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NASA NTRS1999

The Return of Astromaterials to Earth Over the Next Decade

We are entering a new and golden age of sample return missions. In the coming decade we will harvest samples from Comet P/Wild II and interstellar dust courtesy of the STARDUST Mission (Brownlee et al., 1997), an asteroid (probably 4660 Nereus or 1989ML) by the ISAS MUSES-C Mission (ISAS, 1997), and solar wind by the Genesis Mission. A sample return from Mars is also envisioned as early as 2008, and possibly one from the two moons of Mars. It is, however, sobering to realize that MUSES-C aims to return 3-10 g of sample, STARDUST will provide micrograms of comet and interstellar dust, and Genesis will harvest only few micrograms of atoms. The diminutive size of the returning samples may be a source of concern for petrologists used only to looking at hefty lunar rocks and meteorites. How much sample is really needed to achieve prime science objectives, while maintaining a cost effective mission? The range of geological processes that we will want to address with these samples is staggering, encompassing not merely the entire history of the Solar system, but the history of the elements themselves. The interstellar processes include element formation, production and interactions with radiation, formation of organics, grain condensation and evolution, and interactions with magnetic fields. In the pre-accretionary (nebular) environment we wish to understand grain condensation, evaporation and recondensation, shock, radiation processing, solar energetic particle implantation, gas composition, the magnetic environment, and the evolution of organics. Finally, for solid bodies we wish to examine accretion history, shock, brecciation, impact gardening, metamorphism, aqueous alteration, weathering, exposure history, volcanism, fumarolic activity, differentiation, the magnetic environment, atmosphere evolution, and the evolution of organics. Since 1981, NASA has supported asteroid and comet science by collecting dust grains from these bodies in the stratosphere, and making them available for analysis in laboratories worldwide (Warren and Zolensky, 1994). Over the succeeding 17 years, many new techniques have been developed for these painstaking analyses, by at least 24 different laboratories across the globe. Despite the fact that the particle supply has always exceeded the demand, the painstaking efforts required for most of the nano-scale analyses have resulted in only 1520 grains having been analyzed, with a total mass of only 0.52 micrograms. Thus we really require less sample for analysis than one might imagine.

Zolensky, Michael E.↗
NASA NTRS1999

Entry Dispersion Analysis for the Genesis Sample Return Capsule

Genesis will be the first mission to return samples from beyond the Earth-Moon system. The spacecraft will be inserted into a halo orbit about the L1 (Sun- Earth) libration point where it will remain for two years collecting solar wind particles. Upon Earth return, the sample return capsule, which is passively controlled, will descend under parachute to Utah. The present study describes the analysis of the entry, descent, and landing scenario of the returning sample capsule. The robustness of the entry sequence is assessed through a Monte Carlo dispersion analysis where the impact of off-nominal conditions is ascertained. The dispersion results indicate that the capsule attitude excursions near peak heating and drogue chute deployment are within Genesis mission limits. Additionally, the size of the resulting 3-sigma landing ellipse is 47.8 km in downrange by 15.2 km in crossrange, which is within the Utah Test and Training Range boundaries.

Desai, Prasun N.↗
NASA NTRS2005

Entry Dispersion Analysis for the Genesis Sample Return Capsule

Genesis will be the first mission to return samples from beyond the Earth-Moon system. The spacecraft will be inserted into a halo orbit about the L1 (Sun-Earth) libration point where it will remain for two years collecting solar wind particles. Upon Earth return, the sample return capsule, which is passively controlled, will descend under parachute to Utah. The present study describes the analysis of the entry, descent, and landing scenario of the returning sample capsule. The robustness of the entry sequence is assessed through a Monte Carlo dispersion analysis where the impact of off-nominal conditions is ascertained. The dispersion results indicate that the capsule attitude excursions near peak heating and drogue chute deployment are within Genesis mission limits. Additionally, the size of the resulting 3-sigma landing ellipse is 47.8 km in downrange by 15.2 km in crossrange, which is within the Utah Test and Training Range boundaries.

Desai, Prasun N.↗
NASA NTRS1999

Entry Dispersion Analysis for the Genesis Sample Return Capsule

Genesis will be the first mission to return samples from beyond the Earth-Moon system. The spacecraft will be inserted into a halo orbit about the L1 (Sun- Earth) libration point where it will remain for two years collecting solar wind particles. Upon Earth return, the sample return capsule, which is passively controlled, will descend under parachute to Utah. The present study describes the analysis of the entry, descent, and landing scenario of the returning sample cap- sule. The robustness of the entry sequence is assessed through a Monte Carlo dispersion analysis where the impact of off-nominal conditions is ascertained. The dispersion results indicate that the capsule attitude excursions near peak heating and drogue chute deployment are within Genesis mission limits. Additionally, the size of the resulting 3-sigma landing ellipse is 47.8 km in downrange by 15.2 km in crossrange, which is within the Utah Test and Training Range boundaries.

