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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 343 records · Page 19
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Standardization work for the calibration of intensities of celestial objects

Observations of celestial phenomena need to be calibrated, to be related, to some measurable quantity. There continues to be a long-term need for accurate photometric standard stars, those with known intensities and colors, so that brightness and color measurements made of various celestial phenomena by different observers can be integrated and compared with one another. Toward this end, the author has been emphasizing data collection in recent years for stars of 'intermediate' brightness, those approximately in the magnitude range 11.5 is less than V is less than 16.0. Photoelectric data were obtained at the Cerro Tololo InterAmerican Observatory's (CTIO) telescopes for stars in certain selected areas near the celestial equator. Stars of extreme color outside the selected areas, but near the equator, also were selected to provide a more broad and complete range in color index. It was proposed to complete the photoelectric phase of the program. The author proposed developing extremely faint sequences of photometric standard stars useful for both large space-based detectors and for land-based detectors. These data were to be collected via charge-coupled devices (CCD's) at telescopes located at CTIO and at the Las Campanas Observatory (LCO), both observatories being located in Chile. It was hoped that accurate data could be collected down to the 21st or 22nd magnitude.

Landolt, Arlo U.↗
NASA NTRS2001

Multipurpose Spectroradiometer for Satellite Instrument Calibration and Zenith Sky Remote Sensing Measurements

In the early 1990s a series of surface-based direct sun and zenith sky measurements of total column ozone were made with SBUV/2 flight models and the SSBUV Space Shuttle instrument in Boulder, Colorado which were compared with NOAA Dobson Instrument direct sun observations and TOMS instrument overpass observations of column ozone. These early measurements led to the investigation of the accuracy of derived total column ozone amounts and aerosol optical depths from zenith sky observations. Following the development and availability of radiometrically stable IAD narrow band interference filter and nitrided silicon photodiodes a simple compact multifilter spectroradiometer was developed which can be used as a calibration transfer standard spectroradiometer (CTSS) or as a surface based instrument remote sensing instruments for measurements of total column ozone and aerosol optical depths. The total column ozone derived from zenith sky observations agrees with Dobson direct sun AD double wavelength pair measurements and with TOMS overpass ozone amounts within uncertainties of about 1%. When used as a calibration transfer standard spectroradiometer the multifilter spectroradiometer appears to be capable of establishing instrument radiometric calibration uncertainties of the order of 1% or less relative to national standards laboratory radiometric standards.

Heath, Donald F.↗
DOE OSTI2016

Comparison of Analytical Methods for the Determination of Uranium in Seawater Using Inductively Coupled Plasma Mass Spectrometry

Trace element determinations in seawater by inductively coupled plasma mass spectrometry are analytically challenging due to the typically very low concentrations of the trace elements and the potential interference of the salt matrix. In this study, we did a comparison for uranium analysis using inductively coupled plasma mass spectrometry (ICP-MS) of Sequim Bay seawater samples and three seawater certified reference materials (SLEW-3, CASS-5 and NASS-6) using seven different analytical approaches. The methods evaluated include: direct analysis, Fe/Pd reductive precipitation, standard addition calibration, online automated dilution using an external calibration with and without matrix matching, and online automated pre-concentration. The method which produced the most accurate results was the method of standard addition calibration, recovering uranium from a Sequim Bay seawater sample at 101 ± 1.2%. The on-line preconcentration method and the automated dilution with matrix-matched calibration method also performed well. The two least effective methods were the direct analysis and the Fe/Pd reductive precipitation using sodium borohydride

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1981

Solar cell measurements

The measurement of the electrical performance characteristics of individual solar cells is discussed. One of the reasons is determination of the output power, measurement of the effect of various degradation mechanisms, and separation of cells by current and voltage for eventual use in series and parallel combinations. Major problem areas in making accurate performance measurements are the determination of the irradiance level during measurement, the measurement and control of cell junction temperature, and the contacting of the separate current and potential leads to the cell under test. Solar cells respond to only part of the solar spectrum, irradiance measurement made with blackbody detectors lead to spectral mismatch errors. The use of reference cells with a spectral response similar to that of the test cell reduces this error. Reference cells are calibrated at standard atmospheric conditions with all cells calibrated at the same conditions.

