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At least 325 records · Page 18

Drop size distribution and air velocity measurements in air assist swirl atomizer sprays

Detailed measurements of mean drop size (SMD) and size distribution parameters have been made using a Fraunhofer diffraction particle sizing instrument in a series of sprays generated by an air assist swirl atomizer. Thirty-six different combinations of fuel and air mass flow rates were examined with liquid flow rates up to 14 lbm/hr and atomizing air flow rates up to 10 lbm/hr. Linear relationships were found between SMD and liquid to air mass flow rate ratios. SMD increased with distance downstream along the center line and also with radial distance from the axis. Increase in obscuration with distance downstream was due to an increase in number density of particles as the result of deceleration of drops and an increase in the exposed path length of the laser beam. Velocity components of the atomizing air flow field measured by a laser anemometer show swirling jet air flow fields with solid body rotation in the core and free vortex flow in the outer regions.

Mao, C.-P.↗

Gas-Grain Simulation Facility (GGSF)

The goal of the Gas-Grain Simulation Facility project is to provide a microgravity laboratory to facilitate research relevant to exobiology (the study of the origin and evolution of life in the universe). Such a facility will also be useful in other areas of study important to NASA including planetary science, biology, atmospheric science, astrophysics, chemistry, and physics. To achieve this goal, the project will develop and support the GGSF, a modular facility-class payload planned for inclusion on Space Station Freedom. The GGSF will consist of the following: an experiment chamber(s) supported by subsystems that provide chamber environment regulation and monitoring capabilities; sample generation, injection, positioning, and retrieval capabilities; and computer control, data acquisition, and housekeeping capabilities. The facility will also provide analytical tools such as light-scattering measurement systems, aerosol size-spectrum measurement devices, and optical imaging systems.

Greenwald, Ken↗

Instance Segmentation for Direct Measurements of Satellites in Metal Powders and Automated Microstructural Characterization from Image Data

In this work, we propose instance segmentation as a useful tool for image analysis in materials science. Instance segmentation is an advanced technique in computer vision which generates individual segmentation masks for every object of interest that is recognized in an image. Using an out-of-the-box implementation of Mask R-CNN, instance segmentation is applied to images of metal powder particles produced through gas atomization. Leveraging transfer learning allows for the analysis to be conducted with a very small training set of labeled images. As well as providing another method for measuring the particle size distribution, we demonstrate the first direct measurements of the satellite content in powder samples. After analyzing the results for the labeled data dataset, the trained model was used to generate measurements for a much larger set of unlabeled images. The resulting particle size measurements showed reasonable agreement with laser scattering measurements. The satellite measurements were self-consistent and showed good agreement with the expected trends for different samples. Finally, we present a small case study showing how instance segmentation can be used to measure spheroidite content in the UltraHigh Carbon Steel DataBase, demonstrating the flexibility of the technique.

36 MATERIALS SCIENCE↗

New Measurements of the Particle Size Distribution of Apollo 11 Lunar Soil 10084

We have initiated a major new program to determine the grain size distribution of nearly all lunar soils collected in the Apollo program. Following the return of Apollo soil and core samples, a number of investigators including our own group performed grain size distribution studies and published the results [1-11]. Nearly all of these studies were done by sieving the samples, usually with a working fluid such as Freon(TradeMark) or water. We have measured the particle size distribution of lunar soil 10084,2005 in water, using a Microtrac(TradeMark) laser diffraction instrument. Details of our own sieving technique and protocol (also used in [11]). are given in [4]. While sieving usually produces accurate and reproducible results, it has disadvantages. It is very labor intensive and requires hours to days to perform properly. Even using automated sieve shaking devices, four or five days may be needed to sieve each sample, although multiple sieve stacks increases productivity. Second, sieving is subject to loss of grains through handling and weighing operations, and these losses are concentrated in the finest grain sizes. Loss from handling becomes a more acute problem when smaller amounts of material are used. While we were able to quantitatively sieve into 6 or 8 size fractions using starting soil masses as low as 50mg, attrition and handling problems limit the practicality of sieving smaller amounts. Third, sieving below 10 or 20microns is not practical because of the problems of grain loss, and smaller grains sticking to coarser grains. Sieving is completely impractical below about 5- 10microns. Consequently, sieving gives no information on the size distribution below approx.10 microns which includes the important submicrometer and nanoparticle size ranges. Finally, sieving creates a limited number of size bins and may therefore miss fine structure of the distribution which would be revealed by other methods that produce many smaller size bins.

