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At least 343 records · Page 19

Reactive control and reasoning assistance for scientific laboratory instruments

Scientific laboratory instruments that are involved in chemical or physical sample identification frequently require substantial human preparation, attention, and interactive control during their operation. Successful real-time analysis of incoming data that supports such interactive control requires: (1) a clear recognition of variance of the data from expected results; and (2) rapid diagnosis of possible alternative hypotheses which might explain the variance. Such analysis then aids in decisions about modifying the experiment protocol, as well as being a goal itself. This paper reports on a collaborative project at the NASA Ames Research Center between artificial intelligence researchers and planetary microbial ecologists. Our team is currently engaged in developing software that autonomously controls science laboratory instruments and that provides data analysis of the real-time data in support of dynamic refinement of the experiment control. the first two instruments to which this technology has been applied are a differential thermal analyzer (DTA) and a gas chromatograph (GC). coupled together, they form a new geochemicstry and microbial analysis tool that is capable of rapid identification of the organiz and mineralogical constituents in soils. The thermal decomposition of the minerals and organics, and the attendance release of evolved gases, provides data about the structural and molecular chemistry of the soil samples.

Thompson, David E.↗

Magnetic Field Experiment Data Analysis System

The Johns Hopkins University Applied Physics Laboratory (JHU/APL) Magnetic Field Experiment Data Analysis System (MFEDAS) has been developed to process and analyze satellite magnetic field experiment data from the TRIAD, MAGSAT, AMPTE/CCE, Viking, Polar BEAR, DMSP, HILAT, UARS, and Freja satellites. The MFEDAS provides extensive data management and analysis capabilities. The system is based on standard data structures and a standard user interface. The MFEDAS has two major elements: (1) a set of satellite unique telemetry processing programs for uniform and rapid conversion of the raw data to a standard format and (2) the program Magplot which has file handling, data analysis, and data display sections. This system is an example of software reuse, allowing new data sets and software extensions to be added in a cost effective and timely manner. Future additions to the system will include the addition of standard format file import routines, modification of the display routines to use a commercial graphics package based on X-Window protocols, and a generic utility for telemetry data access and conversion.

Holland, D. B.↗

Rayleigh Scattering Measurements Using a Tunable Liquid Crystal Fabry-Perot Interferometer

Spectroscopic Rayleigh scattering is an established flow diagnostic that has the ability to provide simultaneous density, velocity, and temperature measurements. The Fabry-Perot interferometer or etalon is a commonly employed instrument for resolving the spectrum of molecular Rayleigh scattered light for the purpose of evaluating these flow properties. This paper investigates the use of a tunable liquid crystal (LC) Fabry-Perot etalon in Rayleigh scattering experiments at NASA Glenn Research Center. The LC etalon provides a robust interferometry system that can be tuned rapidly by adjusting the voltage applied to the liquid crystal interface. Tuning the interferometer is often necessary to control the physical locations of the concentric interference fringes when Rayleigh light is imaged through the LC etalon. The LC etalon diagnostic system was tested in a 1-cm diameter nozzle flow in two different scattering configurations to evaluate its usefulness for Rayleigh measurements compared to a traditional non-tunable fused silica Fabry-Perot etalon.

Mielke-Fagan, Amy F.↗

NASA’s Ground-Based Microgravity Simulation Facility

Since opportunities to conduct experiments in space are scarce, various microgravity simulators and analogs have been widely used in space biology ground studies. Even though microgravity simulators do not produce all of the biological effects observed in the true microgravity environment, they provide alternative test platforms that are effective, affordable, and readily available to facilitate microgravity research. The Microgravity Simulation Support Facility (MSSF) at the National Aeronautics and Space Administration (NASA) John F. Kennedy Space Center (KSC) has been established for conducting short duration experiments, typically less than 1 month, utilizing a variety of microgravity simulation devices for research at different gravity levels. The simulators include, but are not limited to, 2D Clinostats, 3D Clinostats, Random Positioning Machines, and Rotating Wall Vessels. In this presentation, we will provide an overview of current MSSF capabilities, research conducted in MSSF, new technology developments, customized sample holder designs, and the physical characteristics of these microgravity simulators.