Curtis, H. B.↗
DOE OSTI2026

Binary pseudo-random array standard for extreme ultraviolet lithography tool characterization

Extreme ultraviolet (EUV) imaging tools play a crucial role in EUV lithography. Achieving high accuracy in EUV metrology is essential for advanced semiconductor manufacturing. A thorough characterization of the instrumentation in use is required. Binary pseudo-random arrays (BPRAs) are an established standard for calibrating and characterizing optical instruments in the frequency domain. Here, we expand the BPRA standard to applications in EUV imaging. To extend the technology to the EUV spectral range, a high-resolution BPRA target with the smallest feature size of 40 nm is developed. The EUV BPRA target establishes an in situ and portable calibration and alignment standard for EUV imaging. The target is patterned by means of electron-beam lithography, using a nickel absorber with a thickness of 39 nm. The substrate is a 4″ silicon wafer with a molybdenum/silicon multilayer coating. To demonstrate the efficacy of the target and develop the instrument calibration protocol, the target is imaged on the Sharp Hyper-NA Actinic Reticle Review Project EUV mask microscope. Power spectral density (PSD) data are presented. The characteristics of the imaging system are imprinted on the PSD. The modulation transfer function is extracted from the PSD data. A partially coherent imaging model is used as a reference to the experimental results.

BPRA↗
NASA NTRS1994

Absolute flux calibration of optical spectrophotometric standard stars

A method based on Landolt photometry in B and V is developed to correct for a wavelength independent offset of the absolute flux level of optical spectrophotometric standards. The method is based on synthetic photometry techniques in B and V and is accurate to approximately 1%. The correction method is verified by Hubble Space Telescope Faint Object Spectrograph absolute fluxes for five calibration stars, which agree with Landolt photometry to 0.5% in B and V.

Colina, Luis↗
DOE OSTI2015

STANDARD STARS AND EMPIRICAL CALIBRATIONS FOR Hα AND Hβ PHOTOMETRY

We define an Hα photometric system that is designed as a companion to the well established Hβ index. The new system is built on spectrophotometric observations of field stars as well as stars in benchmark open clusters. We present data for 75 field stars, 12 stars from the Coma star cluster, 24 stars from the Hyades, 17 stars from the Pleiades, and 8 stars from NGC 752 to be used as primary standard stars in the new systems. We show that the system transformations are relatively insensitive to the shape of the filter functions. We make comparisons of the Hα index to the Hβ index and illustrate the relationship between the two systems. In addition, we present relations that relate both hydrogen indices to equivalent width and effective temperature. We derive equations to calibrate both systems for Main Sequence stars with spectral types in the range O9 to K2 for equivalent width and A2 to K2 for effective temperature.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

A round-robin gamma stereotactic radiosurgery dosimetry interinstitution comparison of calibration protocols

