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At least 325 records · Page 18

Using refractive lenses to provide a variable spot size for Kirkpatrick–Baez mirrors

For many X-ray microprobe experiments it is desirable to be able to vary the beam size: using large beams for survey scans and a small beam for the final measurements. Beryllium refractive lenses were found to be a simple and controllable method for enlarging the focus in a Kirkpatrick–Baez-based microprobe. They can provide variable spot size, can be quickly inserted or removed and do not move the beam center on the sample.

47 OTHER INSTRUMENTATION↗

Focusing with saw-tooth refractive lenses at a high-energy X-ray beamline

The Advanced Photon Source 1-ID beamline, operating in the 40–140 keV X-ray energy range, has successfully employed continuously tunable saw-tooth refractive lenses to routinely deliver beams focused in both one and two dimensions to experiments for over 15 years. The practical experience of implementing such lenses, made of silicon and aluminium, is presented, including their properties, control, alignment, and diagnostic methods, achieving ∼1 µm focusing (vertically). Ongoing development and prospects towards submicrometre focusing at these high energies are also mentioned.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

An automated approach to the alignment of compound refractive lenses

Compound refractive lenses (CRLs) are established X-ray focusing optics, and are used to focus the beam or image the sample in many beamlines at X-ray facilities. While CRLs are quite established, the stack of single lens elements affords a very small numerical aperture because of the thick lens profile, making them far more difficult to align than classical optical lenses that obey the thin-lens approximation. This means that the alignment must be very precise and is highly sensitive to changes to the incident beam, often requiring regular readjustments. Some groups circumvent the full realignment procedure by using engineering controls ( e.g. mounting optics) that sacrifice some of the beam's focusing precision, i.e. spot size, or resolution. While these choices minimize setup time, there are clear disadvantages. This work presents a new automated approach to align CRLs using a simple alignment apparatus that is easy to adapt and install at different types of X-ray experiments or facilities. This approach builds on recent CRL modeling efforts, using an approach based on the Stochastic Nelder–Mead (SNM) simplex method. This method is outlined and its efficacy is demonstrated with numerical simulation that is tested in real experiments conducted at the Advanced Photon Source to confirm its performance with a synchrotron beam. This work provides an opportunity to automate key instrumentation at X-ray facilities.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

High-throughput homogenization of a quasi-Gaussian ultrafast laser beam using a combined refractive beam shaper and spatial light modulator

Efficiently shaping femtosecond, transverse Gaussian laser beams to flat-top beams with flat wavefronts is critical for large-scale material processing and manufacturing. Existing beam shaping devices fall short either in final beam homogeneity or efficiency. Here, we present an approach that uses refractive optics to perform the majority of the beam shaping and then uses a fine-tune device (spatial light modulator) to refine the intensity profile. For the beam that we selected, circularly asymmetric with intensity fluctuations, our method achieved a uniformity of 0.055 within 90% of the beam area at 92% efficiency. The optimization involved an iterative beam shaping process that converged to optimum within 10 iterations.

43 PARTICLE ACCELERATORS↗

A Free Spectroscopic Databank of Optical Constants for Use in Optics Education and Modeling: complex refractive index data n and k from 1.0 to 25 um

The reflectance spectra of solid and liquids can be complicated since they depend not only on absorption, but also on the refraction, reflection, and scattering of light, all of which are wavelength dependent. The physical form and morphological effects associated with solid and liquid samples are thus known to affect their reflectance spectra in a non-linear fashion, particularly in the infrared. Measuring the optical constants n(?) and k(?) represents an alternative approach, allowing one to model these many effects and thus requiring fewer laboratory measurements. In this paper an overview is presented of the protocols used to measure the n/k optical constants, particularly for liquids. For the liquids, a multiple path length measurements approach is employed, and in this paper we demonstrate the method to determine the complex optical constants n(?) and k(?) of squalene. The resultant calculated spectra of 1 µm and 100 µm thick layers of squalene on an aluminum substrate as derived from the experimental n(?) and k(?) values are shown to demonstrate such effects. The public availability of the n(?)/k(?) data as well as solids hemispherical reflectance data are also discussed.

optical constants, refractive index, solids, Liqui↗

Correlation between the Molecular Refractions of Crystals and the Ionic Radii of the Cations in the Rare-Earth Trifluoride Homologous Series

