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At least 343 records · Page 19

Thermally distinct ejecta blankets from Martian craters

A study of Martian ejecta blankets is carried out using the high-resolution thermal IR/visible data from the Termoskan instrument aboard Phobos '88 mission. It is found that approximately 100 craters within the Termoskan data have an ejecta blanket distinct in the thermal infrared (EDITH). These features are examined by (1) a systematic examination of all Termoskan data using high-resolution image processing; (2) a study of the systematics of the data by compiling and analyzing a data base consisting of geographic, geologic, and mormphologic parameters for a significant fraction of the EDITH and nearby non-EDITH; and (3) qualitative and quantitative analyses of localized regions of interest. It is noted that thermally distinct ejecta blankets are excellent locations for future landers and remote sensing because of relatively dust-free surface exposures of material excavated from depth.

Betts, Bruce H.↗

Surface characterization of LDEF materials

The NASA Long Duration Exposure Facility (LDEF), a passive experimental satellite, was placed into low-Earth orbit by the Shuttle Challenger in Apr. 1984. The LDEF spent an unprecedented 69 months in space. The flight and recovery of the LDEF provided a wealth of information on the longterm space environmental effects of a variety of materials exposed to the low-Earth orbit environment. Surface characterization of LDEF materials included polymers, composites, thermal control paints, and aluminum. X-ray photoelectron spectroscopy (XPS), Auger electron spectroscopy (AES), scanning electron microscopy (SEM), and contact angle analysis were used to document changes in both the surface composition and surface chemistry of these materials. Detailed XPS analysis of the polymer systems, such as Kapton, polyimide polysiloxane copolymers, and fluorinated ethylene propylene thermal blankets on the backside of the LDEF revealed significant changes in both the surface composition and surface chemistry as a result of exposure to the low-Earth orbit environment. Polymer systems such as Kapton, polyimide polysiloxane copolymers, and polysulfone showed a common trend of decreasing carbon content and increasing oxygen content with respect to the control sample. Carbon 1s curve fit XPS analysis of the composite samples, in conjunction with SEM photomicrographs, revealed significant ablation of the polymer matrix resin to expose the carbon fibers of the composite during exposure to the space environment. Surface characterization of anodized aluminum tray clamps, which were located at regular intervals over the entire LDEF frame, provided the first results to evaluate the extent of contamination with respect to position on the LDEF. The XPS results clearly showed that the amount and state of both silicon and fluorine contamination were directly dependent upon the position of the tray clamp on the LDEF.

Wightman, J. P.↗

Development of processing techniques for advanced thermal protection materials

The main purpose of this work has been in the development and characterization of materials for high temperature applications. Thermal Protection Systems (TPS) are constantly being tested, and evaluated for increased thermal shock resistance, high temperature dimensional stability, and tolerance to environmental effects. Materials development was carried out through the use of many different instruments and methods, ranging from extensive elemental analysis to physical attributes testing. The six main focus areas include: (1) protective coatings for carbon/carbon composites; (2) TPS material characterization; (3) improved waterproofing for TPS; (4) modified ceramic insulation for bone implants; (5) improved durability ceramic insulation blankets; and (6) ultra-high temperature ceramics. This report describes the progress made in these research areas during this contract period.

Selvaduray, Guna S.↗

Thermal Performance of Biological Substance Systems in Vitro Under Static and Dynamic Conditions at the Cryogenic Test Laboratory, NASA Kennedy Space Center, USA