Purpose: Absorbed dose calibration for gamma stereotactic radiosurgery is challenging due to the unique geometric conditions, dosimetry characteristics, and nonstandard field size of these devices. Members of the American Association of Physicists in Medicine (AAPM) Task Group 178 on Gamma Stereotactic Radiosurgery Dosimetry and Quality Assurance have participated in a round-robin exchange of calibrated measurement instrumentation and phantoms exploring two approved and two proposed calibration protocols or formalisms on ten gamma radiosurgery units. The objectives of this study were to benchmark and compare new formalisms to existing calibration methods, while maintaining traceability to U.S. primary dosimetry calibration laboratory standards. Methods: Nine institutions made measurements using ten gamma stereotactic radiosurgery units in three different 160 mm diameter spherical phantoms [acrylonitrile butadiene styrene (ABS) plastic, Solid Water, and liquid water] and in air using a positioning jig. Two calibrated miniature ionization chambers and one calibrated electrometer were circulated for all measurements. Reference dose-rates at the phantom center were determined using the well-established AAPM TG-21 or TG-51 dose calibration protocols and using two proposed dose calibration protocols/formalisms: an in-air protocol and a formalism proposed by the International Atomic Energy Agency (IAEA) working group for small and nonstandard radiation fields. Each institution’s results were normalized to the dose-rate determined at that institution using the TG-21 protocol in the ABS phantom. Results: Percentages of dose-rates within 1.5% of the reference dose-rate (TG-21 + ABS phantom) for the eight chamber-protocol-phantom combinations were the following: 88% for TG-21, 70% for TG-51, 93% for the new IAEA nonstandard-field formalism, and 65% for the new in-air protocol. Averages and standard deviations for dose-rates over all measurements relative to the TG-21 + ABS dose-rate were 0.999 ± 0.009 (TG-21), 0.991 ± 0.013 (TG-51), 1.000 ± 0.009 (IAEA), and 1.009 ± 0.012 (in-air). There were no statistically significant differences (i.e., p > 0.05) between the two ionization chambers for the TG-21 protocol applied to all dosimetry phantoms. The mean results using the TG-51 protocol were notably lower than those for the other dosimetry protocols, with a standard deviation 2–3 times larger. The in-air protocol was not statistically different from TG-21 for the A16 chamber in the liquid water or ABS phantoms (p = 0.300 and p = 0.135) but was statistically different from TG-21 for the PTW chamber in all phantoms (p = 0.006 for Solid Water, 0.014 for liquid water, and 0.020 for ABS). Results of IAEA formalism were statistically different from TG-21 results only for the combination of the A16 chamber with the liquid water phantom (p = 0.017). In the latter case, dose-rates measured with the two protocols differed by only 0.4%. For other phantom-ionization-chamber combinations, the new IAEA formalism was not statistically different from TG-21. Conclusions: Although further investigation is needed to validate the new protocols for other ionization chambers, these results can serve as a reference to quantitatively compare different calibration protocols and ionization chambers if a particular method is chosen by a professional society to serve as a standardized calibration protocol.

07 ISOTOPE AND RADIATION SOURCES↗
NASA NTRS1992

Atmospheric analysis for airdata calibration on research aircraft

In-flight airdata calibrations are used to determine the aerodynamic influence of an airplane on pitot-static pressure measurements of altitude and speed. Conventional flight-test calibration techniques are briefly reviewed and meteorological analysis methods for estimating calibration reference values of atmospheric conditions are described. There are cases where some conventional in-flight techniques are not entirely satisfactory for research aircraft because of added equipment requirements or flight envelope and location limitations. In these cases, atmospheric wind and pressure information can be used to complement conventional techniques. Accuracy of the atmospheric measurements and the variability of upper-air winds and pressure values are discussed. Results from several flight research aircraft show that wind reference calibration is generally less accurate than calibration accuracy standards for civil and research aircraft. Examples of pressure reference altimetry derived from meteorological analyses are also presented for a variety of flight research programs. These flight data show that the reference pressure accuracy provided by meteorological analyses is usually within civil aircraft and flight research airdata calibration accuracy standards. Meteorological analyses altimetry is particularly useful when it is not feasible to restrict the test airplane altitude, location, or maneuver envelope.

Ehernberger, L. J.↗
NASA NTRS1974

Ar-40/Ar-39 ages and trace element contents of Apollo 14 breccias - An interlaboratory cross-calibration of Ar-40/Ar-39 standards

Rare gas data are presented from step-wise heatings of lunar breccias 14066 and 14318 and from an interlaboratory cross-calibration of five standards used in Ar-40/Ar-39 dating. While different in detail, the Ar release patterns in the four samples yield indistinguishable plateau ages of 3.93 plus or minus 0.03 b.y. and above 400 C total ages of 3.87 plus or minus 0.06 b.y. Concentrations of K, Ca, Ba, Br, U and I are given for 14318 and 14066. We also present an updating of all of the Ar-40/Ar-39 ages and trace element concentrations previously published by this laboratory.

Alexander, E. C., Jr.↗
NASA NTRS2007

Validation of Radiometric Standards for the Laboratory Calibration of Reflected-Solar Earth Observing Satellite Instruments

Historically, the traceability of the laboratory calibration of Earth-observing satellite instruments to a primary radiometric reference scale (SI units) is the responsibility of each instrument builder. For the NASA Earth Observing System (EOS), a program has been developed using laboratory transfer radiometers, each with its own traceability to the primary radiance scale of a national metrology laboratory, to independently validate the radiances assigned to the laboratory sources of the instrument builders. The EOS Project Science Office also developed a validation program for the measurement of onboard diffuse reflecting plaques, which are also used as radiometric standards for Earth-observing satellite instruments. Summarized results of these validation campaigns, with an emphasis on the current state-of-the-art uncertainties in laboratory radiometric standards, will be presented. Future mission uncertainty requirements, and possible enhancements to the EOS validation program to ensure that those uncertainties can be met, will be presented.

