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NASA NTRS2020

Aqueous Alteration in the Kuiper Belt: Evidence from Hydrated Interplanetary Dust Particles

Edgeworth-Kuiper belt objects (EKBOs) formed in the outer reaches of the protoplanetary disk and thus avoided much of the high tempera-ture processing experienced by bodies in the inner solar system. For this reason, they contain a wealth of information on the nature of nebular solids and the chemical conditions in the earliest solar system. Astronomical observations of EKBOs have been limited largely to the surface chemistry of the ices covering these small and difficult to observe bodies. The mineralogy of EKBO objects are poorly known, but clues regarding their mineralogical makeup come from studies of samples from short period comets (e.g. Wild2), and interplanetary dust particles (IDPs) produced by collisions in the Kuiper belt. Interplanetary dust particles from objects in the solar system (mainly comets and asteroids) spiral in to-wards the Sun under the influence of Poynting-Robertson (PR) drag forces and accumulate solar flare energetic particle tracks. Recent work has shown that the observed solar flare track densities (~1010-1011/sq.cm) in these IDPs are ~two orders of magnitude higher than expected if they were derived from main belt asteroids or Jupiter family comets and thus require an origin from outer solar system source bodies such as EKBOs. The track-rich IDPs include representatives from the two major groups of IDPs: the chondritic-porous, anhydrous IDPs and the chondritic-smooth, hydrated IDPs, although rare IDPs with mineralogies intermediate between these two groups are known. Here, we report on the mineralogy, composition, organic matter content, and isotopic characteristics of track-rich hydrated IDPs, and implications for aqueous alteration in outer solar system bodies.

Keller, L. P.↗
NASA NTRS2000

Gradient Composition Sol-Gel Materials

The STARDUST Mission, which launched in February of 1999, plans to fly through the coma of Comet 81P/Wild2, capture some of the material ejected by the comet, and return the samples to Earth in 2006.

Sol-Gel↗
NASA NTRS1997

STARDUST: Discovery's InterStellar Dust and Cometary Sample Return Mission

The STARDUST Discovery mission will collect samples of cometary and interstellar dust and return them to Earth. The Jet Propulsion Laboratory provides project management with Lockheed Martin Astronautics as the spacecraft industrial partner. STARDUST management is aggressively pursuing cost control through the use of Total Quality Management principles, specifically operating in a Project Engineering and Integration Team that

STARDUST↗
NASA NTRS2024

Simplified Meteorite Parent Body Alteration of Amino Acids By Hydrothermal Processes

Amino acids have been identified in extraterrestrial materials such as meteorites and returned samples from asteroids and comets. Some of these amino acids or their precursors may have formed on icy interstellar dust grains or at a later phase when these grains became incorporated into larger parent bodies. In this work, we simulated parent body aqueous alteration of the residues from irradiated interstellar ice analogs in the presence of relevant minerals (pulverized serpentinite and Allende meteorite). We tracked the change in amino acid abundances as a function of hydrothermal processing time and examined how these differed based on the presence of minerals. We find that the presence of minerals and their mineralogy can have a significant impact on the formation and destruction of amino acids during simulated aqueous alteration experiments.

Christopher K Materese↗
NASA NTRS2011

Surface Contact Model for Comets and Asteroids

A contact force model was developed for use in touch and go (TAG) surface sampling simulations on small celestial bodies such as comets and asteroids. In TAG scenarios, a spacecraft descending toward the surface of a small body comes into contact with the surface for a short duration of time, collects material samples with a sampler device, and then ascends to leave the surface. The surface contact required 6-DOF (degrees of freedom) dynamics models due to coupling of the attitude and translation dynamics during the contact. The model described here is for contact scenarios that utilize a rotating brush wheel sampler (BWS) to collect surface material. The model includes stiffness and damping of the surface material during BWS vertical motion, lateral friction from the BWS dragging across the surface, and lateral shear from the rotating BWS scooping the surface material. This model is useful for any mission to asteroids or comets that incorporates surface sampling operations.