A unique research program, including a comprehensive study of thermal performance at cryogenic vacuum insulation systems, was performed at the NASA Kennedy Space Center. The main goal was to develop a new soft vacuum system (from 1 torr to 10 torr) that provides an intermediate level of performance (k-value below 4.8 mW/m-K). Liquid nitrogen boil-off methods were used to test conventional materials, novel materials, and certain combinations. The test articles included combinations of aluminum foil, fiberglass paper, polyester fabric, silica aerogel composite blanket, fumed silica, silica aerogel powder, and syntactic foam. A new LCI system was developed at the Cryogenics Test Laboratory. This system performs exceptionally well at soft vacuum levels and nearly as good as an MLI at high vacuum levels. Apparent thermal conductivities for the LCI range from 2 mW/m-K at soft vacuum to 0.1 mW/m-K at high vacuum. Several cryostats were designed, constructed, and calibrated by the Cryogenics Test Laboratory at KSC NASA as part of this research program. The cryostat test apparatus is a liquid nitrogen boil-off calorimeter system for direct measurement of the apparent thermal conductivity at a fixed vacuum level between 5 x 10(exp -5) and 760 torr. The apparatus is also used for transient measurements of temperature profiles. The development of efficient, robust cryogenic insulation systems has been a targeted area of research for a number of years. Improved methods of characterization, testing, and evaluation of complex biological substance systems for cryosurgery and cryobiology are the focus of this paper.

Augustynowicz, S. D.↗

Characterization of the Catalog Fengyun-1C Fragments and Their Long-term Effect on the LEO Environment

The intentional breakup of Fengyun-1C on 11 January 2007 created the most severe orbital debris cloud in history. More than 2500 large fragments were identified and tracked by the U.S. Space Surveillance Network by the end of the year. The altitude where the event occurred was probably the worst location for a major breakup in the low Earth orbit (LEO) region, since it was already highly populated with operational satellites and debris generated from previous breakups. The addition of so many fragments not only poses a realistic threat to operational satellites in the region, but also increases the instability (i.e., collision cascade effect) of the debris population there. Preliminary analysis of the large Fengyun-1C fragments indicates that their size and area-to-mass ratio (A/M) distributions are very different from those of other known events. About half of the fragments appear to be composed of light-weight materials and more than 100 of them have A/M values exceeding 1 square meter per kilogram, consistent with thermal blanket pieces. In addition, the orbital elements of the fragments suggest nontrivial velocity gain by the fragment cloud during the impact. These important characteristics were incorporated into a numerical simulation to assess the long-term impact of the Fengyun-1C fragments to the LEO debris environment. The main objectives of the simulation were to evaluate (1) the collision probabilities between the Fengyun-1C fragments and the rest of the catalog population and (2) the collision activities and population growth in the region in the next 100 years.

Liou, J.-C.↗

Investigation of the NOAA N' S Search and Rescue Antenna Inadvertent Deployment: Type C Mishap

The NOAA N' Search and Rescue Antenna (SRA) inadvertently deployed during a spacecraft rotation on April 14,2007. This rotation was part of a normal operation to configure the spacecraft for additional antenna and the solar array boom deployments. This procedure (red flag written) had been modified to look for a lost metal washer and a thermal blanket button. The modification to the procedure was reviewed and approved by the Lockheed Martin Missiles and Space (LMMS) Material Review Board (MRB) per standard procedures. The flag to the procedure introduced a counter clockwise rotation before the normal clockwise rotation. The antenna was temporally stowed and held in place via lacing cord. The lacing cord broke and allowed the SRA to inadvertently deploy during the clockwise rotation. The SRA broke through a hard stop bracket and damaged an instrument optical sensor radiator panel. The satellite damage appears to be minimal and there were no injuries to personnel. The damage to the Advanced Microwave Sounding Unit (AMSU)-A1 instrument has not been fully assessed. Based on mishap site visits, interviews and data analysis, the Mishap Investigation Team (MIT) identified the underlying causes of the mishap. Event and causal factor tree diagrams were developed, resulting in the identification of the proximate (or direct) cause and root causes of the mishap.