McKay, D.S.↗

Estimation of particle size based on LDV measurements in a de-accelerating flow field

The accuracy of velocity measurements made with a laser velocimeter is strongly dependent upon the response of the seeding particles to the dynamics of the flow field. The smaller the particle the better the response to flow fluctuations and gradients and therefore the more accurate velocity measurement. In direct conflict is the requirement of light scattering efficiency to obtain signals with the laser velocimeter which, in general, is better as the particle size is increased. In low speed flow fields these two requirements on particle size overlap and accurate measurements may be obtained. However in high speed flows, where the velocity gradients may be severe, very small particles are required to maintain sufficient dynamic response characteristics to follow the flow. Therefore if velocity measurements are to be made in these flows, the laser velocimeter must be designed with sufficient sensitivity to obtain signals from these small particles. An insitu determination of the size distribution of kaolin particles (Al2O3, .2 + or - SiO2 . 2H2O) in the 16-foot Transonic Tunnel and the sensitivity characteristics of the laser velocimeter system is described.

Meyers, J. F.↗

Development of a high-resolution automatic digital (urine/electrolytes) flow volume and rate measurement system of miniature size

To aid in the quantitative analysis of man's physiological rhythms, a flowmeter to measure circadian patterns of electrolyte excretion during various environmental stresses was developed. One initial flowmeter was designed and fabricated, the sensor of which is the approximate size of a wristwatch. The detector section includes a special type of dielectric integrating type sensor which automatically controls, activates, and deactivates the flow sensor data output by determining the presence or absence of fluid flow in the system, including operation under zero-G conditions. The detector also provides qualitative data on the composition of the fluid. A compact electronic system was developed to indicate flow rate as well as total volume per release or the cumulative volume of several releases in digital/analog forms suitable for readout or telemetry. A suitable data readout instrument is also provided. Calibration and statistical analyses of the performance functions required of the flowmeter were also conducted.

Liu, F. F.↗

Phase Doppler Interferometry for Efficient Cloud Drop Size Distribution, Number Density, and LWC Measurements

Threats to aviation safety as a result of super-cooled large drops (SLD) has been addressed by the FAA rules change (14 CFR Part 25) with the additional icing certification requirement. SLD clouds often consist of bi-modal drop size spectra leading to significant problems in simulating and characterizing these conditions in situ and in icing wind tunnels. Legacy instrumentation for measuring drop size distributions and liquid water content are challenged under these conditions. The large size range measurement problem is addressed with the development of the Phase Doppler Interferometer, Flight Probe Dual-Range (PDI FPDR). The method is described in this report along with the measurement capabilities including the dynamic measurement range and overall working size range. The PDI instrument bases drop size measurements on the light wavelength as the measurement length scale. The light wavelength is a much more robust scale, especially as compared to the light scattering intensity. Additionally, methods for accurately characterizing the sample volume in situ based on measured drop velocity and transit time are reviewed, given the importance of this parameter for merging results and measuring LWC. Droplet coincidence in the sample volume can be problematic so this condition is treated with an innovative signal parsing approach. Measurement examples acquired in the NASA IRT are provided. Measurements of LWC showed good agreement with the Artium Particle Imaging (PI) instrument but diverged from the tunnel calibration results for larger MVD values.