Desai, Prasun, N.↗
NASA NTRS2010

Sample Return: What Happens to the Samples on Earth?

As space agencies throughout the world turn their attention toward human exploration of the Moon, Mars, and the solar system beyond, there has been an increase in the number of robotic sample return missions proposed as precursors to these human endeavors. In reality, however, we, as a global community, have very little experience with robotic sample return missions: 3 of the Russian Luna Missions successfully returned lunar material in the 1970s; 28 years later, in 2004, NASA s Genesis Mission returned material from the solar wind; and in 2006, NASA s Stardust Mission returned material from the Comet Wild2. [Note: The Japanese Hyabusa mission continues in space with the hope of returning material from the asteroid 25143 Itokawa.] We launch many spacecraft to LEO and return them to Earth. We also launch spacecraft beyond LEO to explore the planets, our solar system, and beyond. Some even land on these bodies. But these do not return. So as we begin to contemplate the sample return missions of the future, some common questions arise: "What really happens when the capsule returns?" "Where does it land?" "Who retrieves it and just how do they do that?" "Where does it go after that?" "How do the scientists get the samples?" "Do they keep them?" "Who is in charge?" The questions are nearly endless. The goal of this paper/presentation is to uncover many of the mysteries of the post-return phase of a mission - from the time the return body enters the atmosphere until the mission ends and the samples become part of a long term collection. The discussion will be based largely on the author s own experience with both the Genesis and Stardust missions. Of course, these two missions have a great deal in common, being funded by the same NASA Program (Discovery) and having similar team composition. The intent, however, is to use these missions as examples in order to highlight the general requirements and the challenges in defining and meeting those requirements for the final phase of sample return missions. The choices made by the Genesis and Stardust teams regarding recovery and sample handling will be discussed. These will be compared with the handling of returned lunar samples and the proposed handling of the Hyabusa samples as well. Finally, though none of these recent missions have been restricted within NASA s Planetary Protection Protocol, this is likely to change as missions venture farther from Earth. The implementation of Planetary Protection requirements will vary significantly based on mission scenario, however some of the potential implications of restricted Earth return will be considered.

McNamara, Karen↗
NASA NTRS2011

Sample Return Missions Where Contamination Issues are Critical: Genesis Mission Approach

The Genesis Mission, sought the challenging analytical goals of accurately and precisely measuring the elemental and isotopic composition of the Sun to levels useful for planetary science, requiring sensitivities of ppm to ppt in the outer 100 nm of collector materials. Analytical capabilities were further challenged when the hard landing in 2004 broke open the canister containing the super-clean collectors. Genesis illustrates that returned samples allow flexibility and creativity to recover from setbacks.

Allton, Judith H.↗
NASA NTRS2013

Plan for Subdividing Genesis Mission Diamond-on-Silicon 60000 Solar Wind Collector

NASA's Genesis solar wind sample return mission experienced an off nominal landing resulting in broken, albeit useful collectors. Sample 60000 from the collector is comprised of diamond-like-carbon film on a float zone (FZ) silicon wafer substrate Diamond-on-Silicon (DOS), and is highly prized for its higher concentration of solar wind (SW) atoms. A team of scientist at the Johnson Space Center was charged with determining the best, nondestructive and noncontaminating method to subdivide the specimen that would result in a 1 sq. cm subsample for allocation and analysis. Previous work included imaging of the SW side of 60000, identifying the crystallographic orientation of adjacent fragments, and devising an initial cutting plan.

Burkett, Patti J.↗
NASA NTRS2005

Genesis: Removing Contamination from Sample Collectors

The Genesis mission returned to Earth on September 8, 2004, experiencing a non-nominal reentry. The parachutes which were supposed to slow and stabilize the capsule throughout the return failed to deploy, causing the capsule to impact the desert floor at a speed of nearly 200 MPH. Both the science canister and the major components of the SRC were returned before nightfall on September 8 to the prestaged cleanroom at UTTR , avoiding prolonged exposure or pending weather changes which might further contaminate the samples. The majority of the contaminants introduced as a result of the anomalous landing were in the form of particulates, including UTTR dust and soil, carbon-carbon heat shield material, and shattered collector dust (primarily silicon and germanium). Additional information is included in the original extended abstract.

