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DOE OSTI2026

Isostructural electronic transition in MoS 2 probed by solid-state high-harmonic generation spectroscopy

Studying materials under extreme pressure in diamond anvil cells (DACs) is key to discovering emergent states of matter, yet no method currently allows the direct measurement of the electronic structure in this environment. Solid-state high-harmonic generation (sHHG) offers a unique all-optical window into the electronic structure of materials. We demonstrate sHHG spectroscopy inside a DAC by probing 2H-MoS 2 , up to 30 GPa, revealing a pressure-induced crossover of the lowest direct bandgap from the K-point to the Γ-point. This transition manifests as a sharp minimum in harmonic intensity and a 30° rotation of the sHHG polarization anisotropy, despite the absence of a structural phase change. First-principles simulations attribute these features to interference between competing excitation pathways at distinct points in the Brillouin zone. Our results establish sHHG as a sensitive probe of electronic transitions at high pressure, enabling access to quantum phenomena that evade detection by conventional techniques.

Nebgen, Bailey R. [University of California, Berke↗

NASA NTRS1973

Opportunities for space surveys of moisture anomalies

Review of a combination of infrared scanning, unsupervised spectroscopic classification, change detection, and perturbation spectroscopy for monitoring anomalous moisture exchange from space. Infrared sensors have been developed which can monitor the solar reflectance from droplet distributions in vegetation and clouds, the absorption of thermal radiation by water vapor, and the microwave attenuation by atmospheric water. Unsupervised spectroscopic classification techniques are emerging which have the potential to subdivide strip maps from infrared scanners into different moisture targets. Intersecting and parallel spacecraft orbits provide opportunities to study the change of recognized targets between two scans and to recognize anomalous moisture exchange from those changes which significantly exceed the statistical uncertainty of the spectroscopic target signature. The new concept of perturbation spectroscopy shows a potential to quantitatively determine the change of integrated water vapor pressure with a minimum of 'atmospheric truth' and with low spectroscopic resolution that is typical of simple interference filters.

Krause, F. R.↗

NASA NTRS1975

Transonic buffet behavior of Northrop F-5A aircraft

Flight tests were performed on an extensively instrumented F-5A aircraft to investigate the dynamic buffet pressure distribution on the wing surfaces and the responses during a series of transonic maneuvers called the windup turns. The maneuvers to maximum lift were performed at three Mach number-altitude combinations with a constant 'q' of approximately 14,360 N/sq m (300 psf). The fluctuating buffet pressure data at 24 stations on the right wing of the F-5A were acquired by miniaturized semiconductor type pressure transducers mounted on the wing. A new transducer mounting and wiring technique was applied where the interference with the natural flow condition was minimized. The data acquired in this manner were found adequate to trace the shock origin, the movement of the shock front and the development of the separated flow (shock induced or leading edge induced) on the wing surface.

Hwang, C.↗

NASA NTRS1989

A three-dimensional upwind finite element point implicit unstructured grid Euler solver

A three-dimensional upwind finite element technique that uses cell-centered quantities and implicit and/or explicit time marching was developed for computing hypersonic inviscid flows using adaptive unstructured grids. This technique was used to predict shock interference on a swept cylinder. An attempt was made to determine the flowfield and, in particular, the pressure augmentation caused by an impinging shock on the swept leading edge of a cowl lip of an engine inlet.

Thareja, Rajiv R.↗

NASA NTRS1988

Fore-and-aft stiffness and damping characteristics of 30 x 11.5-14.5, Type VIII, bias-ply and radial-belted aircraft tires

Measurements of footprint geometrical properties and fore and aft stiffness and damping characteristics were obtained on 30 x 11.5-14.5 bias-ply and radial-belted aircraft tires. Significant differences in stiffness and damping characteristics were found between the two design types. The results show that footprint aspect ratio effects may interfere with the improved hydroplaning potential associated with the radial-belted tire operating at higher inflation pressures.