42 ENGINEERING↗

CACTI: Best Estimate Aerosol Size Distribution by airborne measurements

These data were collected during the Cloud, Aerosol, and Complex Terrain Interactions (CACTI; https://www.arm.gov/research/campaigns/amf2018cacti ) field campaign in the Sierras de Córdoba mountain range of north-central Argentina as part of ARM Aerial Facility (AAF) deployment. The ARM Aerial Facility Gulfstream-1 was operated from Las Higueras Airport (IATA: RCU, ICAO: SAOC), Río Cuarto, Córdoba, Argentina, for the Intensive Observation Period (IOP) from Nov. 1 through Dec. 15, 2018. The G-1 aircraft performed 22 research flights over the first ARM Mobile Facility (AMF1) location in the Sierras de Córdoba mountain range to measure atmospheric state and turbulence, cloud water content and droplet size distributions, aerosol precursor gases, aerosol chemical composition and size distributions. The current data set presents Best Estimate Aerosol Size Distribution: a merged aerosol size distribution composed of the data from 5 sensors; three aerosol spectrometers: Scanning Mobility Particle Sizer (SMPS), Ultra-High Sensitivity Aerosol Spectrometer (UHSAS), and Passive Cavity Aerosol Spectrometer (PCASP); and two cloud probes: Cloud Aerosol Spectrometer (CAS) and Fast Cloud Droplet Probe (FCDP). The SMPS data were interpolated to 1 second from “native” time resolution of about 64 second to match all other probes.

54 ENVIRONMENTAL SCIENCES↗

Antimisting fuel breakup and flammability

The breakup behavior and flammability of antimisting turbine fuels subjected to aerodynamic shear are investigated. Fuels tested were Jet A containing 0.3% FM-9 polymer at various levels of degradation ranging from virgin AMK to neat Jet A. The misting behavior of the fuels was quantified by droplet size distribution measurements. A technique based on high resolution laser photography and digital image processing of photographic records for rapid determination of droplet size distribution was developed. The flammability of flowing droplet-air mixtures was quantified by direct measurements of temperature rise in a flame established in the wake of a continuous ignition source. The temperature rise measurements were correlated with droplet size measurements. The flame anchoring phenomenon associated with the breakup of a liquid fuel in the wake of bluff body was shown to be important in the context of a survivable crash scenario. A pass/fail criterion for flammability testing of antimisting fuels, based on this flame-anchoring phenomenon, was proposed. The role of various ignition sources and their intensity in ignition and post-ignition behavior of antimisting fuels was also investigated.

Parikh, P.↗

Particle size distributions from TRACER-MAP

Particle size distributions measured using a custom scanning mobility analyzer (SMPS) and a TSI, Inc. aerodynamic particle sizer (APS). The size distributions measured with the two instruments were merged during data inversion to produce a single distribution spanning a diameter range from approximately 19 nanometers to 15 micrometers. Size-dependent cloud condensation nuclei (CCN) activity measured with a CCN counter operated in parallel to the condensation particle counter in the SMPS are reported separately. The measurements were made from the Baylor University/University of Houston Mobile Air Quality Laboratory (MAQL) between July 5 and August 30, 2022 during the TRACER-MAP project. The trailer moved between five sites in the Houston regions as follows: Aldine: 7/5-7/8, 7/21-7/26, 8/15-8/24 University of Houston: 7/8-7/16, 8/8-8/15 San Jacinto monument: 7/16-7/21 Jones State Forest: 7/26-8/1; 8/24-8/30 AMF site in La Porte: 8/1-8/8

