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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
NASA NTRS2001

Behavior of Three Metallic Alloys Under Combined Axial-Shear Stress at 650 C

Three materials, Inconel 718, Haynes 188, and 316 stainless steel, were tested under an axial-torsional stress state at 650 C. The objective of this study was to quantify the evolution of the material while in the viscoplastic domain. Initial and subsequent yield surfaces were experimentally determined to quantify hardening. Subsequent yield surfaces (yield surfaces taken after a preload) had a well-defined front side, in the prestrain direction, but a poorly defined back side, opposite the prestrain direction. Subsequent yield surfaces exhibited isotropic hardening by expansion of the yield surface, kinematic hardening by translation of the yield surface, and distortional hardening by flattening of the yield surface in the direction opposite to the last prestrain. An existing yield function capable of representing isotropic, kinematic, and distortional hardening was used to fit each yield surface. Four variables are used to describe each surface. These variables evolve as the material state changes and have been regressed to the yield surface data.

Colaiuta, Jason F.↗
NASA NTRS2003

Behavior of Three Metallic Alloys under Combined Axial-Shear Stresses at Elevated Temperature

Type 316 stainless steel, Haynes 188, and Inconel 718 samples were subjected to an axial-shear strain controlled loading history while the specimen temperature was held at 650 C to quantify the evolution of material state under a complex biaxial load path when the material is in the viscoplastic domain. Yield surfaces were constructed in the axial-shear stress plane using a sensitive, 30 x 10(exp -6)m/m, equivalent offset strain definition for the yield strain. Subsequent yield surfaces were constructed at various points along the strain path to define the material evolution. These subsequent yield surface translated, expanded, and distorted relative to the initial yield surface. Each of these very different materials exhibited components of isotropic, kinematic and distortional hardening. Furthermore, subsequent yield surfaces for each material have a very well defined front face and a poorly defined, flattened, back side.

Colaiuta, J. F.↗
DOE OSTI2017

Residual Stresses in SAVY 4000 and Hagan Container Bodies

Chloride-induced stress corrosion cracking (SCC) has been investigated as a potential failure mechanism for the SAVY 4000 and the Hagan containers used to store plutonium-bearing materials at Los Alamos National Laboratory. This report discusses the regions of the container bodies most susceptible to SCC and the magnitude of the residual stresses in those regions. Boiling MgCl2 testing indicated that for both containers the region near the top weld was most susceptible to SCC. The Hagan showed through wall cracking after 22-24 hours of exposure both parallel (axial stresses) and perpendicular (hoop stresses) to the weld. The SAVY 4000 container showed significant cracking above and below the weld after 47 hours of exposure but there was no visual evidence of a through wall crack and the cracks did not leak water. Two through wall holes formed in the bottom of the SAVY 4000 container after 44-46 hours of exposure. For both containers, average “through wall” residual stresses were determined from hole drilling data 4 mm below the weld. In the Hagan body, average tensile hoop stresses were 194 MPa and average compressive axial stresses were -120 MPa. In the SAVY 4000 body, average compressive hoop stresses were 11 MPa and average tensile axial stresses were 25 MPa. Results suggest that because the Hagan container exhibited through wall cracking in a shorter time in boiling MgCl2 and had the higher average tensile stress, 194 MPa hoop stress, it is more susceptible to SCC than the SAVY 4000 container.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2017

Overview of Alloy 617 Notched Specimen Testing

Prior to use in high temperature nuclear applications, Alloy 617, which is currently undergoing approval for inclusion in codes and regulations related to high temperature construction, must be approved by the Nuclear Regulatory Commission. Several concerns relating to the effects of geometric discontinuities, such as notches, and multi-axial stress states (as opposed to uniaxial stress states typically present in laboratory run creep tests) must first be addressed. This work has shown that at short time intervals (1000-2500 hours), 617 is notch strengthening and will fail preferentially at locations away from the notch, provided that diameters are similar (resulting in similar stresses). Additionally, specimens designed with semi-circular notches (or U-notches, as they are referred to in this report) to impose multi-axial stress states on the specimen during creep testing were found to either maintain similar creep rupture lives as uniaxial stress specimens tested at similar conditions, or have creep rupture lives that were significantly longer. This work, while not fully completed, shows that notches and multi-axial stress states do not appear to raise concerns with relation to the use of design rules created for Alloy 617 using smooth, straight gauge test specimens and uniaxial creep tests.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2018

Notch Effects on the Short Term Rupture Properties of Alloy 617 Base Metal and Weldments