Ye Zhang↗

Mars aqueous chemistry experiment

The Mars Aqueous Chemistry Experiment (MACE) is designed to conduct a variety of measurements on regolith samples, encompassing mineral phase analyses, chemical interactions with H2O, and physical properties determinations. From these data, much can be learned or inferred regarding the past weathering environment, the contemporaneous soil micro-environments, and the general chemical and physical state of the Martian regolith. By analyzing both soil and duricrust samples, the nature of the latter may become more apparent. Sites may be characterized for comparative purposes and criteria could be set for selection of high priority materials on future sample return missions. Progress for the first year MACE PIDDP is reported in two major areas of effort: (1) fluids handling concepts, definition, and breadboard fabrication and (2) aqueous chemistry ion sensing technology and test facility integration. A fluids handling breadboard was designed, fabricated, and tested at Mars ambient pressure. The breadboard allows fluid manipulation scenarios to be tested under the reduced pressure conditions expected in the Martian atmosphere in order to validate valve operations, orchestrate analysis sequences, investigate sealing integrity, and to demonstrate efficacy of the fluid handling concept. Additional fluid manipulation concepts have also been developed based on updated MESUR spacecraft definition. The Mars Aqueous Chemistry Experiment Ion Selective Electrode (ISE) facility was designed as a test bed to develop a multifunction interface for measurements of chemical ion concentrations in aqueous solution. The interface allows acquisition of real time data concerning the kinetics and heats of salt dissolution, and transient response to calibration and solubility events. An array of ion selective electrodes has been interfaced and preliminary calibration studies performed.

Clark, Benton C.↗

Forward production of protons in relativistic 12C-nucleus collisions

The production of protons in heavy ion collisions through the knockout mechanism (abrasion) is described using the Glauber model. The multiple knockouts from the projectile, including the inelastic collision series with the target, are considered using a closure approximation in treating energy conservation. Calculations for reactions of 12C projectiles with several targets at energies of 1 and 2A GeV arc compared to experiments. For large secondary proton momentum a strong dependence on the target mass is found and attributed to multiple scattering of the projectile knockouts.

NASA Discipline Radiation Health↗

Gamma-Ray Observatory - The next great observatory in space

The Gamma-Ray Observatory (GRO) which is part of NASA's Great Observatories space program is presented. The GRO is equipped with the Burst and Transient Source Experiment (which detects low-energy gamma-ray photons from 20 keV to 600 keV and locates sources of gamma-ray bursts), the Oriented Scintillation Spectrometer Experiment (which detects celestial gamma rays from 100 keV to 10 MeV and identifies the elements producing these rays by measuring the ray's spectra and time variability), the Imaging Compton Telescope (which images gamma rays with energies from 1 to 30 MeV created when cosmic rays interact with interstellar matter), and the Energetic Gamma-Ray Experiment Telescope (which detects high-energy photons associated with the most energetic processes occurring in nature). After the energies of photons from each source are classified, the gamma-ray mechanisms can be modelled. Nuclei, radioactive isotopes, and nuclear reactions can be identified, and the physical conditions at the radiation's source can also be modelled. From these models, theories can be developed about the creation of elements in the explosion and collapse of giant stars, the acceleration of charged particles to velocities approaching the speed of light, and the destruction of matter and antimatter.

Neal, Valerie↗

The Effect of Alloying on Topologically Close Packed Phase Instability in Advanced Nickel-Based Superalloy Rene N6

An investigation was conducted to describe topologically close packed (TCP) phase instability as a function of composition in the advanced Ni-base superalloy Rene N6. TCP phases are detrimental to overall high-temperature performance of Ni-base superalloys because of their brittle nature and because they deplete the Ni-rich matrix of potent solid solution strengthening elements. Thirty-four variations of polycrystalline Rene N6 determined from a design-of-experiments approach were cast and homogenized at 1315"C for 80 hours followed by exposure at 10930C for 400 hours to promote TCP formation. The alloys had the following composition ranges in atomic percent: Co 10.61 to 16.73%, Mo 0.32 to 1.34%, W 1.85 to 2.52%, Re 1.80 to 2.1 1 %, Ta 2.36 to 3.02%, Al 11.90 to 14.75%, and Cr 3.57 to 6.23%. Physical and chemical characteristics of all n-ticrostructures obtained were described using various analytical techniques. From these observations, a mathematical description of TCP occurrence (omega and P phase) was generated for polycrystalline Rene N6.