Butler, James J.↗
NASA NTRS1972

Piston manometer as an absolute standard for vacuum gage calibration in the range 10 to 700 microtorr

Total pressure in a calibration chamber is determined by measuring the force on a disk suspended in an orifice in the baseplate of the chamber. The disk forms a narrow annular gap with the orifice. A continuous flow of calibration gas passes through the chamber and annulus to a downstream pumping system. The ratio of pressures on the two faces of the disk exceeds 100:1, so that chamber pressure is substantially equal to the product of disk area and net force on the disk. This force is measured with an electrodynamometer that can be calibrated in situ with dead weights. Probable error in pressure measurement is plus or minus (0.5 microtorr + 0.6 percent).

Warshawsky, I.↗
NASA NTRS1979

Comparison tests and experimental compliance calibration of the proposed standard round compact plane strain fracture toughness specimen

Standard round specimen fracture test results compared satisfactorily with results from standard rectangular compact specimens machined from the same material. The location of the loading pin holes was found to provide adequate strength in the load bearing region for plane strain fracture toughness testing. Excellent agreement was found between the stress intensity coefficient values obtained from compliance measurements and the analytic solution proposed for inclusion in the standard test method. Load displacement measurements were made using long armed displacement gages and hollow loading cylinders. Gage points registered on the loading hole surfaces through small holes in the walls of the loading cylinders.

Fisher, D. M.↗
NASA NTRS1998

The Space Interferometry Mission

The Space Interferometry Mission (SIM) is the next major space mission in NASA's Origins program after SIRTF. The SIM architecture uses three Michelson interferometers in low-earth orbit to provide 4 microarcsecond precision absolute astrometric measurements on approx. 40,000 stars. SIM will also provide synthesis imaging in the visible waveband to a resolution of 10 milliarcsecond, and interferometric nulling to a depth of 10(exp -4). A near-IR (1-2 micron) capability is being considered. Many key technologies will be demonstrated by SIM that will be carried over directly or can be readily scaled to future Origins missions such as TPF. The SIM spacecraft will carry a triple Michelson interferometer with baselines in the 10 meter range. Two interferometers act as high precision trackers, providing attitude information at all time, while the third one conducts the science observations. Ultra-accurate laser metrology and active systems monitor the systematic errors and to control the instrument vibrations in order to reach the 4 microarcsecond level on wide-angle measurements. SIM will produce a wealth of new astronomical data. With an absolute positional precision of 4 microarcsecond, SIM will improve on the best currently available measures (the Hipparcos catalog) by 2 or 3 orders of magnitude, providing parallaxes accurate to 10% and transverse velocities to 0.2 km/s anywhere in the Galaxy, to stars as faint as 20th magnitude. With the addition of radial velocities, knowledge of the 6-dimension phase space for objects of interest will allow us to attack a wide array of previously inaccessible problems such as: search for planets down to few earth masses; calibration of stellar luminosities and by means of standard candles, calibration of the cosmic distance scale; detecting perturbations due to spiral arms, disk warps and central bar in our galaxy; probe of the gravitational potential of the Galaxy, several kiloparsecs out of the galactic plane; synthesis imaging of circumstellar disks around young stellar objects; imaging the narrow-line regions of AGNs in the optical; direct distance determination of a half dozen nearby spiral galaxies using rotational kinematics, thereby sidestepping reddening and metallicity issues in the calibration of distance estimators like Tully-Fisher; imaging exozodiacal dust disks (when operating in its nulling mode, SIM will be sensitive, at a distance of (beta) Pic (20 pc), to scales ranging from 0.2 to 5 AU).