Lauer, H. V.↗
NASA NTRSDate not supplied

Genesis Solar Wind Sample Curation Documentation

Introduction: A scientist with experience as a sample science analyst, provider of flight hardware for multiple missions, and senior engineer in an ISO 2000-rated manufacturing plant has described the timeline of key participants in any PI-led sample return mission, the breadth of the organizations involved [1,2], and, of interest to this meeting, choosing the types of data to preserve and issues of future data accessibility. This work broadens that perspective by giving similar lessons from Genesis sample curation point-of-view. Curation participation regarding data gathering was part of the mission review process from the beginning. Genesis’ story illustrates outcome of several choices about types of data to record and preserve. Precision analysis of solar wind atoms captured in pure, ultraclean substrates is the driving science goal; therefore, detailed documentation was captured from all mission and curation phases and from investigator laboratories because these processes affect the final analytical results [3]. Pre-flight: Design and fabrication of the spacecraft. Like many modern small sample return missions, Genesis was a tightly managed team integrated across science, engineering and curation. Communication across the team was excellent, and, for the most part, the hands-on engineering technicians understood the impacts of “small choices” they routinely make, and the eyes-on oversight of manufacturing processes by scientists was mindful of details. The payload was designed by the Jet Propulsion Laboratory and the spacecraft by Lockheed Martin. Solar wind collectors and instruments were fabricated by multiple vendors and laboratories. The main portion of the payload was assembled at JSC. Fabrication procedures and contamination-control data (with witness coupons) were stored primarily at JSC. The original composition, dimensions and configuration of components, results of thermal testing, etc. are still needed for interpretation of analytical data. At times, these must be estimated from secondary information acquired pre-flight. Moreover, some files (e.g., original 3-D models and early Powerpoint) cannot be opened using software. Archived curation data includes 2-D drawings, material usage lists, QA documentation and analyses of consumables used during fabrication. Important chemical information still resides in archived hardware, paints and lubricants, material coupons, cleaning coupons, environmental witness plates and reference materials from manufacturing facilities. Purity and cleanliness of collector substrates. Semi-conductor vendors provided surface cleanliness data and some purity data. Purity for specific elements of interest was verified by science team members in their laboratories [4]. Curation archived procurement and shipping records, analysis reports, and non-proprietary fabrication data. A physical archive of flight collector reference materials is maintained for future use so additional data can be collected as analytical techniques improve. These are of increased value due to the hard landing upon re-entry. Cleaning and cleanliness assessments of flight hardware. Cleaning of the science canister payload was performed at JSC in a dedicated ISO 4 cleanroom using ultrapure water (UPW). The cleanliness of this UPW was monitored throughout processing. The archive for the clean lab also includes airborne particle counts, airborne molecular and inorganic contamination measurements as well as cleanroom construction material coupons and witness coupons. Hardware cleanliness was assessed by particle counts in rinse water batches. This information is recorded in batch cleaning forms and logbooks, and are, perhaps, of decreased value due to the hard landing. Post-flight: Curation-generated data. The curation handling history of each Genesis sample is documented in a typical astromaterials sample database which captures sample location, physical description and characterization data. Samples have a “shelf life”. Crucial to the preservation of samples is ongoing documentation of the sample environment, initially under curatorial control but is now a separate facility function with requires coordination. PI-generated data. Data on sample characterization and cleaning techniques continues to be generated by sample users [5]. These are often captured in LPSC abstracts, but these “engineering” results often are not publishable as stand-alone papers. We are actively looking for ways to make this information more accessible to users. Ion implants into samples have aided science return and can be shared among investigators. These (and similar) materials should be added to the curatorial collection with appropriate process and characterization data generated externally. Summary: Complete data archives for returned astromaterial samples must be broad in types and formats, and inclusive of environmental monitoring.

Genesis↗
NASA NTRS2017

NASA Sample Return Missions: Recovery Operations

The Utah Test and Training Range (UTTR), southwest of Salt Lake City, Utah, is the site of all NASA unmanned sample return missions. To date these missions include the Genesis solar wind samples (2004) and Stardust cometary and interstellar dust samples (2006). NASA’s OSIRIS-REx Mission will return its first asteroid sample at UTTR in 2023.

