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DOE OSTI2021

Gamma Spectrometry Examination of the AGR-3/4 Irradiation

The results from gamma spectrometry examination of the different components from the combined third and fourth U.S. Advanced Gas Reactor (AGR) TRISO-coated particle fuel irradiation tests (AGR-3/4) have been analyzed. This experiment was designed to provide information about in-pile fission product migration. In each of the 12 capsules, a single stack of four compacts with designed-to-fail (DTF) particles surrounded by inner and outer graphite and/or graphitic matrix rings and a graphite sink ring were irradiated in the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL). Gamma spectrometry has been used to evaluate the gamma-emitting fission product inventory of compacts from the irradiation and evaluate the burnup of these compacts based on the activity of the radioactive cesium isotopes (i.e., Cs-134 and Cs-137) in the compacts. Burnup from gamma spectrometry compares well with predicted burnup from simulations. The inner and outer rings were also examined by gamma spectrometry to evaluate the total fission product inventory of the rings, and gamma emission computed tomography (GECT) was used to investigate the spatial distribution of gamma-emitting fission products within the rings. This report focuses on results obtained via the Precision Gamma Scanner (PGS) for the compacts and inner and outer rings. These non-destructive gamma measurements are currently being compared to recent destructive measurements of spatial fission product distributions in the rings and to predictions made via mathematical modeling. A separate report discusses the entire AGR-3/4 fission product mass balance for all irradiation capsule components including the inner and outer rings, graphite sink rings, capsule spacers, capsule foils, through tubes, and felts. This report is similar to the conference proceedings: Harp, J.M., Demkowicz, P.A., and Stempien, J.D., “Initial gamma spectrometry examination of the AGR-3/4 irradiation,” International Topical Meeting High Temperature Reactor Technology (HTR 2016), Las Vegas, NV, USA, November 2016, Paper HTR2016-18593, but it has been updated to reflect all the data that has been collected on AGR-3/4 using PGS. The Appendices contain extensive data from the collected gamma spectra.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS1980

Orbit accuracy assessment for Seasat

Laser range measurements are used to determine the orbit of Seasat during the period from July 28, 1978, to Aug. 14, 1978, and the influence of the gravity field, atmospheric drag, and solar radiation pressure on the orbit accuracy is investigated. It is noted that for the orbits of three-day duration, little distinction can be made between the influence of different atmospheric models. It is found that the special Seasat gravity field PGS-S3 is most consistent with the data for three-day orbits, but an unmodeled systematic effect in radiation pressure is noted. For orbits of 18-day duration, little distinction can be made between the results derived from the PGS gravity fields. It is also found that the geomagnetic field is an influential factor in the atmospheric modeling during this time period. Seasat altimeter measurements are used to determine the accuracy of the altimeter measurement time tag and to evaluate the orbital accuracy.

Schutz, B. E.↗

NASA NTRS1982

The Seasat altimeter mean sea surface model

Gridding techniques are used to combine an 18-day set of Seasat altimeter data and two precisely-computed Seasat ephemerides, in order to arrive at global contour maps of the mean sea surface topography. The altimeter data have an rms agreement of 111 cm with the SS3 mean sea surface computed by means of the PGS-S3 ephemerides, and of 70 cm with the SS4 mean surface derived from the PGS-S4 ephemerides. While comparisons with the GEM 10B 1 x 1 deg gravimetric geoid have yielded rms differences of 2.8 m, those with a global mean sea surface derived from GEOS 3 altimeter data show rms differences of 1.3 m and 1.1 m for the cases of the SS3 and SS4 surfaces, respectively. An SS4 mean sea surface topograph is featured among the study findings presented. Further improvements in the representation of mean sea surface topography are expected with the development of more accurate gravity models for orbit computation.