Blackmore, Lars James C.↗
NASA NTRS2005

Stardust@home: A Massively Distributed Public Search for Interstellar Dust in the Stardust Interstellar Dust Collector

In January 2006, the Stardust mission will return the first samples from a solid solar system body beyond the Moon. Stardust was in the news in January 2004, when it encountered comet Wild2 and captured a sample of cometary dust. But Stardust carries an equally important payload: the first samples of contemporary interstellar dust ever collected. Although it is known that interstellar (IS) dust penetrates into the inner solar system [2, 3], to date not even a single contemporary interstellar dust particle has been captured and analyzed in the laboratory. Stardust uses aerogel collectors to capture dust samples. Identification of interstellar dust impacts in the Stardust Interstellar Dust Collector probably cannot be automated, but will require the expertise of the human eye. However, the labor required for visual scanning of the entire collector would exceed the resources of any reasonably-sized research group. We are developing a project to recruit the public in the search for interstellar dust, based in part on the wildly popular SETI@home project, which has five million subscribers. We call the project Stardust@home. Using sophisticated chemical separation techniques, certain types of refractory ancient IS particles (so-called presolar grains) have been isolated from primitive meteorites (e.g., [4] ). Recently, presolar grains have been identified in Interplanetary Dust Particles[6]. Because these grains are not isolated chemically, but are recognized only by their unusual isotopic compositions, they are probably less biased than presolar grains isolated from meteorites. However, it is entirely possible that the typical interstellar dust particle is isotopically solar in composition. The Stardust collection of interstellar dust will be the first truly unbiased one.

Westphal, Andrew J.↗
NASA NTRS2015

The Compositional Evolution of C/2012 S1 (ISON) from Ground-Based High-Resolution Infrared Spectroscopy as Part of a Worldwide Observing Campaign

Volatile production rates, relative abundances, rotational temperatures, and spatial distributions in the coma were measured in C/2012 S1 (ISON) using long-slit high-dispersion (lambda/delta lambda approximately 2.5 times 10 (sup 4)) infrared spectroscopy as part of a worldwide observing campaign. Spectra were obtained on Universal Time 2013 October 26 and 28 with NIRSPEC (Near Infrared Spectrometer) at the W.M. Keck Observatory, and Universal Time 2013 November 19 and 20 with CSHELL (Cryogenic Echelle Spectrograph) at the NASA IRTF (Infrared Telescope Facility). H2O was detected on all dates, with production rates increasing markedly from (8.7 plus or minus 1.5) times 10 (sup 27) molecules per second on October 26 (Heliocentric Distance = 1.12 Astronomical Units) to (3.7 plus or minus 0.4) times 10 (sup 29) molecules per second on November 20 (Heliocentric Distance = 0.43 Astronomical Units). Short-term variability of H2O production is also seen as observations on November 19 show an increase in H2O production rate of nearly a factor of two over a period of about 6 hours. C2H6, CH3OH and CH4 abundances in ISON (International Scientific Optical Network) are slightly depleted relative to H2O when compared to mean values for comets measured at infrared wavelengths. On the November dates, C2H2, HCN and OCS abundances relative to H2O appear to be within the range of mean values, whereas H2CO and NH3 were significantly enhanced. There is evidence that the abundances with respect to H2O increased for some species but not others between October 28 (Heliocentric Distance = 1.07 Astronomical Units) and November 19 (Heliocentric Distance = 0.46 Astronomical Units). The high mixing ratios of H2CO to CH3OH and C2H2 to C2H6 on November 19, and changes in the mixing ratios of some species with respect to H2O between October 28 to November 19, indicates compositional changes that may be the result of a transition from sampling radiation-processed outer layers in this dynamically new comet to sampling more pristine natal material as the outer processed layer was increasingly eroded and the thermal wave propagated into the nucleus as the comet approached perihelion for the first time. On November 19 and 20, the spatial distribution for dust appears asymmetric and enhanced in the antisolar direction, whereas spatial distributions for volatiles (excepting CN) appear symmetric with their peaks slightly offset in the sunward direction compared to the dust. Spatial distributions for H2O, HCN, C2H6, C2H2, and H2CO on November 19 show no definitive evidence for significant contributions from extended sources; however, broader spatial distributions for NH3 and OCS may be consistent with extended sources for these species. Abundances of HCN and C2H2 on November 19 and 20 are insufficient to account for reported abundances of CN and C2 in ISON near this time. Differences in HCN and CN spatial distributions are also consistent with HCN as only a minor source of CN in ISON on November 19 as the spatial distribution of CN in the coma suggests a dominant distributed source that is correlated with dust and not volatile release. The spatial distributions for NH3 and NH2 are similar, suggesting that NH3 is the primary source of NH2 with no evidence of a significant dust source of NH2; however, the higher production rates derived for NH3 compared to NH2 on November 19 and 20 remain unexplained. This suggests a more complete analysis that treats NH2 as a distributed source and accounts for its emission mechanism is needed for future work.