Pace, L. F.↗
NASA NTRS2003

Future Mission Proposal Opportunities: Discovery, New Frontiers, and Project Prometheus

The NASA Office of Space Science is expanding opportunities to propose missions to comets, asteroids, and other solar system targets. The Discovery Program continues to be popular, with two sample return missions, Stardust and Genesis, currently in operation. The New Frontiers Program, a new proposal opportunity modeled on the successful Discovery Program, begins this year with the release of its first Announcement of Opportunity. Project Prometheus, a program to develop nuclear electric power and propulsion technology intended to enable a new class of high-power, high-capability investigations, is a third opportunity to propose solar system exploration. All three classes of mission include a commitment to provide data to the Planetary Data System, any samples to the NASA Curatorial Facility at Johnson Space Center, and programs for education and public outreach.

Niebur, S. M.↗
NASA NTRS2016

Cleaning Genesis Sample Return Canister for Flight: Lessons for Planetary Sample Return

Sample return missions require chemical contamination to be minimized and potential sources of contamination to be documented and preserved for future use. Genesis focused on and successfully accomplished the following: - Early involvement provided input to mission design: a) cleanable materials and cleanable design; b) mission operation parameters to minimize contamination during flight. - Established contamination control authority at a high level and developed knowledge and respect for contamination control across all institutions at the working level. - Provided state-of-the-art spacecraft assembly cleanroom facilities for science canister assembly and function testing. Both particulate and airborne molecular contamination was minimized. - Using ultrapure water, cleaned spacecraft components to a very high level. Stainless steel components were cleaned to carbon monolayer levels (10 (sup 15) carbon atoms per square centimeter). - Established long-term curation facility Lessons learned and areas for improvement, include: - Bare aluminum is not a cleanable surface and should not be used for components requiring extreme levels of cleanliness. The problem is formation of oxides during rigorous cleaning. - Representative coupons of relevant spacecraft components (cut from the same block at the same time with identical surface finish and cleaning history) should be acquired, documented and preserved. Genesis experience suggests that creation of these coupons would be facilitated by specification on the engineering component drawings. - Component handling history is critical for interpretation of analytical results on returned samples. This set of relevant documents is not the same as typical documentation for one-way missions and does include data from several institutions, which need to be unified. Dedicated resources need to be provided for acquiring and archiving appropriate documents in one location with easy access for decades. - Dedicated, knowledgeable contamination control oversight should be provided at sites of fabrication and integration. Numerous excellent Genesis chemists and analytical facilities participated in the contamination oversight; however, additional oversight at fabrication sites would have been helpful.

Allton, J. H.↗
NASA NTRS2005

Genesis Recovery Processing

The Genesis spacecraft, launched in August 2001 to collect samples of the solar wind, returned to Earth on 8 September 2004. The Sample Return Capsule (SRC) failed to deploy its drogue parachute and parafoil and subsequently impacted the Utah Test and Training Range (UTTR) at an estimated 310 kph (193 mph). The goal of the Genesis mission to collect and return samples of the solar wind for precise elemental and isotopic analysis provides the scientific community with a unique set of materials to aid in understanding the origin of our solar system. The spacecraft orbited the Earth-Sun L1 point for 29 months exposing a suite of fifteen types of ultrapure, ultraclean materials in several different locations. Most of the materials were mounted on fixed or deployable wafer panels called collector arrays . A few materials were mounted as targets in the focal spot of an electrostatic mirror (the concentrator ). Other materials were strategically placed to maximize the area for solar-wind collection.

Stansbery, E. K.↗
NASA NTRS2013

Genesis Ultrapure Water Megasonic Wafer Spin Cleaner

A device removes, with high precision, the majority of surface particle contamination greater than 1-micron-diameter in size from ultrapure semiconductor wafer materials containing implanted solar wind samples returned by NASA's Genesis mission. This cleaning device uses a 1.5-liter/minute flowing stream of heated ultrapure water (UPW) with 1- MHz oscillating megasonic pulse energy focused at 3 to 5 mm away from the wafer surface spinning at 1,000 to 10,000 RPM, depending on sample size. The surface particle contamination is removed by three processes: flowing UPW, megasonic cavitations, and centripetal force from the spinning wafer. The device can also dry the wafer fragment after UPW/megasonic cleaning by continuing to spin the wafer in the cleaning chamber, which is purged with flowing ultrapure nitrogen gas at 65 psi (.448 kPa). The cleaner also uses three types of vacuum chucks that can accommodate all Genesis-flown array fragments in any dimensional shape between 3 and 100 mm in diameter. A sample vacuum chuck, and the manufactured UPW/megasonic nozzle holder, replace the human deficiencies by maintaining a consistent distance between the nozzle and wafer surface as well as allowing for longer cleaning time. The 3- to 5-mm critical distance is important for the ability to remove particles by megasonic cavitations. The increased UPW sonication time and exposure to heated UPW improve the removal of 1- to 5-micron-sized particles.