54 ENVIRONMENTAL SCIENCES↗

Particle size distributions from TRACER-MAP

Particle size distributions measured using a custom scanning mobility analyzer (SMPS) and a TSI, Inc. aerodynamic particle sizer (APS). The size distributions measured with the two instruments were merged during data inversion to produce a single distribution spanning a diameter range from approximately 19 nanometers to 15 micrometers. Size-dependent cloud condensation nuclei (CCN) activity measured with a CCN counter operated in parallel to the condensation particle counter in the SMPS are reported separately. The measurements were made from the Baylor University/University of Houston Mobile Air Quality Laboratory (MAQL) between July 5 and August 30, 2022 during the TRACER-MAP project. The trailer moved between five sites in the Houston regions as follows: Aldine: 7/5-7/8, 7/21-7/26, 8/15-8/24 University of Houston: 7/8-7/16, 8/8-8/15 San Jacinto monument: 7/16-7/21 Jones State Forest: 7/26-8/1; 8/24-8/30 AMF site in La Porte: 8/1-8/8

54 ENVIRONMENTAL SCIENCES↗

NPFTURBULENCE: Best Estimate Aerosol Size Distribution by airborne measurements

The original data were collected during the field campaign of “Turbulent layers promoting New Particle Formation” experiment (NPFTURBULENCE; https://www.arm.gov/research/campaigns/aaf2024npfturbulence) over the Atmospheric Radiation Measurement (ARM) Southern Great Plains (SGP) Atmospheric Observatory (https://www.arm.gov/capabilities/observatories/sgp ) in north-central Oklahoma. The ARM Aerial Facility ArcticShark uncrewed aerial system (UAS) was based at Blackwell–Tonkawa Municipal Airport (IATA: BWL, ICAO: KBKN, FAA LID: BKN, 36.74475° N, 97.34918° W, 313.9 m MSL), for the field campaign from May 5 through May 29, 2024. The ArcticShark UAS performed 11 flights, including 10 research flights over the Central Facility of the ARM SGP to measure atmospheric state, turbulence, surface IT temperature and imagery, aerosol number concentration and size distribution. The current data set presents Best Estimate Aerosol Size Distribution: a merged aerosol size distribution composed of the data from 2 sensors: miniaturized Scanning Electrical Mobility Sizer (mSEMS) and Portable Optical Particle Spectrometer (POPS). The mSEMS data were interpolated to 1 second from “native” time resolution of about 15 second to match the other probe. The POPS data were converted from equivalent optical size into geometric size using value of aerosol refractive index of 1.477 from the HISCALE field campaign (same geographical area, altitudes, and time of year; http://www.arm.gov/campaigns/aaf2016hiscale ).

54 ENVIRONMENTAL SCIENCES↗

Measurement of Screen-Size Effects on Intensity, Scale, and Spectrum of Turbulence in a Free Subsonic Jet

The results are reported of hot-wire anemometer measurements of the fluctuating longitudinal component of the turbulent velocities in the mean flow downstream of screens in an air jet. These measurements have been analyzed by well-established techniques to give the influence of tile screen mesh size on the turbulent intensity, scale, and the power-spectral-density. The results show a linear dependence of the intensity upon the screen mesh size for locations within the central core of the air jet. The spectral-density curves show that the screens redistribute the turbulent energy from the low frequencies (<1000 cps) to the high frequencies (>1000 cps). The effects of the screens are overwhelmed in the mixing region of the jet flow by the turbulence levels existing there. The large pressure drops occurring across the screens reduce the velocity of the jet as compared to the jet without screens by approximately one-third for the velocity and range of mesh sizes investigated and reported in this report. The turbulence scale is a linear function of distance from the nozzle exit and is somewhat greater than comparable jets without screens.

Howard, Charles D.↗

A Summary of the Microstructural Characterization Results for the A709 Commercial Heats