We have identified linear correlations between the molecular refractions R{sub mol} (cm{sup 3}/mol) of crystals and the ionic radii r{sub i} (Å) of the cations in the RF{sub 3} rare-earth trifluoride homologous series: R{sub mol} = 8.33r{sub i} + 0.102 for R = La–Nd and R{sub mol} = 13.03r{sub i}–4.42 for R = Sm–Lu. The fact that the RF{sub 3} rare-earth trifluorides can be divided into two groups is related to the morphotropic transition from the LaF{sub 3} (tysonite) structure to the β-YF{sub 3} structure. The correlation found here for RF{sub 3} crystals with the β-YF{sub 3} structure because the electronic structure of Y (4d{sup 1}5s{sup 2}) differs from that of Sm–Lu (4f{sup 6–14}5d{sup 0–1}6s{sup 2}) in that it has no 4f electrons.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Dynamics of a Wave Packet of Whispering-Gallery-Mode Type in an Optical Waveguide in the Presence of a Traveling Refractive-Index Wave

It is demonstrated that strong ultrafast modulation of a tunneling wave packet of the whispering-gallery-mode type can be implemented in a cylindrical optical waveguide exhibiting spatiotemporal inhomogeneity induced by a travelling refractive-index wave. The corresponding optical waveguides can be used for efficient generation of picosecond and subpicosecond laser pulses.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Optical properties and refractive indices of Gd{sub 3}Al{sub 2}Ga{sub 3}O{sub 12}:Ce{sup 3+} crystals

Crystals of cerium-doped gadolinium–gallium–aluminum garnet have been grown by the Czochralski method. The transmission and reflection spectra of these crystals in the wavelength range of 250–800 nm have been obtained by optical spectroscopy. Refractive indices are calculated based on the measured Brewster angles, the experimental results are approximated using the Cauchy equation, and a dispersion dependence is obtained.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Violation of light beam reversibility principle in optical media with a random quasi-zero refractive index

We report on experimental and theoretical evidence of the violation of one of the fundamental principles in the Fresnel optics, namely, light beam reversibility, in new nanostructured composite metamaterials with silver nanoparticle in a polymer matrix. It is shown that optical transmittance of (PMMA + Ag)/glass samples in counter directions is not the same. We propose a theoretical explanation of this phenomenon based on the effect of photon localization on the surface of the composite layer with a random quasizero refractive index.

36 MATERIALS SCIENCE↗

An Optical Differentiator Based on a Three-Layer Structure with a W-Shaped Refractive Index Profile

An optical differentiator based on a three-layer resonant structure with a W-shaped refractive index profile is proposed. The differentiation operation is performed in reflection and is associated with the resonant excitation of an eigenmode of the structure localized in the central layer. The presented results of numerical simulations demonstrate the possibility of spatial differentiation of the transverse profile of an incident optical beam, temporal differentiation of the envelope of an incident optical beam, and simultaneous spatial and temporal differentiation with a high quality. The proposed structure can find applications in designing analog optical computing and optical information processing systems.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Masking of a High-Reflectivity Sphere by a Layer with a Random Quasi-Zero Refractive Index

The method of masking of a large-radius sphere made of an arbitrary material by a masking coating with a random quasi-zero refractive index is substantiated theoretically and experimentally. In this method of masking, the sphere is first coated with a mirror layer (e.g., high-reflectivity silver) and then with a masking layer with a thickness much smaller than the radius of the sphere. The fraction of the external radiation intensity bending around the sphere at the points of observation near the surface of the sphere and the extinction cross section of the sphere with the masking coating for points of observation far away from the sphere are calculated. It is shown that extinction cross section Q of the sphere with a masking coating is much smaller than 2D, where D is the geometrical cross section of the sphere; this corresponds to the masking effect for the sphere in the wavelength range of at least 450–1200 nm in the transparency region of the masking coating.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Model of Metamaterial Based on Graphene Scrolls and Carbon Nanotubes with Negative Refractive Index

The structure of a new metamaterial with negative permittivity and permeability that is made of periodically positioned graphene/boron nitride nanoscrolls and carbon nanotubes is proposed. The parameters of the metamaterial structure with a negative refractive index for the frequency of an electromagnetic wave within the visible range (namely, from near infrared to yellow) are calculated.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