Lopez, Mercedes C.↗

NASA NTRS1994

Computation of wind tunnel wall effects for complex models using a low-order panel method

A technique for determining wind tunnel wall effects for complex models using the low-order, three dimensional panel method PMARC (Panel Method Ames Research Center) has been developed. Initial validation of the technique was performed using lift-coefficient data in the linear lift range from tests of a large-scale STOVL fighter model in the National Full-Scale Aerodynamics Complex (NFAC) facility. The data from these tests served as an ideal database for validating the technique because the same model was tested in two wind tunnel test sections with widely different dimensions. The lift-coefficient data obtained for the same model configuration in the two test sections were different, indicating a significant influence of the presence of the tunnel walls and mounting hardware on the lift coefficient in at least one of the two test sections. The wind tunnel wall effects were computed using PMARC and then subtracted from the measured data to yield corrected lift-coefficient versus angle-of-attack curves. The corrected lift-coefficient curves from the two wind tunnel test sections matched very well. Detailed pressure distributions computed by PMARC on the wing lower surface helped identify the source of large strut interference effects in one of the wind tunnel test sections. Extension of the technique to analysis of wind tunnel wall effects on the lift coefficient in the nonlinear lift range and on drag coefficient will require the addition of boundary-layer and separated-flow models to PMARC.

Ashby, Dale L.↗

NASA NTRS1996

Baseline acoustic levels of the NASA Active Noise Control Fan rig

Extensive measurements of the spinning acoustic mode structure in the NASA 48 inch Active Noise Control Fan (ANCF) test rig have been taken. A continuously rotating microphone rake system with a least-squares data reduction technique was employed to measure these modes in the inlet and exhaust. Farfield directivity patterns in an anechoic environment were also measured at matched corrected rotor speeds. Several vane counts and spacings were tested over a range of rotor speeds. The Eversman finite element radiation code was run with the measured in-duct modes as input and the computed farfield results were compared to the experimentally measured directivity pattern. The experimental data show that inlet spinning mode measurements can be made very accurately. Exhaust mode measurements may have wake interference, but the least-squares reduction does a good job of rejecting the non-acoustic pressure. The Eversman radiation code accurately extrapolates the farfield levels and directivity pattern when all in-duct modes are included.

Sutliff, Daniel L.↗

NASA NTRS2002

Vapor transport growth of organic solids in microgravity and unit gravity: some comparisons and results to date

Thin films of an organic nonlinear optical (NLO) material, N, N-dimethyl-p-(2,2-dicyanovinyl) aniline (DCVA), have been grown in space and on the ground by physical vapor transport in an effusive ampoule arrangement. The thin film growth technique developed on the ground is a direct result of information gleaned from experiments in microgravity. This paper covers the results of our experimental investigations for establishing "ideal" terrestrial conditions for deposition of a DCVA film. The active control during the deposition process was exercised by three deposition variables: the material source temperature, the background pressure external to the growth ampoule and the substrate temperature. Successful growth occurred when the difference in temperature between the source material and the copper substrate was 14 degrees C and the background nitrogen pressure was such that the transport was either diffusive or convective. A qualitative diffusion limited boundary was estimated to occur at a pressure of approximately 20 torr. We have probed the DCVA thin films with visible-near infrared reflection absorption spectroscopy, polarized Fourier transform infrared spectrometry, differential interference contrast optical microscopy, and stylus profilometry.

short duration↗

NASA NTRS2001

Application of Pressure-Based Wall Correction Methods to Two NASA Langley Wind Tunnels

This paper is a description and status report on the implementation and application of the WICS wall interference method to the National Transonic Facility (NTF) and the 14 x 22-ft subsonic wind tunnel at the NASA Langley Research Center. The method calculates free-air corrections to the measured parameters and aerodynamic coefficients for full span and semispan models when the tunnels are in the solid-wall configuration. From a data quality point of view, these corrections remove predictable bias errors in the measurement due to the presence of the tunnel walls. At the NTF, the method is operational in the off-line and on-line modes, with three tests already computed for wall corrections. At the 14 x 22-ft tunnel, initial implementation has been done based on a test on a full span wing. This facility is currently scheduled for an upgrade to its wall pressure measurement system. With the addition of new wall orifices and other instrumentation upgrades, a significant improvement in the wall correction accuracy is expected.