Alloy 617 is currently undergoing approval for inclusion in the ASME Boiler and Pressure Vessel Code in Section III Division 5 for use in high temperature nuclear reactors. Prior to use in construction of these reactors, however, it must be approved by the Nuclear Regulatory Commission. Several concerns relating to the effects of geometric discontinuities, such as notches and multi-axial stress states (as opposed to uniaxial stress states typically present in laboratory run creep tests), must first be addressed. Alloy 617 has been found to be notch-strengthening in short term (1000-2500 hour) creep testing for both base metal and weld metal and will fail preferentially in a straight gauge section rather than at a sharp notch, provided that the applied stresses are similar in both the straight gauge and notch sections. Additionally, specimens designed with semi-circular notches (or U notches, as they are referred to in this report) to impose multi-axial stress states on the specimen during creep-testing were found to either maintain similar creep-rupture-lives as uniaxial stress specimens tested at similar conditions, or have creep-rupture-lives that were significantly longer. This work shows that notches and multi-axial stress states do not appear to raise concerns with relation to the use of design rules created for Alloy 617 using smooth, straight-gauge test specimens and uniaxial creep tests.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2020

Needle-Like Ferroelastic Domains in Individual Ferroelectric Nanoparticles

Superior structural, physical and electronic properties make ferroelectric nanocrystals essential in enabling a range of next-generation devices. Ferroelectric responses are determined by crystal structure and domain morphology. The ability to reversibly displace, create and annihilate elastic domains is critical to device applications. Whereas electric-field control has been demonstrated for ferroelectric 180° surface domain walls and vortices, similar control of ferroelastic domains and domain boundaries within individual nanocrystals remains challenging. Using controlled external compressive and tensile axial stress, deterministic and reversible control of highly mobile ferroelastic domains and axial polarization in three dimensions is demonstrated in this study. While many studies exist on ferroelastic domains in thin films and bulk, little is known about ferroelastic interactions at the single nanoparticle level, especially involving domain boundaries. Through combining Bragg coherent X-ray diffractive imaging and Landau theory, strain gradients in individual BaTiO3 nanocrystals are shown to stabilize needle-like ferroelastic twin domains. These domains are highly labile under applied axial stress, producing a locally enhanced electric polarization mediated by a ferroelectric phase transition. The efficacy of Bragg coherent X-ray diffractive imaging in studying in operando domains in three-dimensions is demonstrated, while synergy with theory provides a paradigm for domain boundary engineering and potential for nanoscale functional devices.

36 MATERIALS SCIENCE↗
NASA NTRS1988

Raman determination of layer stresses and strains for heterostructures and its application to the cubic SiC/Si system

A set of formulas for a generalized axial stress in diamond and zinc-blende semiconductors under axial stress is derived to calculate stress-related Raman shifts. By analyzing known Raman data on cubic SiC under hydrostatic pressures, one of the Raman-stress coefficients was obtained, and the existing elastic stiffness constants of cubic SiC were optimized. A method for calculating the stress and strain in SiC films on (100) Si is proposed. It is suggested that the stress and strain expressions and the method of the stress and strain determinations in heterostructures are quite general and may be used for other systems.

Feng, Z. C.↗
DOE OSTI2018

A Simplified Procedure to Determine Post-necking True Stress–Strain Curve from Uniaxial Tensile Test of Round Metallic Specimen Using DIC

Triaxial state of stress is usually generated in the necked zone because of neck geometry, and as a consequence proper correction of true tensile stress–strain curve after necking is mandatory. Various correction factors like Bridgman, Davidenkov and Spiridonova, Siebel and Schwaigere are available in the published literature to calculate true stress from mean axial stress. Similarly true strains can be calculated from the minimum diameters of the round specimen in the necked region for various true stress levels. But experimental determination of correction factors and minimum diameters of the round specimen in the necked region is a cumbersome task. This investigation shows a simplified procedure to determine true strains and the correction factors from digital image correlation-based local strain measurement in the necked region. The present procedure is validated by experimental results of rail steel.

36 MATERIALS SCIENCE↗
DOE OSTI2022

3D Simulations of gas injection on callovo-oxfordian claystone assuming spatial heterogeneity and anisotropy

A series of gas injection tests on Callovo-Oxfordian (COx) claystone from the Bure underground research laboratory (URL) in France were carried out at the British Geological Survey (BGS). The tests were performed using a triaxial apparatus specifically designed to capture small volumetric strains induced by the injected gas flow and consequent material dilatancy. The long-duration experiments were monitored throughout. Measurements also included pressure, stresses (axial and radial stresses prescribed for each test stage), rate of gas inflow, gas outflow volume as well as pore-pressures observed at various points of the sample. A coupled hydro-gas-mechanical 3D numerical model has been developed to simulate the tests. Initial permeability is assumed heterogeneous throughout the specimen and embedded fractures are incorporated in the formulation. Gas pressure-induced deformations during the test lead to variations of permeability due to changes in matrix porosity and, especially, fracture aperture as well as fracture orientation due to material anisotropy. A programme of sensitivity analyses involving the variation of different aspects and parameters of the model contributes to a better understanding of the phenomena and highlights its complexity. The model is able to reproduce the observed behaviour of the tests.