Russo, N. Dello↗
NASA NTRS1993

Collecting cometary soil samples? Development of the ROSETTA sample acquisition system

In the reference scenario of the ROSETTA CNRS mission, the Sample Acquisition System is mounted on the Comet Lander. Its tasks are to acquire three kinds of cometary samples and to transfer them to the Earth Return Capsule. Operations are to be performed in vacuum and microgravity, on a probably rough and dusty surface, in a largely unknown material, at temperatures in the order of 100 K. The concept and operation of the Sample Acquisition System are presented. The design of the prototype corer and surface sampling tool, and of the equipment for testing them at cryogenic temperatures in ambient conditions and in vacuum in various materials representing cometary soil, are described. Results of recent preliminary tests performed in low temperature thermal vacuum in a cometary analog ice-dust mixture are provided.

Coste, P. A.↗
NASA NTRS2006

Optical Spectroscopy of Stardust Samples

The Stardust spacecraft collected dust samples of the Kuiper belt comet 81P Wild-2 in aerogel and returned them to Earth January 15, 2006. Preliminary examination (PE) of the collected dust includes teams focused on mineralogy, chemical composition, isotopic measurements, organic analysis, cratering and spectroscopic properties. The main PE science goals are to provide an initial characterization of the returned samples with an emphasis on the capture process and its effects on the samples, a comparison of Stardust samples to other meteoritic materials, and the abundance of presolar materials in the Stardust samples. The science objectives of the Spectroscopy team are to obtain spectroscopic data on Stardust particles through infrared (IR), UV/Vis and Raman measurements of particles in aerogel, extracted particles, keystones, and microtome thin sections. These data will be used to answer fundamental science questions about the nature of the samples, but will also serve as preliminary mineralogical data to guide follow-on measurements that will be performed in the other preliminary examination teams. The IR characteristics of Stardust particles are measured to determine: 1) the nature of the indigenous 3.4 micron organic feature, is it detected and can it be differentiated/deconvolved from the contaminated aerogel? How does it compare to features observed in interplanetary dust particles (IDPs) and to astronomical measurements of comets and interstellar dust? 2) the shape and fine structure within the 10 micron silicate feature. Overlap with the strong Si-O stretching vibration from the aerogel complicates this analysis, but we hope to determine if the feature is dominated by amorphous silicates such as those observed in IDPs and comets and whether or not crystalline silicates (e.g. olivine, pyroxene, clays) are present, 3) the presence of secondary (alteration) phases. Deep Impact results suggest that IR observations of Stardust particles should be evaluated for the presence of hydrated materials (water bands at 3 and 6 microns) and carbonates (6.8 microns and other resonances) and 4) the detection of crystalline features in the far-IR (20-100 microns) region where crystalline silicates and other minerals have strong bands that can be used both for phase analysis and phase chemistry. It has been demonstrated that these far-IR measurements can be obtained in situ on particles in aerogel keystones.

Keller, Lindsay P.↗
NASA NTRS1998

Aerothermal Effects of Cavities and Protuberances for High-Speed Sample Return Capsules

Extraterrestrial sample return is a growing component of solar system exploration. Currently, four missions, Stardust, 1 Muses-C, 2 Genesis, and Mars Sample Return, are under development that employ sample return as a prime component of the mission architecture. Respectively, these missions will return samples from the tail of a comet, an asteroid, the solar wind, and, Mars. An important component of these missions and the focus of this paper is the design of the sample return capsule (SRC). The purpose of the SRC is to safely return to Earth any gathered samples for terrestrial analysis. The two major design constraints for any SRC are as follows: 1) it must be able to survive a high-speed Earth entry (11 km/s to as a high as 15 km/s), 2) the mass of the SRC must be as small as possible. Because the SRC mass is carried from Earth to the sample sight and back, the SRC mass is a strong driver in the mission mass budget. Further, for the Mars Sample Return Capsule, planetary protection is another constraint. For this capsule, the probability of planetary contamination at Earth due to an SRC failure at entry must be minimal. For an SRC, a possible failure mechanism is severe local heating as a result of cavities and or protuberances in the SRC forebody heatshield. For example, the Apollo Command Module had a number of cavities and protuberances as part of the baseline designs Wind-tunnel tests of models containing small cavities and protuberances showed severe local heating augmentations in the vicinity of these surface discontinuities.4-5 As another example, the Genesis SRC forebody heat-shield contains penetrations (cavities) to mount the vehicle to the carrier bus. It is expected that these penetrations will also experience a severe local heating environment. A concern is that the large thermal gradients may produce sufficient thermal stress to cause local mechanical failure of the heatshield. Penetrations to the forebody heat-shield can also result from damage at vehicle integration, during launch, or during transportation of the sample return capsule from earth to the sample site and back. For example, the Starting SRC was damaged near the shoulder during the heatshield integration process producing a local surface discontinuity. Also, the Starting SRC traverses through the tail of a comet and is in space for 7 years. Thus, damage to the heatshield as a result of micrometeroid impact is a concern. Finally, it is difficult to characterize the effects of these potential heatshield singularities with ground-test facilities. Either detailed simulation or a dedicated flight test is required.