Sabelhaus, Phil↗

Atomic Oxygen Fluence Monitor

This innovation enables a means for actively measuring atomic oxygen fluence (accumulated atoms of atomic oxygen per area) that has impinged upon spacecraft surfaces. Telemetered data from the device provides spacecraft designers, researchers, and mission managers with real-time measurement of atomic oxygen fluence, which is useful for prediction of the durability of spacecraft materials and components. The innovation is a compact fluence measuring device that allows in-space measurement and transmittance of measured atomic oxygen fluence as a function of time based on atomic oxygen erosion yields (the erosion yield of a material is the volume of material that is oxidized per incident oxygen atom) of materials that have been measured in low Earth orbit. It has a linear electrical response to atomic oxygen fluence, and is capable of measuring high atomic oxygen fluences (up to >10(exp 22) atoms/sq cm), which are representative of multi-year low-Earth orbital missions (such as the International Space Station). The durability or remaining structural lifetime of solar arrays that consist of polymer blankets on which the solar cells are attached can be predicted if one knows the atomic oxygen fluence that the solar array blanket has been exposed to. In addition, numerous organizations that launch space experiments into low-Earth orbit want to know the accumulated atomic oxygen fluence that their materials or components have been exposed to. The device is based on the erosion yield of pyrolytic graphite. It uses two 12deg inclined wedges of graphite that are over a grit-blasted fused silica window covering a photodiode. As the wedges erode, a greater area of solar illumination reaches the photodiode. A reference photodiode is also used that receives unobstructed solar illumination and is oriented in the same direction as the pyrolytic graphite covered photodiode. The short-circuit current from the photodiodes is measured and either sent to an onboard data logger, or transmitted to a receiving station on Earth. By comparison of the short-circuit currents from the fluence-measuring photodiode and the reference photodiode, one can compute the accumulated atomic oxygen fluence arriving in the direction that the fluence monitor is pointing. The device produces a signal that is linear with atomic oxygen fluence using a material whose atomic oxygen erosion yield has been measured over a period of several years in low-Earth orbit.

Banks, Bruce A.↗

Analyses of Hubble Space Telescope Aluminized-Teflon Insulation Retrieved After 19 Years of Space Exposure

Since its launch in April 1990, the Hubble Space Telescope (HST) has made many important observations from its vantage point in low Earth orbit (LEO). However, as seen during five servicing missions, the outer layer of multilayer insulation (MLI) has become successively more embrittled and has cracked in many areas. In May 2009, during the 5th servicing mission (called SM4), two MLI blankets were replaced with new insulation pieces and the space-exposed MLI blankets were retrieved for degradation analyses by teams at NASA Glenn Research Center (GRC) and NASA Goddard Space Flight Center (GSFC). The MLI blankets were from Equipment Bay 8, which received direct sunlight, and Equipment Bay 5, which received grazing sunlight. Each blanket contained a range of unique regions based on environmental exposure and/or physical appearance. The retrieved MLI blanket s aluminized-Teflon (DuPont) fluorinated ethylene propylene (Al-FEP) outer layers have been analyzed for changes in optical, physical, and mechanical properties, along with space induced chemical and morphological changes. When compared to pristine material, the analyses have shown how the Al-FEP was severely affected by the space environment. This paper reviews tensile properties, solar absorptance, thermal emittance, x-ray photoelectron spectroscopy (XPS) data and atomic oxygen erosion values of the retrieved HST blankets after 19 years of space exposure.

deGroh, Kim K.↗

Fresh lunar impact craters - Review of variations with size

Thirty-three morphologic characteristics are reviewed for fresh lunar impact craters wider than 1 km. Bar graphs express the way each characteristic varies with crater size. The features are grouped as crater structure, ejecta, and downhill flow features. Major structural transitions occur at diameters of about 15 and 200 km. Details of the ejecta blanket, which include several kinds of lineations, dunelike ridges, troughs, and lobes, reflect different transport regimes in the ejecta. Some materials at larger craters flowed downhill in lavalike fashion after the ejecta was deposited; the lavalike materials are probably impact melt.