Unwin, Stephen C.↗
DOE OSTI2020

Versailles Project on Advanced Materials and Standards interlaboratory study on intensity calibration for x-ray photoelectron spectroscopy instruments using low-density polyethylene

We report the results of a Versailles Project on Advanced Materials and Standards interlaboratory study on the intensity scale calibration of x-ray photoelectron spectrometers using low-density polyethylene (LDPE) as an alternative material to gold, silver, and copper. An improved set of LDPE reference spectra, corrected for different instrument geometries using a quartz-monochromated Al Kα x-ray source, was developed using data provided by participants in this study. Using these new reference spectra, a transmission function was calculated for each dataset that participants provided. When compared to a similar calibration procedure using the NPL reference spectra for gold, the LDPE intensity calibration method achieves an absolute offset of ~3.0% and a systematic deviation of ±6.5% on average across all participants. For spectra recorded at high pass energies (≥90 eV), values of absolute offset and systematic deviation are ~5.8% and ±5.7%, respectively, whereas for spectra collected at lower pass energies (<90 eV), values of absolute offset and systematic deviation are ~4.9% and ±8.8%, respectively; low pass energy spectra perform worse than the global average, in terms of systematic deviations, due to diminished count rates and signal-to-noise ratio. Differences in absolute offset are attributed to the surface roughness of the LDPE induced by sample preparation. We further assess the usability of LDPE as a secondary reference material and comment on its performance in the presence of issues such as variable dark noise, x-ray warm up times, inaccuracy at low count rates, and underlying spectrometer problems. In response to participant feedback and the results of the study, we provide an updated LDPE intensity calibration protocol to address the issues highlighted in the interlaboratory study. Finally, we also comment on the lack of implementation of a consistent and traceable intensity calibration method across the community of x-ray photoelectron spectroscopy (XPS) users and, therefore, propose a route to achieving this with the assistance of instrument manufacturers, metrology laboratories, and experts leading to an international standard for XPS intensity scale calibration.

36 MATERIALS SCIENCE↗
DOE OSTI2016

Two Photon Absorption Laser Induced Fluorescence for Neutral Hydrogen Profile Measurements

The magnitude and spatial dependence of neutral density in magnetic confinement fusion experiments is a key physical parameter, particularly in the plasma edge. Modeling codes require precise measurements of the neutral density to calculate charge-exchange power losses and drag forces on rotating plasmas. However, direct measurements of the neutral density are problematic. In this work, we proposed to construct a laser-based diagnostic capable of providing spatially resolved measurements of the neutral density in the edge of plasma in the DIII-D tokamak. The diagnostic concept is based on two-photon absorption laser induced fluorescence (TALIF). By injecting two beams of 205 nm light (co or counter propagating), ground state hydrogen (or deuterium or tritium) can be excited from the n = 1 level to the n = 3 level at the location where the two beams intersect. Individually, the beams experience no absorption, and therefore have no difficulty penetrating even dense plasmas. After excitation, a fraction of the hydrogen atoms decay from the n = 3 level to the n = 2 level and emit photons at 656 nm (the H α line). Calculations based on the results of previous TALIF experiments in magnetic fusion devices indicated that a laser pulse energy of approximately 3 mJ delivered in 5 ns would provide sufficient signal-to-noise for detection of the fluorescence. In collaboration with the DIII-D engineering staff and experts in plasma edge diagnostics for DIII-D from Oak Ridge National Laboratory (ORNL), WVU researchers designed a TALIF system capable of providing spatially resolved measurements of neutral deuterium densities in the DIII-D edge plasma. The laser systems were specified, purchased, and assembled at WVU. The TALIF system was tested on a low-power hydrogen discharge at WVU and the plan was to move the instrument to DIII-D for installation in collaboration with ORNL researchers. After budget cuts at DIII-D, the DIII-D facility declined to support installation on their tokamak. Instead, after a no-cost extension, the apparatus was moved to the University of Washington-Seattle and successfully tested on the HIT-SI3 spheromak experiment. As a result of this project, TALIF measurements of the absolutely calibrated neutral density hydrogen and deuterium were obtained in a helicon source and in a spheromak, designs were developed for installation of a TALIF system on a tokamak, and a new, xenon-based calibration scheme was proposed and demonstrated. The xenon-calibration scheme eliminates significant problems that were identified with the standard krypton calibration scheme.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