Ritzert, Frank↗

Experimental Study of Transitional Flow Behavior in a Simulated Low Pressure Turbine

A detailed investigation of the flow physics occurring on the suction side of a simulated Low Pressure Turbine (LPT) blade was performed. A contoured upper wall was designed to simulate the pressure distribution of an actual LPT airfoil onto a flat lower plate. The experiments were carried out for the Reynolds numbers of 35,000, 70,000, 100,000 and 250,000 with four levels of freestream turbulence ranging from 1% to 4%. For the three lower Reynolds numbers, the boundary layer on the flat plate was separated and formed a bubble. The size of laminar separation bubble was measured to be inversely proportional to the freestream turbulence levels and Reynolds numbers. However, no separation was observed for the Re = 250,000 case. The transition on a separated flow was found to proceed through the formation of turbulent spots in the free shear layer as evidenced in the intermittency profiles for Re = 35,000, 70,000 and 100,000. Spectral data show no evidence of Kelvin-Helmholtz or Tollmien-Schlichting instability waves in the free shear layer over a separation bubble (bypass transition). However, the flow visualization revealed the large vortex structures just outside of the bubble and their development to turbulent flow for Re = 50,000, which is similar to that in the free shear layer (separated-flow transition). Therefore, it is fair to say that the bypass and separated-flow transition modes coexist in the transitional flows over the separation bubble for certain conditions. Transition onset and end locations and length determined from intermittency profiles decrease as Reynolds number and freestream turbulence levels increase.

Sohn, Ki Hyeon↗

Particle Engulfment and Pushing by Solidifying Interfaces

The scientific objectives of the work on Particle Engulfment and Pushing by Solidifying Interfaces (PEP) include: (1) to enhance the fundamental understanding of the physics of interaction between inert particles and the solidification interface, and (2) to investigate aspects of melt processing of particulate metal matrix composites in the unique microgravity environment that will yield some vital information for terrestrial applications. The proposal itself calls for a long-term effort on the Space Station. This paper reports on ground experiments performed to date, as well as on the results obtained from two flight opportunities, the LMS mission (1996) and the USMP-4 mission (1997).

Stefanescu, Doru M.↗

Experimental Study of Transitional Flow Behavior in a Simulated Low Pressure Turbine

A detailed investigation of the flow physics occurring on the suction side of a simulated Low Pressure Turbine (LPT) blade was performed. A contoured upper wall was designed to simulate the pressure distribution of an actual LPT airfoil onto a flat lower plate. The experiments were carried out for the Reynolds numbers of 35,000, 70,000, 100,000, and 250,000 with four levels of freestream turbulence ranging from 1 to 4 percent. For the three lower Reynolds numbers, the boundary layer on the flat plate was separated and formed a bubble. The size of laminar separation bubble was measured to be inversely proportional to the freestream turbulence levels and Reynolds numbers. However, no separation was observed for the Re = 250,000 case. The transition on a separated flow was found to proceed through the formation of turbulent spots in the free shear layer as evidenced in the intermittency profiles for Re = 35,000, 70,000, and 100,000. Spectral data show no evidence of Kelvin-Helmholtz of Tollmien-Schlichting instability waves in the free shear layer over a separation bubble (bypass transition). However, the flow visualization revealed the large vortex structures just outside of the bubble and their development to turbulent flow for Re = 50,000, which is similar to that in the free shear layer (separated-flow transition). Therefore, it is fair to say that the bypass and separated-flow transition modes coexist in the transition flows over the separation bubble of certain conditions. Transition onset and end locations and length determined from intermittency profiles decreased as Reynolds number and freestream turbulence levels increase.

Sohn, Ki Hyeon↗

Experiments and Models for Polymeric Microsphere Foams

The current project was performed under the direction of Dr. Byron Pipes as its lead investigator from January 2001 to August 2004. With the permission of the NASA, the project was transferred to Dr. Thein Kyu as the principle investigator for the period of September 2004 - June 2005. There were two major thrust areas in the original proposal; (1) experimental characterization and kinematics of foam structure formation and (2) determination of the mechanical, physical, and thermal properties, although these thrust areas were further sub- divided into 7 tasks. The present project has been directed primarily to elucidate kinematics of micro-foam formation (tasks 1 and 3) and to characterize micro-foam structures, since the control of the micro-structure of these foams is of paramount importance in determining their physical, mechanical and thermal properties. The first thrust area was accomplished in a timely manner; however, the second thrust area of foam properties (tasks 2,4-7) has yet to be completed because the area of kinematics of foam structure formation turned out to be extremely complex and thus consumed more time than what have been anticipated. As will be reported in what follows, the present studies have greatly enhances the in-depth understanding of mechanisms and kinematics of the micro-foam formation from solid powders. However, in order to implement all objectives of the second thrust areas regarding investigations of mechanical, physical, and thermal properties and establishment of the correlation of structure - properties of the foams, the project needs additional time and resources. The technical highlights of the accomplishment are summarized as follows. The present study represents a first approach to understanding the complexities that act together in the powder foaming process to achieve the successful inflation of polyimide microstructures. This type of study is novel as no prior work had dissected the fundamentals that govern the inflation process in this type of systems. The systematic approach to each of the different phenomena (i.e. morphological, diffusive, kinetic and dynamic) brings into context each of them in a way that allows separate understanding and analysis. Of the different phenomena studied, probably the one that gives a higher level of control over the inflation process has been shown to be the morphological aspects of the precursor particles. It is a major contribution of the present work to isolate and identify this phenomenon and highlight the features that with careful control during the synthesis of the precursor material can lead to a highly optimized and specialized final product (neat foam or microstructure). Some of these accomplishments have been presented in various national meetings and some of which are either published in refereed journals or still in various stages of publications. One of the presentations was selected for "Best of ANTEC 2004" Online Presentation Series of the Society of Plastics Engineers (SPE) (September 2004)