To improve high temperature strength for advanced nuclear reactors, it is necessary to qualify additional structural materials for introduction into the American Society of Mechanical Engineers (AMSE) Boiler and Pressure Vessel Code (BPVC). Specifically, Alloy 709 was identified as a material for Sodium-cooled Fast Reactors to enhance time-dependent mechanical properties compared to 316H stainless steel, a code qualified high temperature alloy. Idaho National Laboratory (INL) and Oak Ridge National Laboratory (ORNL) performed initial microstructure and mechanical property testing on a third, commercial heat of Alloy 709 stainless steel. The Alloy 709 plate was produced by Allegheny Technology Inc. (ATI) and in the solution annealed condition. The chemical composition was within the limits for an American Society of Testing and Materials (ASTM) A213 specification for seamless tube for material UNS S31025. Grain size was measured as an average ASTM size of 6.5, which was larger than the ASTM 7 required according to ASTM A213 for seamless tube. The chemical composition was within the limits for an ASTM A213, and the room temperature tensile tests and hardness data met ASTM A213 specifications. Creep-fatigue results showed similar behavior to previous heats of Alloy 709.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Pinatubo and pre-Pinatubo optical-depth spectra: Mauna Loa measurements, comparisons, inferred particle size distributions, radiative effects, and relationship to lidar data

The Ames airborne tracking sunphotometer was operated at the National Oceanic and Atmospheric Administration (NOAA) Mauna Loa Observatory (MLO) in 1991 and 1992 along with the NOAA Climate Monitoring and Diagnostics Laboratory (CMDL) automated tracking sunphotometer and lidar. June 1991 measurements provided calibrations, optical-depth spectra, and intercomparisons under relatively clean conditions; later measurements provided spectra and comparisons for the Pinatubo cloud plus calibration checks. June 1991 results are similar to previous MLO springtime measurements, with midvisible particle optical depth at the near-background level of 0.012 +/- 0.006 and no significant wavelength dependence in the measured range (lambda = 0.38 to 1.06 micrometers). The arrival of the Pinatubo cloud in July 1991 increased midvisible particle optical depth by more than an order of magnitude and changed the spectral shape of to an approximate power law with an exponent of about -1.4. By clearly September 1991, the spectrum was broadly peaked near 0.5 micrometers, and by July 1992, it was peaked near 0.8 micrometers. Our optical-depth spectra include corrections for diffuse light. NOAA- and Ames Research Center (ARC)-measured spectra are in good agreement. Columnar size distributions inverted from the spectra show that the initial (July 1991) post-Pinatubo cloud was relatively rich in small particles (r less than 0.25 micrometers), which were progressively depleted in the August-September 1991 and July 1992 periods. Conversely, both of the later periods had more of the optically efficient medium-sized particles (0.25 less than r less than 1 micrometers) than did the fresh July 1991 cloud. These changes are consistent with particle growth by condensation and coagulation. Photometer-inferred column backscatter values agree with those measured by the CMDL lidar on nearby nights. Combining lidar-measured backscatter profiles with photometer-derived backscatter-to-area ratios gives peak particle areas that could cause rapid heterogeneous loss of ozone, given sufficiently low particle acidity and suitable solar zenith angles (achieved at mid- to high latitudes). Top-of-troposphere radiative forcings for the September 1991 and July 1992 optical depths and size distributions over MLO are about -5 and -3 W/sq m, respectively (hence comparable in magnitude but opposite in sign to the radiative forcing caused by the increase in manmade greenhouse gases since the industrial revolution). Heating rates in the Pinatubo layer over MLO are 0.55 +/- 0.13 and 0.41 +/- 0.14 K/d for September 1991 and July 1992, respectively.

Russell, P. B.↗

Measuring the sea ice floe size distribution

The sea ice covering the Arctic Ocean is broken into distinct pieces,called floes. In the summer, these floes, which have diameters ranging up to 100 km, are separated from each other by a region of open water. In the winter, floes still exist, but they are less easily identified. An understanding of the geometry of the ice pack is of interest for a number of practical applications associated with transportation in ice-covered seas and with the design of offshore structures intended to survive in the presence of ice. The present investigation has the objective to clarify ideas about floe sizes and to propose techniques for measuring them. Measurements are presented with the primary aim to illustrate points of technique or approach. A preliminary discussion of the floe size distribution of sea ice is devoted to questions of definition and of measurement.

Rothrock, D. A.↗