Marsh, J. G.↗

NASA NTRS1989

Gravitational model improvement at the Goddard Space Flight Center

Major new computations of terrestrial gravitational field models were performed by the Geodynamics Branch of Goddard Space Flight Center (GSFC). This development has incorporated the present state of the art results in satellite geodesy and have relied upon a more consistent set of reference constants than was heretofore utilized in GSFC's GEM models. The solutions are complete in spherical harmonic coefficients out to degree 50 for the gravity field parameters. These models include adjustment for a subset of 66 ocean tidal coefficients for the long wavelength components of 12 major ocean tides. This tidal adjustment was made in the presence of 550 other fixed ocean tidal terms representing 32 major and minor ocean tides and the Wahr frequency dependent solid earth tidal model. In addition 5-day averaged values for Earth rotation and polar motion were derived for the time period of 1980 onward. Two types of models were computed. These are satellite only models relying exclusively on tracking data and combination models which have incorporated satellite altimetry and surface gravity data. The satellite observational data base consists of over 1100 orbital arcs of data on 31 satellites. A large percentage of these observations were provided by third generation laser stations (less than 5 cm). A calibration of the model accuracy of the GEM-T2 satellite only solution indicated that it was a significant improvement over previous models based solely upon tracking data. The rms geoid error for this field is 110 cm to degree and order 36. This is a major advancement over GEM-T1 whose errors were estimated to be 160 cm. An error propagation using the covariances of the GEM-T2 model for the TOPEX radial orbit component indicates that the rms radial errors are expected to be 12 cm. The combination solution, PGS-3337, is a preliminary effort leading to the development of GEM-T3. PGS-3337 has incorporated global sets of surface gravity data and the Seasat altimetry to produce a model complete to (50,50). A solution for the dynamic ocean topography to degree and order 10 was included as part of this adjustment.

Marsh, J. G.↗

NASA NTRS1990

Dynamic sea surface topography, gravity, and improved orbit accuracies from the direct evaluation of Seasat altimeter data

A gravitational model incorporating Seasat altimetry, surface gravimetry, and satellite tracking data has been determined in terms of global spherical harmonics complete to degree and order 50. This model, PGS-3337, uses altimeter data as a dynamic observation of the satellite's height above the sea surface. A solution for the ocean's dynamic topography is recovered simultaneously with the orbit parameters, gravity, and ocean tidal terms. The recovered dynamic topography reveals the global long wavelength circulation of the oceans with a resolution of 2000 km and is very similar to the mean upper ocean dynamic height derived from historical ship observations. The PGS-3337 geoid has an uncertainty of 60 cm rms globally but 25 cm rms over the ocean because of the altimeter measurements. Seasat orbits determined in this solution have an estimated accuracy for the radial position of 20 cm rms. The difference between the altimeter observed sea height and the geoid plus dynamic topography model is 30 cm rms. Contained in these residuals are the sea height variability, as well as errors from the geoid, orbits, tidal models, and altimeter range measurement. This performance level is 2 to 3 times better than that achieved with previous Goddard gravitational models.

Marsh, J. G.↗

NASA NTRS1991

WetNet operations

WetNet is an interdisciplinary Earth science data analysis and research project with an emphasis on the study of the global hydrological cycle. The project goals are to facilitate scientific discussion, collaboration, and interaction among a selected group of investigators by providing data access and data analysis software on a personal computer. The WetNet system fulfills some of the functionality of a prototype Product Generation System (PGS), Data Archive and Distribution System (DADS), and Information Management System for the Distributed Active Archive Center. The PGS functionality is satisfied in WetNet by processing the Special Sensor Microwave/Imager (SSM/I) data into a standard format (McIDAS) data sets and generating geophysical parameter Level II browse data sets. The DADS functionality is fulfilled when the data sets are archived on magneto optical cartridges and distributed to the WetNet investigators. The WetNet data sets on the magneto optical cartridges contain the complete WetNet processing, catalogue, and menu software in addition to SSM/I orbit data for the respective two week time period.