Allton, Judith H.↗
NASA NTRS2002

The Genesis Mission: Contamination Control and Curation

The Genesis mission, launched in August 2001, is collecting samples of the solar wind and will return to Earth in 2004. Genesis can be viewed as the most fundamental of NASA's sample return missions because it is expected to provide insight into the initial elemental and isotopic composition of the solar nebula from which all other planetary objects formed. The data from this mission will have a large impact on understanding the origins and diversity of planetary materials. The collectors consist of clean, pure materials into which the solar wind will imbed. Science and engineering issues such as bulk purity, cleanliness, retention of solar wind, and ability to withstand launch and entry drove material choices. Most of the collector materials are installed on array frames that are deployed from a clean science canister. Two of the arrays are continuously exposed for collecting the bulk solar wind; the other three are only exposed during specific solar wind regimes as measured by ion and electron monitors. Other materials are housed as targets at the focal point of an electrostatic mirror, or "concentrator", designed to enhance the flux of specific solar wind species. Johnson Space Center (JSC) has two principal responsibilities for the Genesis mission: contamination control and curation. Precise and accurate measurements of the composition of the solar atoms require that the collector materials be extremely clean and well characterized before launch and during the mission. Early involvement of JSC curation personnel in concept development resulted in a mission designed to minimize contaminants from the spacecraft and operations. A major goal of the Genesis mission is to provide a reservoir of materials for the 21 51 century. When the collector materials are returned to Earth, they must be handled in a clean manner and their condition well documented. Information gained in preliminary examination of the arrays and detailed surveys of each collector will be used to guide sample allocations to the scientific community. Samples allocated for analysis are likely to be small sections of individual collectors, therefore subdividing the materials must take place in a clean, well characterized way. A major focus of current research at JSC includes identifying and characterizing the contamination, waste, and alteration of the sample when using different subdividing, transport, and storage techniques and developing protocols for reducing their impact on the scientific integrity of the mission.

Stansbery, E. K.↗
NASA NTRS2011

Airborne Observation of the Hayabusa Sample Return Capsule Re-Entry

NASA Ames Research Center and the SETI Institute collaborated on an effort to observe the Earth re-entry of the Japan Aerospace Exploration Agency's Hayabusa sample return capsule. Hayabusa was an asteroid exploration mission that retrieved a sample from the near-Earth asteroid Itokawa. Its sample return capsule re-entered over the Woomera Prohibited Area in southern Australia on June 13, 2010. Being only the third sample return mission following NASA's Genesis and Stardust missions, Hayabusa's return was a rare opportunity to collect aerothermal data from an atmospheric entry capsule returning at superorbital speeds. NASA deployed its DC-8 airborne laboratory and a team of international researchers to Australia for the re-entry. For approximately 70 seconds, spectroscopic and radiometric imaging instruments acquired images and spectra of the capsule, its wake, and destructive re-entry of the spacecraft bus. Once calibrated, spectra of the capsule will be interpreted to yield data for comparison with and validation of high fidelity and engineering simulation tools used for design and development of future atmospheric entry system technologies. A brief summary of the Hayabusa mission, the preflight preparations and observation mission planning, mission execution, and preliminary spectral data are documented.

Spectroscopy↗
NASA NTRS2017

Value of Sample Return and High Precision Analyses: Need for A Resource of Compelling Stories, Metaphors and Examples for Public Speakers

There is widespread agreement among planetary scientists that much of what we know about the workings of the solar system comes from accurate, high precision measurements on returned samples. Precision is a function of the number of atoms the instrumentation is able to count. Accuracy depends on the calibration or standardization technique. For Genesis, the solar wind sample return mission, acquiring enough atoms to ensure precise SW measurements and then accurately quantifying those measurements were steps known to be non‐trivial pre‐flight. The difficulty of precise and accurate measurements on returned samples, and why they cannot be made remotely, is not communicated well to the public. In part, this is be-cause "high precision" is abstract and error bars are not very exciting topics. This paper explores ideas for collecting and compiling compelling metaphors and colorful examples as a resource for planetary science public speakers.

Allton, J. H.↗