Olynick, David↗
NASA NTRS2018

Signatures of the Impact Histories of Comets and Asteroids within Shocked Phyllosilicates, Enstatite, and Forsterite Minerals

Throughout the lifetime of the solar system, collisions between small bodies and impacts on the surfaces of small bodies in the Kuiper Belt have occured at speeds of 1.5 - 3 km s-1 (Stern, Astron J 124, 2002), typically at 1-10 km s-1 between Trojan asteroids (Marzari et al. Icarus 119, 1996), and at ~4-8 km s-1 in the asteroid belt (Farinella and Davis, Icarus 97, 1992). Shock effects recorded by minerals composing these bodies are one observable legacy of this evolutionary process, whether they were generated through large collisions, micrometeoroid impacts, or processing during the formation of the solar system. Shock metamorphism has been observed in cometary samples such as those from Comet Wild 2 (Keller et al. Geochim. Cosmochim. Acta 72, 2008; Tomeoka et al. MAPS 43, 2008; Jacobs et al. MAPS 44, 2009) as well as in forsterites and enstatites found in meteorites (McCausland et al. AGU, 2010). To investigate the observable signatures of these processes, we have conducted a suite of impact experiments at NASA Johnson Space Center's Experimental Impact Laboratory (EIL). Target materials included Mg-rich forsterite (olivine), Mg-rich enstatite (orthopyroxene), and antigorite and lizardite (both in the serpentine group of phyllosilicates). Alumina-ceramic spheres were launched at speeds ranging from ~2.0 - 2.6 km s-1 into targets at temperatures from 25degC to -100degC. Recent advancements have been made in cooling targets in the EIL's vertical gun. Liquid nitrogen (LN2) is fed through a unique jacket surrounding the metallic sample container to chill the samples. Real-time values from temperature sensors attached to the sample holder are converted to target temperature through predetermined regression relationships, providing the target temperature at the time of impact with sub-degree accuracy. Fourier Transform Infrared Spectrometer (FTIR) data in the near to mid-IR will be presented, along with trends relating temperature and velocity with impact speeds, and thereby peak shock stresses experienced by the impacted minerals.

Lederer, Susan M.↗
NASA NTRS1989

Physical processing of cometary nuclei

Cometary nuclei were formed far from the Sun in the colder regions of the solar nebula, and have been stored in distant orbits in the Oort cloud over most of the history of the solar system. It had been thought that this benign environment would preserve comets in close to their original pristine state. However, recent studies have identified a number of physical processes that have likely acted to modify cometary nuclei in a variety of significant ways. It is important to consider all of these possible processes, both in deciding on a site on the nucleus for collection of cometary samples, and in interpreting the results of analyses of returned cometary samples. Although it can no longer be said that comets are pristine samples of original solar nebula material, they are still the best obtainable samples of that unique period in the formation of the planetary system.

Weissman, Paul R.↗
NASA NTRS2005

Measurement Protocols for In situ Analysis of Organic Compounds at Mars and Comets

The determination of the abundance and chemical and isotopic composition of organic molecules in comets and those that might be found in protected environments at Mars is a first step toward understanding prebiotic chemistries on these solar system bodies. While future sample return missions from Mars and comets will enable detailed chemical and isotopic analysis with a wide range of analytical techniques, precursor insitu investigations can complement these missions and facilitate the identification of optimal sites for sample return. Robust automated experiments that make efficient use of limited spacecraft power, mass, and data volume resources are required for use by insitu missions. Within these constraints we continue to explore a range of instrument techniques and measurement protocols that can maximize the return from such insitu investigations.