Goodman, H. Michael↗

DOE OSTI2020

Gamma Spectrometry Examination of the AGR-3/4 Irradiation

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2025

Fission Product Quantification and Burnup Analysis via Gamma Spectrometry of the AGR-5/6/7 TRISO Fuel Experiment

Five capsules containing varying configurations of TRISO fuel compacts were irradiated in the most recent Advanced Gas Reactor (AGR) TRISO test campaign, AGR-5/6/7. As part of the post-irradiation examination (PIE) of this work all the fuel compacts and capsule graphite holders were measured with the Precision Gamma Scanner (PGS) to determine isotopic activities and locations using gamma spectrometry. Measuring the compacts allowed for the comparison of physics model depletion calculations with the measured compact activity to validate models. These measurements also are used to find compacts of interest with low fission product retention that may be tested in subsequent PIE. Measurements of the holders can confirm fission product distribution and migration. Of the isotopes measured, Cs-137 and Cs-134 were used to estimate location of failed particles as well as determine a measured burnup estimation. Results from Capsule 1 compacts and the holder indicate many fuel particle failures occurred. There are high amounts of cesium in the holder near Stack 9 of Capsule 1 that corresponds to low fractions?measured-to-calculated (M/C) ratio?of cesium remaining in those compacts. All other capsules had cesium retention ratios near 1. The isotope 110mAg had less consistent results. Capsule 2 compacts exhibited a M/C of 0.20, much lower than anticipated for the temperatures these compacts underwent. Capsule 3 experienced much higher temperatures, >1300C and had an average M/C of 0.75. These are the opposite results than what was predicted by past AGR experiments for the relationship between temperature and isotope retention. Capsule 4 and 5 showed good fission product retention and agreement with the physics model predictions. The burnup results from the PGS measurements showed strong agreement between the physics models and the measured values. Using a ratio of Cs-134/Cs-137 to calculate the burnup match closely with the physics models. Additionally, the Cs-137 burnup results were less accurate but extremely close to the model results.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2021

A Genotype Signature for Predicting Pathologic Complete Response in Locally Advanced Rectal Cancer

To construct and validate a predicting genotype signature for pathologic complete response (pCR) in locally advanced rectal cancer (PGS-LARC) after neoadjuvant chemoradiation.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2026

Restoring Symmetry and Enhancing Exchange via Chiral Molecular-Magnetic Hexagons

Modified behaviors of molecules, designed for device or energy applications, can occur due to lattice-molecule incompatibilities in point-group symmetries (PGS), long-range interactions between neighboring molecules, or latticemolecule charge transfer. Such sensitivities are prerequisite for the use of quantum molecules as devices, but removing certain broken symmetries is desirable from the standpoint of simplifying their behaviors. Here, we demonstrate symmetry restoration to molecular-magnetic lattices and show that it leads to strengthened exchange-coupling due to dipolar electrostatic interactions between neighboring molecules and due to manifestations of an earlier identification of a spin-sensitive slightly mobile electron by Hooshmand et al. Starting with a broken symmetry molecular magnet of current interest, we demonstrate a more robust structure composed of six molecular magnets on a h-BN-like surface. The broken point-group symmetry is healed by constructing interpenetrating equilateral triangular structures that are appropriately ratcheted to preserve three-fold rotational symmetry and inversion symmetry.

Pederson, Mark R.↗

DOE OSTI2021

Singlet Oxygen Leads to Structural Changes to Chloroplasts during their Degradation in the Arabidopsis thaliana plastid ferrochelatase two Mutant