58 GEOSCIENCES↗
DOE OSTI2017

Experimental investigation of injection-induced fracturing during supercritical CO 2 sequestration

Leakage risk assessment is an inevitable procedure in permanent sequestration and storage of CO 2 in deep saline aquifers and depleted oil and gas reservoirs, where the integrity of caprock is most critical. Here, low porosity and low permeability concrete cubes were employed as caprock analogs to investigate the supercritical CO 2 injection-induced fracturing processes under true tri-axial stress conditions. A systematic experimental procedure, consisting of active acoustic emission measurement, pressure decay, injection pressure and temperature monitoring, fracture coloring, and gas fracturing, is formulated to qualitatively and quantitatively characterize the injection-induced fracturing processes and fracture morphology. Occurrence of injection-induced fracturing can be directly identified from peaks of borehole pressure profiles as well as sharp drops on temperature profiles due to CO 2 expansion, but generally there was no fracture propagation plateau appearing for the 20 cm rock cubes with zero pore pressure. Acoustic wave signatures, including both waveform change and arrival time delay, can effectively capture the extension of induced fractures inside the opaque rock. Initiation and propagation of supercritical CO 2 injection-induced fractures are highly dominated by the tri-axial stresses, following the general trend of continuum mechanics at high stress levels with large stress difference. As the stress difference decreases, induced fractures branch off in relatively arbitrary directions. For these supercritical CO 2 injection-induced fracturing experiments, poroelastic mechanics model makes a decent fit with the measured breakdown pressure of the caprock analogs. Findings in this study are valuable for risk analysis and operation optimization of geological CO 2 sequestration and storage as well as for CO 2 fracturing design and implementation in shale and tight reservoirs.

42 ENGINEERING↗
NASA NTRS1980

Influence of stress interaction on the behavior of off-axis unidirectional composites

The yield function for plane stress of a transversely isotropic composite lamina consisting of stiff, linearly elastic fibers and a von Mises matrix material is formulated in terms of Hill's elastic stress concentration factors and a single plastic constraint parameter. The above are subsequently evaluated on the basis of observed average lamina and constituent response for the Avco 5505 boron epoxy system. It is shown that inclusion of residual stresses in the yield function together with the incorporation of Dubey and Hillier's concept of generalized yield stress for anisotropic media in the constitutive equation correctly predicts the trends observed in experiments. The incorporation of the strong axial stress interaction necessary to predict the correct trends in the shear response is directly traced to the high residual axial stresses in the matrix induced during fabrication of the composite.

Pindera, M. J.↗
NASA NTRS1992

Thermal residual stresses in silicon-carbide/titanium (0/90) laminate

The current work formulated a micromechanical analysis of a cross-ply laminate and calculated the thermal residual stress in a very thick (0/90)(sub 2n) silicon-carbide/titanium laminate. Results were also shown for a unidirectional laminate of the same material. Discrete fiber-matrix models assuming a rectangular array of fibers with a fiber volume fraction of 32.5 percent and a three-dimensional, finite-element analysis were used. Significant differences in the trends and magnitudes for the fiber, matrix, and interface stresses were calculated for unidirectional and (0/90) models. Larger hoop stresses calculated for the (0/90) model indicate that it may be more susceptible to radial cracking when subjected to mechanical loading than the unidirectional model. The axial stresses in the matrix were calculated to be slightly larger for the (0/90) model. The compressive axial stresses in the fiber were significantly larger in the (0/90) model. The presence of the cross-ply in the (0/90) model reduced the constraint on the fiber, producing radial interface stresses that were less compressive, which could lead to earlier failure of the fiber-matrix interface.

Bigelow, C. A.↗
DOE OSTI2017

CO 2 injection-induced fracturing in naturally fractured shale rocks

In this study, Niobrara shale cubes of 20 cm from Colorado were employed to investigate gas and supercritical CO 2 injection-induced fracturing in naturally fractured caprocks of deep aquifers/depleted reservoirs and fractured shale reservoirs. Under tri-axial stresses, gas or supercritical CO 2 was injected into the center of the cubes to induce fracturing. Real-time pressure and temperature, acoustic wave, pressure decay, fracture coloring, and gas fracturing were used to characterize the fracturing process and fracture morphology. Without pore pressure, CO 2 injection-induced fracturing occurred and completed instantly, accompanied by an evident temperature drop. Strongly bonded fractures barely affected transverse fracture propagation, whereas weakly bonded or open fractures arrested the injected fluid first and then allowed it to generate new fractures perpendicular to the minimum horizontal stress. Breakdown pressures for cubes with preexisting fractures using gas and supercritical CO 2 are much lower than both poroelastic predictions and slick-water fracturing pressure, and some are even lower than the minimum horizontal stress. This is attributed to unconformable preexisting fractures and the low viscosity of CO 2 . Moreover, decreasing tri-axial stress levels and increasing stress differences tend to lower the breakdown pressure. In conclusion, this study is instructive for understanding and tackling geomechanical issues related to CO 2 geological storage and fracturing of shale reservoirs.