Howard, K. A.↗

LDEF materials results for spacecraft applications: Executive summary

To address the challenges of space environmental effects, NASA designed the Long Duration Exposure Facility (LDEF) for an 18-month mission to expose thousands of samples of candidate materials that might be used on a space station or other orbital spacecraft. LDEF was launched in April 1984 and was to have been returned to Earth in 1985. Changes in mission schedules postponed retrieval until January 1990, after 69 months in orbit. Analyses of the samples recovered from LDEF have provided spacecraft designers and managers with the most extensive data base on space materials phenomena. Many LDEF samples were greatly changed by extended space exposure. Among even the most radially altered samples, NASA and its science teams are finding a wealth of surprising conclusions and tantalizing clues about the effects of space on materials. Many were discussed at the first two LDEF results conferences and subsequent professional papers. The LDEF Materials Results for Spacecraft Applications Conference was convened in Huntsville to discuss implications for spacecraft design. Already, paint and thermal blanket selections for space station and other spacecraft have been affected by LDEF data. This volume synopsizes those results.

Whitaker, A. F.↗

Effect of Cyclic Aeroconvective Heating on Flexible Thermal Insulations

This paper describes the effect of cyclic aeroconvective heating on the thermal performance of ceramic flexible insulations considered for potential use as thermal protection systems or thermal insulations for future hypersonic vehicles such as the Reusable Launch Vehicles (RLV's) and other applications where structures require thermal protection from severe heating. The thermal response of these materials after exposure to cyclic aeroconvective heating from a plasma arc is described. The thermal insulations evaluated were Composite Flexible Blanket Insulations composed of an outer layer of aluminoborosilicate fabric and alumina insulation. The insulations were evaluated with and without a high emissivity coating. These insulations were exposed to the plasma arc stream for nine minutes reaching surface temperatures of 1150 C and a heat flux of 10.5 W/sq cm. Insulations were exposed three, six, or nine times in order to demonstrate reusability and to determine the effect oi coatings on the surface durability of these insulations. Test results demonstrated the capability of these insulations to protect either composite or metallic structures from high heating environments. It is shown that high emittance coatings reduce backface temperatures. The durability of these insulations when impacted at low velocities was also demonstrated. The interaction of the coatings with the ceramic fibers was characterized. An analytical thermal model was utilized to correlate experimental thermal test results with calculated values.

Kourtides, Demetrius A.↗

Martian Surface Properties: Inferences from Resolved Differences in Crater Geometries

Impact craters are a natural probe of planetary sub-surfaces, both from the excavated material and from crater geometries, which are sensitive to material properties of the target. One of the most intriguing aspects of Martian craters is the morphology of the ejecta blankets. All fresh and many older Martian craters larger than a few km are surrounded by ejecta blankets which appear fluidized, with morphologies believed to form by entrainment of liquid water. In addition to the ejecta morphology, quantitative information about the subsurface composition may be derived from geometrical measurements, e.g., rim uplift height and ejecta blanket volumes. In order to use craters to derive subsurface composition or test rampart morphology formation hypotheses, accurate measurements with quantified error estimates are required. We have developed and tested a toolkit for measurements of crater geometry using the MOLA altimetry data. Here, we present the results from geometry measurements on fresh craters in Lunae Planum and Utopia Planitia.

Valiant, G. J.↗

History and State of the Art in Advanced Thermal Protection Systems

This report documents the current state of the art of thermal protection systems (TPS) relevant to missile application materials and MTCR control language. The information is intended to provide data on current TPS for determining the current state of development and identifying potential research directions. Various vehicle configurations and types of TPS are described, including the evolution of materials and systems. Vehicle configurations such as high drag rocket and capsule systems and low-drag air-breathers are discussed. TPS are complex, transitioning from often very low temperatures to temperatures exceeding 3000°C and heat fluxes of up to 30,000 W/cm 2 . They can take the form of blankets, sheets, tiles and fabricated rigid structures, and can be made from high temperature capable alloys, refractory metals, ceramics, ceramic matrix composites, ultra-high temperature ceramics, carbon-carbon composites or ablative carbonaceous materials. Current state of the art in TPS is based on materials any systems developed for the initial space program. TPS was upgraded to the point of the Space Shuttle development and has stagnated since them.