Abstract During stress, chloroplasts produce large amounts of reactive oxygen species (ROS). Chloroplasts also contain many nutrients, including 80% of a leaf’s nitrogen supply. Therefore, to protect cells from photo-oxidative damage and to redistribute nutrients to sink tissues, chloroplasts are prime targets for degradation. Multiple chloroplast degradation pathways are induced by photo-oxidative stress or nutrient starvation, but the mechanisms by which damaged or senescing chloroplasts are identified, transported to the central vacuole and degraded are poorly defined. Here, we investigated the structures involved with degrading chloroplasts induced by the ROS singlet oxygen (1O2) in the Arabidopsis thaliana plastid ferrochelatase two (fc2) mutant. Under mild 1O2 stress, most fc2 chloroplasts appeared normal, but had reduced starch content. A subset of chloroplasts was degrading, and some protruded into the central vacuole via ‘blebbing’ structures. A 3D electron microscopy analysis demonstrated that up to 35% of degrading chloroplasts contained such structures. While the location of a chloroplast within a cell did not affect the likelihood of its degradation, chloroplasts in spongy mesophyll cells were degraded at a higher rate than those in palisade mesophyll cells. To determine if degrading chloroplasts have unique structural characteristics, allowing them to be distinguished from healthy chloroplasts, we analyzed fc2 seedlings grown under different levels of photo-oxidative stress. A correlation was observed among chloroplast swelling, 1O2 signaling and the state of degradation. Finally, plastoglobule (PG) enzymes involved in chloroplast disassembly were upregulated while PGs increased their association with the thylakoid grana, implicating an interaction between 1O2-induced chloroplast degradation and senescence pathways.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2022

Pseudogauge dependence of the spin polarization and of the axial vortical effect

The mean spin polarization vector of spin 1/2 particles in a relativistic fluid at local thermal equilibrium (LTE) in different pseudogauges (PGs), i.e., with different choices for the decomposition of orbital and spin angular momentum, is obtained. The spin polarization obtained in the canonical PG differs from the one obtained in the Belinfante PG. It is found that this difference can not be written by replacing the thermal vorticity with the spin potential in the usual polarization formula. Other PG choices affect the contribution of thermal shear to the spin polarization. So, the choice of a PG affects the predictions for the polarization measured in heavy-ion collisions. In general, it is shown that the Wigner function of a noninteracting Dirac field at LTE is affected by the PG transformations. Explicit expressions of the mean axial current are also calculated and it is found that even the axial vortical effect conductivity depends on the PG.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2025

Sulfur Species in Zinc-Rich Condylar Zones of a Rat Temporomandibular Joint

We performed synchrotron-based micro-X-ray absorption near-edge spectroscopy (µ-XANES) coupled with micro-X-ray fluorescence (µ-XRF) for the identification of elements that included biometal zinc (Zn) and nonmetal sulfur (S) (and its species) in the condylar zones of a rat temporomandibular joint (TMJ). Zone-specific spatial localization of biometal Zn and nonmetal S from a materials viewpoint when correlated with hypoxia inducible factor-1α (HIF-1α) (a surrogate for tissue oxygenation) can provide insights into Zn-specific redox pathways at the vulnerable subchondral interface. Histologic localization of Zn, HIF-1α, and sulfur-rich proteoglycans (PGs) were mapped using an optical microscope. The µ-XRF maps coupled with site-specific micro-X-ray diffraction (µ-XRD) patterns were used to underline Zn-incorporated biological apatite in the subchondral bone and the bone of a rat TMJ condyle. Results demonstrated an association between Zn, PG, and HIF-1α histologic maps with µ-XRF, µ-XANES, and µ-XRD data and provided insights into plausible biological S species in Zn-enriched zones of a rat TMJ condyle. Spatially localized Zn and S underscore their roles in cell and tissue functions in a zone-specific manner. Elemental Zn with organic and inorganic S species at the cartilage-bone interface and the biomineral phase of Zn-enriched biological apatite from subchondral bone to condylar bone were ascertained using µ-XRF-XANES and µ-XRF-XRD. The coupled µ-XRF-XANES in situ complemented with µ-XRF-XRD in situ and immunohistochemistry provided valuable biological insights into zone-specific biological pathways in rat TMJ condyles. Based on these data, we present a workflow to reliably map and correlate S species within Zn-enriched regions of cartilage, bone, and their interface. We suggest the use of this correlative and complementary microspectroscopic spatial information for zone-specific localization of biometal Zn and nonmetal S to gain insights into plausible microanatomy-specific oxidative stress in the TMJ.

