any special treatment processes. These cluster and pool scan statistics can be used as criteria to judge statistical equivalency of artificially constructed microstructures.

Statistics↗
NASA NTRS2007

Fluence Uniformity Measurements in an Electron Accelerator Used for Irradiation of Extended Area Solar Cells and Electronic Circuits for Space Applications

It is common to have liquid crystal displays and electronic circuit boards with area sizes of the order of 20x20 sq cm on board of satellites and space vehicles. Usually irradiating them at different fluence values assesses the radiation damage in these types of devices. As a result, there is a need for a radiation source with large spatial fluence uniformity for the study of the damage by radiation from space in those devices. Kent State University s Program on Electron Beam Technology has access to an electron accelerator used for both research and industrial applications. The electron accelerator produces electrons with energies in the interval from 1 to 5 MeV and a maximum beam power of 150 kW. At such high power levels, the electron beam is continuously scanned back and forth in one dimension in order to provide uniform irradiation and to prevent damage to the sample. This allows for the uniform irradiation of samples with an area of up to 1.32 sq m. This accelerator has been used in the past for the study of radiation damage in solar cells (1). However in order to irradiate extended area solar cells there was a need to measure the uniformity of the irradiation zone in terms of fluence. In this paper the methodology to measure the fluence uniformity on a sample handling system (linear motion system), used for the irradiation of research samples, along the irradiation zone of the above-mentioned facility is described and the results presented. We also illustrate the use of the electron accelerator for the irradiation of large area solar cells (of the order of 156 sq cm) and include in this paper the electrical characterization of these types of solar cells irradiated with 5 MeV electrons to a total fluence of 2.6 x 10(exp 15) e/sq cm.

Uribe, Roberto M.↗
DOE OSTI2025

Mapping causal patterns in crystalline solids

The evolution of the atomic structures of the combinatorial library of Sm-substituted thin film BiFeO 3 along the phase transition boundary from the ferroelectric rhombohedral phase to the non-ferroelectric orthorhombic phase is explored using scanning transmission electron microscopy. Localized properties, including polarization, lattice parameter, and chemical composition, are parameterized from atomic-scale imaging, and their causal relationships are reconstructed using a linear non-Gaussian acyclic model. This approach is further extended to explore the spatial variability of the causal coupling using the sliding window transform method, which revealed that new causal relationships emerged at both the expected locations, such as domain walls and interfaces, and at additional regions forming clusters in the vicinity of the walls or spatially distributed features. While the exact physical origins of these relationships are unclear, they likely represent nanophase-separated regions in the morphotropic phase boundaries. Overall, we posit that an in-depth understanding of complex disordered materials away from thermodynamic equilibrium necessitates understanding not only the generative processes that can lead to observed microscopic states but also the causal links between multiple interacting subsystems.

Causal inference↗