58 GEOSCIENCES↗
NASA NTRS1987

Damage growth in composite laminates with interleaves

The influence of placing interleaves between fiber reinforced plies in multilayered composite laminates is investigated. The geometry of the composite is idealized as two dimensional, isotropic, linearly elastic media made of a damaged layer bonded between two half planes and separated by thin interleaves of low extensional and shear moduli. The damage in the layer is taken in the form of a symmetric crack perpendicular to the interface and may extend up to the interface. The case of an H-shaped crack in the form of a broken layer with delamination along the interface is also analyzed. The interleaves are modeled as distributed shear and tension springs. Fourier integral transform techniques are used to develop solutions in terms of singular integral equations. An asymptotic analysis of the integral equations based on Muskhelishvili's techniques reveals logarithmically singular axial stresses in the half plane at the crack tips for the broken layer. For the H shaped crack, similar singularities are found to exist in the axial stresses at the interface crack tips in the layer and the half plane. The solution of the equations is found numerically for the stresses and displacements by using the Hadamard's concept of direct differentiation of Cauchy integrals as well as Gaussian integration techniques.

Goree, James G.↗
DOE OSTI2019

Experimental Studies of Anisotropy on Borehole Breakouts in Mancos Shale

Calculating the size and orientation of borehole breakouts is one of the key methods for determining the orientation and magnitudes of the in situ stresses in the subsurface. To better understand the effects of anisotropy on borehole breakouts, experiments were conducted on Mancos Shale, a finely laminated mudrock. A novel testing configuration was developed to conduct borehole breakout experiments in a standard triaxial vessel and load frame. Samples were prepared at three different orientations and deformed under 6.9 to 20.7 MPa confining pressure. The results show a variation of peak strength and breakout geometry depending on the lamination orientation. Samples deformed parallel to laminations failed at a higher maximum compressive stress than samples deformed perpendicular to laminations, which were stronger than inclined samples. These relationships are quantified by a cosine-based failure envelope. Observed breakout shapes in perpendicular samples are V-shaped and symmetric around the borehole, which advance as a series of fractures of increasing size into the sidewalls. In inclined samples, fractures form along weaker laminations planes and grow in an en echelon pattern towards the axial stress direction. In parallel samples, long fractures grow from the wellbore towards the axial stress direction. The observed geometries point to potential sources of error in calculating in situ stresses from borehole breakouts.

58 GEOSCIENCES↗
NASA NTRS1987

Thermally induced stresses and deformations in angle-ply composite tubes

Cure-induced uniform temperature change effects on the stresses, axial expansion, and thermally-induced twist of four specific angle-ply tube designs are discussed with a view to the tubes' use as major space structure components. The stresses and deformations in the tubes are studied as a function of the four designs, the off-axis angle, and the single-material and hybrid reinforcing-material construction used. It is found that tube design has a minor influence on the stresses, axial stiffness, and axial thermal expansion characteristics, which are more directly a function of off-axis angle and material selection; tube design is, however, the primary influence in the definition of thermally-induced twist and torsional stiffness characteristics. None of the designs is free of thermally induced twist.

Hyer, M. W.↗
NASA NTRS2006

Compressive Failure of Fiber Composites under Multi-Axial Loading

This paper examines the compressive strength of a fiber reinforced lamina under multi-axial stress states. An equilibrium analysis is carried out in which a kinked band of rotated fibers, described by two angles, is sandwiched between two regions in which the fibers are nominally straight. Proportional multi-axial stress states are examined. The analysis includes the possibility of bifurcation from the current equilibrium state. The compressive strength of the lamina is contingent upon either attaining a load maximum in the equilibrium response or satisfaction of a bifurcation condition, whichever occurs first. The results show that for uniaxial loading a non-zero kink band angle beta produces the minimum limit load. For multi-axial loading, different proportional loading paths show regimes of bifurcation dominated and limit load dominated behavior. The present results are able to capture the beneficial effect of transverse compression in raising the composite compressive strength as observed in experiments.

Basu, Shiladitya↗