Pipes, R. Byrona↗

Airborne simulation of Shuttle/Spacelab management and operation

The ASSESS (Airborne Science/Spacelab Experiments System Simulation) program is discussed. A simulated Spacelab operation was carried out aboard the CV-990 airborne laboratory at Ames Research Center. A scientific payload was selected to conduct studies in upper atmospheric physics and infrared astronomy with principal investigators from France, the Netherlands, England and the U.S. Two experiment operators (EOs) from the U.S. and two from Europe were trained to function as proxies for the principal investigators in operating, maintaining, and repairing the scientific instruments. The simulated mission, in which the EOs and a Mission Manager were confined to the aircraft and living quarters for a 1-week period while making scientific observations during nightly flights, provided experience in the overall management of a complex international payload, experiment preparation, testing, and integration, the training and selection of proxy operators, and data handling.

Mulholland, D. R.↗

Magnetospheric and interplanetary physics 1979-1982

Major trends in the study of magnetospheric and interplanetary physics during the 1979-1982 period are surveyed. Topics discussed include the exploration of the Saturnian and Jovian magnetospheres by Voyagers 1 and 2, the behavior of different ions in the earth magnetosphere, auroral kilometric radiation, computer modeling of global magnetospheric MHD flow, the magnetic substorm, the quiet state, the earth's bow shock, the heliospheric current sheet, and new techniques such as electron beam experiments, 'active' injection experiments, auroral radars, and observations of the earth's distant magnetic tail. The future of this area of research is seen in the combination of data from different spacecraft and ground observations in a single correlated data set, and in the consolidation of past gains by analysis of the large data backlog, while a small number of new missions goes forward.

Stern, D. P.↗

Atmospheric Trace Molecule Spectroscopy (ATMOS)

The Atmospheric Trace Molecule Spectroscopy (ATMOS) experiment is a space-borne investigation designed to obtain fundamental information related to the chemistry and physics of the earth's upper atmosphere (20 to 120 km altitude). The instrument, a high resolution (0.01/cm) interferometric spectrometer, measures the atmospheric absorption of solar radiation over the wavelength range from 2 to 16 micrometers, a spectral band which encompasses active transitions of all of the molecular species of current importance in upper atmospheric studies. There are two major aspects to the experiment: (1) the determination of the detailed compositional structure of the stratosphere and mesosphere, and its global, seasonal, and long-term variability; and (2) the study of the partitioning of absorbed solar energy at levels in the atmosphere characterized by dissociation of many of the constituents and by the breakdown of thermodynamic equilibrium. Characteristics of ATMOS are given. This experiment will be part of the atmospheric science research payload flown on the Atmospheric Laboratory for Applications and Science (ATLAS 1) NASA mission planned for late 1990.