Iyer, V.↗

NASA NTRS1978

Comparison of nozzle and afterbody surface pressures from wind tunnel and flight test of the YF-17 aircraft

Results are reported from the initial phase of an effort to provide an adequate technical capability to accurately predict the full scale, flight vehicle, nozzle-afterbody performance of future aircraft based on partial scale, wind tunnel testing. The primary emphasis of this initial effort is to assess the current capability and identify the cause of limitations on this capability. A direct comparison of surface pressure data is made between the results from an 0.1-scale model wind tunnel investigation and a full-scale flight test program to evaluate the current subscale testing techniques. These data were acquired at Mach numbers 0.6, 0.8, 0.9, 1.2, and 1.5 on four nozzle configurations at various vehicle pitch attitudes. Support system interference increments were also documented during the wind tunnel investigation. In general, the results presented indicate a good agreement in trend and level of the surface pressures when corrective increments are applied for known effects and surface differences between the two articles under investigation.

Lucas, E. J.↗

DOE OSTI2021

Design of Sample Holder for Plutonium Coupon Studies

In order to gain better understanding of the plutonium (Pu) corrosion behaviors and reaction kinetics, it is imperative that coupon experiments must be performed on well-defined surfaces. The reactions at the samples’ surfaces have to be properly monitored in terms of reactive gaseous pressures and temperatures. The pressure can be measured by using a pressure gauge, the temperature can be detected with calibrated thermal couples and/or pyrometric camera. These devices do not interfere with the chemistry of the surface reaction. However, to obtain information from the surface reaction, the aggressively machined edge and the back side of the Pu coupons need to be shielded from the applied gases. The coupons are typically made to 5/8 inch in diameter and 0.065 inch in thickness. To this end, a sample holder was designed which can seal the machined edge and the back side of coupons from the exposed gases, thus allowing proper surface reaction. The holder design was fabricated and had been tested with several coupon samples. We have achieved perfect sealing of the machined edge and the back side of the coupons, even when the coupons’ thicknesses are vastly different than the nominal thickness for which the sample holders were fabricated for. This write-up is to document the design of the holder and provide a description of the procedures to properly put the components together.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1981

Pressure-Reduction Technique for Crystal Growth

Large crystals grown by varying pressure rather than temperature. In constant temerature pressure-reduction process crystal growth promoted as solubility decreases by factor of more than 10. Technique used to study crystal growth kinetics by "pressure wave"" analog of conventional "thermal wave" experiments. Technique has advantages of faster response and freedom from convective interference.

Shlichta, P. J.↗

NASA NTRS1983

An experimental investigation of the subcritical and supercritical flow about a swept semispan wing

An experimental investigation of the turbulent, subcritical and supercritical flow over a swept, semispan wing in a solid wall wind tunnel is described. The program was conducted over a range of Mach numbers, Reynolds numbers, and angles of attack to provide a variety of test cases for assessment of wing computer codes and tunnel wall interference effects. Wing flows both without and with three dimensional flow separation are included. Data include mean surface pressures for both the wing and tunnel walls; surface oil flow patterns on the wing; and mean velocity, flow field surveys. The results are given in tabular form and presented graphically to illustrate some of the effects of the test parameters. Comparisons of the wing pressure data with the results from two inviscid wing codes are also shown to assess the importance of viscous flow and tunnel wall effects.

Lockman, W. K.↗

NASA NTRS1973

The effects on cruise drag of installing refan-engine nacelles on the McDonnell-Douglas DC-9

A high speed wind tunnel test has been conducted to determine the effect on cruise drag for installing larger JT8D Refan engine nacelles on the Douglas DC-9. Drag data and wing- and nacelle/pylon/fuselage-channel pressure data are presented. Reduced pylon spares, required to minimize effects of the nacelle installation on low-speed deep stall, were investigated. The reduce span pylons resulted in no adverse interference effects. At typical cruise Mach numbers the measured penalty for the Refan installation was less than estimated due to a favorable effect of the larger entering engine stream tube suppressing the wing upper-surface velocities with subsequent wing compressibility drag reduction. Channel pressures show no shock waves or boundary layer separations.