Mahaffy, P. R.↗
NASA NTRS2005

Measurement Protocols for In Situ Analysis of Organic Compounds at Mars and Comets

The determination of the abundance and chemical and isotopic composition of organic molecules in comets and those that might be found in protected environments at Mars is a first step toward understanding prebiotic chemistries on these solar system bodies. While future sample return missions from Mars and comets will enable detailed chemical and isotopic analysis with a wide range of analytical techniques, precursor insitu investigations can complement these missions and facilitate the identification of optimal sites for sample return. Robust automated experiments that make efficient use of limited spacecraft power, mass, and data volume resources are required for use by insitu missions. Within these constraints we continue to explore a range of instrument techniques and measurement protocols that can maximize the return from such insitu investigations.

Mahaffy, P. R.↗
NASA NTRSDate not supplied

Dust Composition of Comet 81P/Wild 2 From JWST Spectroscopy Compared to Stardust’s Fine-Grained Materials and Gems-Rich IDPS

The Stardust Mission returned samples from the coma of Jupiter Family comet 81P/Wild 2 for detailed laboratory analyses. Here we present and discuss the best-fit thermal dust model for the coma dust of comet 81P/Wild 2 as observed by JWST. Comet 81P was observed through JWST GO 018xx, using NIRSpec (2.9–5.3µm, λ/∆λ≈1000) and MRS IFU (4.9–28.1µm, λ/∆λ≈3000) on 2023-03-20 UT and 2023-03-24 UT, respectively, at a heliocentric distance of 1.85 au and JWST distance of 1.43 au (phase angle of 32 degrees). The dust coma of 81P as revealed by JWST offers a salient compliment to laboratory studies of Stardust samples that typically are bigger than 2 µm and up to 60 µm in size.

D H Wooden↗
NASA NTRS2002

Technology Development and Advanced Planning for Curation of Returned Mars Samples

NASA Johnson Space Center (JSC) curates extraterrestrial samples, providing the international science community with lunar rock and soil returned by the Apollo astronauts, meteorites collected in Antarctica, cosmic dust collected in the stratosphere, and hardware exposed to the space environment. Curation comprises initial characterization of new samples, preparation and allocation of samples for research, and clean, secure long-term storage. The foundations of this effort are the specialized cleanrooms (class 10 to 10,000) for each of the four types of materials, the supporting facilities, and the people, many of whom have been doing detailed work in clean environments for decades. JSC is also preparing to curate the next generation of extraterrestrial samples. These include samples collected from the solar wind, a comet, and an asteroid. Early planning and R\&D are underway to support post-mission sample handling and curation of samples returned from Mars. One of the strong scientific reasons for returning samples from Mars is to search for evidence of current or past life in the samples. Because of the remote possibility that the samples may contain life forms that are hazardous to the terrestrial biosphere, the National Research Council has recommended that all samples returned from Mars be kept under strict biological containment until tests show that they can safely be released to other laboratories. It is possible that Mars samples may contain only scarce or subtle traces of life or prebiotic chemistry that could readily be overwhelmed by terrestrial contamination . Thus, the facilities used to contain, process, and analyze samples from Mars must have a combination of high-level biocontainment and organic / inorganic chemical cleanliness that is unprecedented. JSC has been conducting feasibility studies and developing designs for a sample receiving facility that would offer biocontainment at least the equivalent of current maximum containment BSL-4 (BioSafety Level 4) laboratories, while simultaneously maintaining cleanliness levels equaling those of state-of-the-art cleanrooms. Unique requirements for the processing of Mars samples have inspired a program to develop handling techniques that are much more precise and reliable than the approach (currently used for lunar samples) of employing gloved human hands in nitrogen-filled gloveboxes. Individual samples from Mars are expected to be much smaller than lunar samples, the total mass of samples returned by each mission being 0.5- 1 kg, compared with many tens of kg of lunar samples returned by each of the six Apollo missions. Smaller samples require much more of the processing to be done under microscopic observation. In addition, the requirements for cleanliness and high-level containment would be difficult to satisfy while using traditional gloveboxes. JSC has constructed a laboratory to test concepts and technologies important to future sample curation. The Advanced Curation Laboratory includes a new-generation glovebox equipped with a robotic arm to evaluate the usability of robotic and teleoperated systems to perform curatorial tasks. The laboratory also contains equipment for precision cleaning and the measurement of trace organic contamination.

Lindstrom, David J.↗