Farmer, C. B.↗

STS-107 Microgravity Environment Summary Report

This summary report presents the results of the processed acceleration data measured aboard the Columbia orbiter during the STS-107 microgravity mission from January 16 to February 1, 2003. Two accelerometer systems were used to measure the acceleration levels due to vehicle and science operations activities that took place during the 16-day mission. Due to lack of precise timeline information regarding some payload's operations, not all of the activities were analyzed for this report. However, a general characterization of the microgravity environment of the Columbia Space Shuttle during the 16-day mission is presented followed by a more specific characterization of the environment for some designated payloads during their operations. Some specific quasi-steady and vibratory microgravity environment characterization analyses were performed for the following payloads: Structure of Flame Balls at Low Lewis-number-2, Laminar Soot Processes-2, Mechanics of Granular Materials-3 and Water Mist Fire-Suppression Experiment. The Physical Science Division of the National Aeronautics and Space Administration sponsors the Orbital Acceleration Research Experiment and the Space Acceleration Measurement System for Free Flyer to support microgravity science experiments, which require microgravity acceleration measurements. On January 16, 2003, both the Orbital Acceleration Research Experiment and the Space Acceleration Measurement System for Free Flyer accelerometer systems were launched on the Columbia Space Transportation System-107 from the Kennedy Space Center. The Orbital Acceleration Research Experiment supported science experiments requiring quasi-steady acceleration measurements, while the Space Acceleration Measurement System for Free Flyer unit supported experiments requiring vibratory acceleration measurement. The Columbia reduced gravity environment analysis presented in this report uses acceleration data collected by these two sets of accelerometer systems: The Orbital Acceleration Research Experiment is a low frequency sensor, which measures acceleration up to 1 Hz, but the 1 Hz acceleration data is trimmean filtered to yield much lower frequency acceleration data up to 0.01 Hz. This filtered data can be mapped to other locations for characterizing the quasi-steady environment for payloads and the vehicle. The Space Acceleration Measurement System for Free Flyer measures vibratory acceleration in the range of 0.01 to 200 Hz at multiple measurement locations. The vibratory acceleration data measured by this system is used to assess the local vibratory environment for payloads as well as to measure the disturbance causes by the vehicle systems, crew exercise devices and payloads operation disturbances. This summary report presents analysis of selected quasi-steady and vibratory activities measured by these two accelerometers during the Columbia 16-day microgravity mission from January 16 to February 1, 2003.

Jules, Kenol↗

The effects of energetic proton bombardment on polymeric materials: Experimental studies and degradation models

This report describes 3 MeV proton bombardment experiments on several polymeric materials of interest to NASA carried out on the Tandem Van De Graff Accelerator at the California Institute of Technology's Kellogg Radiation Laboratory. Model aromatic and aliphatic polymers such as poly(1-vinyl naphthalene) and poly(methyl methacrylate), as well as polymers for near term space applications such as Kapton, Epoxy and Polysulfone, have been included in this study. Chemical and physical characterization of the damage products have been carried out in order to develop a model of the interaction of these polymers with the incident proton beam. The proton bombardment methodology developed at the Jet Propulsion Laboratory and reported here is part of an ongoing study on the effects of space radiation on polymeric materials. The report is intended to provide an overview of the mechanistic, as well as the technical and experimental, issues involved in such work rather than to serve as an exhaustive description of all the results.

Coulter, D. R.↗

Evaluation of Factors Affecting Powdered Drug Reconstitution in Microgravity

Owing to the high cost of transporting mass into space, and the small volume available for equipment in the Space Shuttle Orbiter and the International Space Station, refrigeration space is extremely limited. For this reason, there exists strong motivation for transporting certain drugs in powdered form so that they do not require refrigeration. When needed, the powdered drug will be mixed with saline to obtain a liquid form that may be injected intravenously. While this is a relatively simple task in a 1-G environment, there are some difficulties that may be encountered in 0-G. In non-accelerated spaceflight, gravitational and inertial forces are eliminated allowing other smaller forces, such as capillary forces and surface tension, to dominate the behavior of fluids. For instance, water slowly ejected from a straw will tend to form a sphere, while fluid in a container will tend to wet the inside surface forming a highly rounded meniscus. Initial attempts at mixing powdered drugs with saline in microgravity have shown a tendency toward forming foamy emulsions instead of the desired homogeneous solution. The predominance of adhesive forces between the drug particles and the interface tensions at the gas/liquid and solid/liquid interfaces drastically reduce the rate of deaggregation of the drug powder and also reduce the rate of absorption of saline by the powder mass. In addition, the capillary forces cause the saline to wet the inside of the container, thus trapping air bubbles within the liquid. The rate of dissolution of a powder drug is directly proportional to the amount of surface area of the solid that is exposed to liquid solvent. The surface area of drug that is in contact with the liquid is greatly reduced in microgravity and, as a result, the dissolution rate is reduced as well. The KC-135 research described here was aimed at evaluating the extent to which it is possible to perform drug reconstitution in the weightlessness of parabolic flight using standard pharmacological supplies. The experiment included a parametric assessment of possible factors affecting the reconstitution process. The specific questions that we wished to answer were: (1) Is it possible to reconstitute powdered drugs in weightlessness using standard pharmacological equipment? (2) What are the differences between drug reconstitution in a 1-G and a 0-G environment? (3) What techniques of mixing the drug powder and diluent are more successful? (4) What physical and chemical factors play a role in determining the success of mixing and dissolution? (5) Is it necessary to employ crewmember and equipment restraints during the reconstitution process?

Schaffner, Grant↗