Callaghan, J. T.↗

NASA NTRS1996

Cryogenic Brush Seal Test Results

Brush seals are compliant, contact seals that have long-life, low-leakage characteristics desirable for use in rocket engine turbopumps. 50.8-mm (2.0 inch) diameter brush seals with a nominal initial radial interference of 0.127-mm (0.005 inch) were tested in liquid nitrogen at shaft speeds up to 35,000 rpm and differential pressure loads up to 1.21 MPa (175 psi) per brush. The measured leakage rate of a single brush was 2-3 times less than that measured for a 12-tooth, 0.127-mm (0.005 inch) radial clearance labyrinth seal used as a baseline. Stage effects were studied and it was found that two brush seals with a large separation distance leaked less than two brushes tightly packed together. The maximum measured groove depth on the Inconel 718 rotor was 25.4 (mu)m (0.001 inch) after 4.31 hours of shaft rotation. The Haynes-25 bristles wore approximately 25.4-76.2 (mu)m (0.001-0.003 inch) under the same conditions. Three seal runner coatings, chromium carbide, Teflon impregnated chromium, and zirconium oxide, were tested in liquid hydrogen at 35,000 and 65,000 rpm with separate 50.8 mm diameter brush seals made of Haynes-25 bristles and having a nominal initial radial interference of 129 rpm. Two bare Inconel-718 rotors were also tested as a baseline. The test results revealed significant differences between the wear characteristics of the uncoated and coated seal runners. At both speeds the brush seal with the bare Inconel-718 seal runner exhibited significant bristle wear with excessive material transferring to the runner surface. In contrast, the coated seal runners inhibited the transfer and deposit of bristle material. The chromium carbide coating showed only small quantities of bristle material transferring to its surface. The Teflon impregnated chromium coating also inhibited material transfer and provided some lubrication. This coating, however, is self-sacrificing. The Teflon remained present on the low speed runner, but it was completely removed from the high speed brush seal, which was tested considerably longer. The tests of the Teflon coating revealed the importance of using a lubricating and low friction coating for brush seals to reduce bristle and seal runner wear. The zirconium oxide coating exhibited the greatest amount of coating wear, while the brushes incurred only slight wear. Further testing of ceramics is recommended before making a final judgement on the viability of ceramic coatings for brush seals because of the contrast between the results reported by Carlile and the results presented herein. Strictly based on the results presented hereinabove, the chromium carbide and Teflon impregnated chromium coatings were considered preferable to the uncoated Inconel-718 and zirconium oxide coatings because of their good wear resistance and characteristics to inhibit bristle material wear and transfer to the seal runner.

Proctor, Margaret P.↗

NASA NTRS2005

Transferable Calibration Standard Developed for Quantitative Raman Scattering Diagnostics in High-Pressure Flames

Researchers from NASA Glenn Research Center s Combustion Branch and the Ohio Aerospace Institute (OAI) have developed a transferable calibration standard for an optical technique called spontaneous Raman scattering (SRS) in high-pressure flames. SRS is perhaps the only technique that provides spatially and temporally resolved, simultaneous multiscalar measurements in turbulent flames. Such measurements are critical for the validation of numerical models of combustion. This study has been a combined experimental and theoretical effort to develop a spectral calibration database for multiscalar diagnostics using SRS in high-pressure flames. However, in the past such measurements have used a one-of-a-kind experimental setup and a setup-dependent calibration procedure to empirically account for spectral interferences, or crosstalk, among the major species of interest. Such calibration procedures, being non-transferable, are prohibitively expensive to duplicate. A goal of this effort is to provide an SRS calibration database using transferable standards that can be implemented widely by other researchers for both atmospheric-pressure and high-pressure (less than 30 atm) SRS studies. A secondary goal of this effort is to provide quantitative multiscalar diagnostics in high pressure environments to validate computational combustion codes.

Nguyen, Quang-Viet↗

NASA NTRS1981

Thermal tides in the dusty martian atmosphere - A verification of theory

Major features of the daily surface pressure oscillations observed by the Viking landers during the two great dust storms on Mars in 1977 can be explained in terms of the classical atmospheric tidal theory developed for the earth's atmosphere. The most dramatic exception is the virtual disappearance of only the diurnal tide at Viking Lander 1 just before the second storm. This disappearance is attributed to destructive interference between the usually westward-traveling tide and an eastward-traveling diurnal Kelvin mode generated by orographically induced differential heating. The continuing Viking Lander 1 pressure measurements can be used with the model to monitor future great dust storms.

Zurek, R. W.↗

NASA NTRS1974

A note on the interference of two collinear cracks in a cylindrical shell

A simple interference problem in shells is evaluated and the results are compared with the obtained data for flat plates. A pressurized shallow cylindrical shell containing two collinear axial through cracks of equal lengths is investigated. It is found that as the size of the net ligament between the two cracks approaches zero, the stress intensity factors at the inner crack tips go to infinity, and the factors at the outer tips approach values that correspond to a single crack except that they are twice as long.

Erdogan, F.↗