36 MATERIALS SCIENCE↗

Degradation of Hubble Space Telescope Metallized Teflon(trademark) FEP Thermal Control Materials

The mechanical and optical properties of the metallized Teflon Fluorinated Ethylene Propylene (FEP) thermal control materials on the Hubble Space Telescope (HST) have degraded over the seven years the telescope has been in orbit. Astronaut observations and photographic documentation from the Second Servicing Mission revealed severe cracks of the multi-layer insulation (MLI) blanket outer layer in many locations around the telescope, particularly on solar facing surfaces. Two samples, the outer Teflon FEP MLI layer and radiator surfaces, were characterized post- mission through exhaustive mechanical, thermal, chemical, and optical testing. The observed damage to the thermal control materials, the sample retrieval and handling, and the significant changes to the radiator surfaces of HST will be discussed. Each of these issues is addressed with respect to current and future mission requirements.

Hansen, Patricia A.↗

Evaluation of the interaction between SiC, pre-oxidized FeCrAlMo with aluminized and pre-oxidized Fe-8Cr-2W in flowing PbLi

We report dissimilar materials interactions are a major concern when liquid metals are used as a working fluid. To simulate a dual-coolant PbLi blanket, chemical vapor deposited (CVD) SiC, pre-oxidized FeCrAlMo (APMT) and pre-oxidized aluminized coating on Fe-8Cr-2 W (F82H) specimens were exposed to flowing commercial Pb-17at.%Li with a peak temperature of 650 °C in a pre-oxidized APMT thermal convection loop (TCL) for 1000 h. Similar to prior results in static PbLi, the coated F82H showed small mass changes and limited degradation of room-temperature tensile properties. After exposure, the α-Al 2 O 3 on the surface coated F82H reacted with the PbLi to form LiAlO 2 . However, no significant Al coating loss or interdiffusion was observed. Mass transfer was observed between the APMT, TCL and the SiC specimens. Fe, Cr and Ni were dissolved into the molten flowing PbLi and transported through the TCL to react with the SiC specimens. Compared to a prior experiment with a majority of bare FeCrAl specimens that were exposed in a TCL with a peak temperature of 700 °C for 1000 h, the SiC reaction was reduced to only a few microns of carbides and silicides. Oxygen dissolved in the molten PbLi sustained the formation of an Al 2 O 3 scale on the surface of the coating and induced the formation of a thin surface SiO 2 layer on the surface of the SiC.

36 MATERIALS SCIENCE↗

Hypersonic Airbreathing Missile

A hypersonic airbreathing missile using dual mode scramjet engines for propulsion is described. The fuselage is constructed of a material with a high heat sink capacity and is covered with a thermal protective shield and lined with an internal insulating blanket. The engine airframe integration uses the flat lower portion of the lower fuselage to precompress the air entering the scramjet engines. The precompression of air entering the scramjet inlets increases as the angles of attack. This feature results in a highly maneuverable missile which can accelerate as it banks into a turn.

Hunt, J. L.↗

New estimates of area and mass for the North American tektite strewn field

A revised estimate is given for the total mass of the North American tektite material, which is based on a concept of patches or rays of distribution rather than on a continuous tektite and microtektite blanket. This concept yields a total mass of about 3 x 10 to the 14th g, which is less than a third of previous estimates. The shape of the North American tektite strewn field is in agreement with other tektite strewn fields.

Koeberl, C.↗

Study of balloon and thermal control material degradation aboard LDEF

The initial results of analysis performed on a number of polymeric materials which were exposed aboard the Long Duration Exposure Facility (LDEF) are discussed. These materials include two typical high altitude balloon films (a polyester and a polyethylene) and silver-backed Teflon from thermal control blanket samples. The techniques used for characterizing changes in mechanical properties, chemical structure and surface morphology include Fourier Transform Infrared (FTIR) spectroscopy, scanning electron microscopy, and dynamic mechanical analysis.

Letton, Alan↗