apatites↗

DOE OSTI2021

Specification of EBR-II Gamma Scan Data from the Precision Gamma Scanner

The gamma scan data stored in the FIPD was originally measured using the Precision Gamma Scanner (PGS) at the Hot Fuel Examination Facility (HFEF) at Idaho National Laboratory (INL). This system was originally manufactured in 1971 (when the facilities, now at INL, were operated by Argonne National Laboratory) and was upgraded on several occasions. It consists of a germanium gamma ray detector (the exact nature of which changed over time as technology improved), a variable-slit collimator that blocks the view of gamma emissions from all but the selected area of the target, and a computer-controlled system for translating a sample past the slit and logging the data.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2023

ECAR-6589 Reflector Support Structure Analysis: Project #33526

The MARVEL microreactor consists of five main systems: MRS (MARVEL Reactor Structure), PGS (Power Generation System), FCS (Fuel Core System), RCS (Reactivity Control System), and ICS (Instrument Control System). The RSS (Reflector Control System) is a sub system of the MRS which contains the upper and lower reflector support plates which support and locate the stationary core reflector and provide vertical support for the control drums. They are suspended from the Primary Coolant System by bolted structural straps which utilize a turnbuckle to allow for adjustment and leveling of the support plates. The stainless-steel support plates are each formed from four quarter circle segments which are bolted together around the lower core barrel. Bearing plates of non-galling Nitronic 60 alloy are fitted to the inner diameter of the support plates to prevent adhesive wear between the plates and the core barrel as the barrel expands and contracts due to changes in the temperature of the reactor.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

NASA NTRS1985

Global mean sea surface computation based upon a combination of SEASAT and GEOS-3 satellite altimeter data

A mean sea surface map was computed for the global ocean areas between 70 deg N latitude and 62 deg S latitude based upon the 70 day SEASAT and 3.5 year GEOS-3 altimeter data sets. The mean sea surface is presented in the form of a global contour map and a 0.25 deg x 0.25 deg grid. A combination of regional adjustments based upon crossover techniques and the subsequent adjustment of the regional solutions into a global reference system was employed in order to minimize the effects of radial orbit error. A global map of the crossover residuals after the crossover adjustments are made is in good agreement with earlier mesoscale variability contour maps based upon the last month of SEASAT collinear data. This high level of agreement provides good evidence that relative orbit error was removed to the decimeter level on a regional basis. This represents a significant improvement over our previous maps which contained patterns, particularly in the central Pacific, which were due to radial orbit error. Long wavelength, basin scale errors are still present with a submeter amplitude due to errors in the PGS-S4 gravity model. Such errors can only be removed through the improvement of the Earth's gravity model and associated geodetic parameters.

Marsh, J. G.↗

NASA NTRS1988

Evaluation of advanced geopotential models for operational orbit determination

To meet future orbit determination accuracy requirements for different NASA projects, analyses are performed using Tracking and Data Relay Satellite System (TDRSS) tracking measurements and orbit determination improvements in areas such as the modeling of the Earth's gravitational field. Current operational requirements are satisfied using the Goddard Earth Model-9 (GEM-9) geopotential model with the harmonic expansion truncated at order and degree 21 (21-by-21). This study evaluates the performance of 36-by-36 geopotential models, such as the GEM-10B and Preliminary Goddard Solution-3117 (PGS-3117) models. The Earth Radiation Budget Satellite (ERBS) and LANDSAT-5 are the spacecraft considered in this study.

Radomski, M. S.↗

NASA NTRS1994

MODIS. Volume 1: MODIS level 1A software baseline requirements

This document describes the level 1A software requirements for the moderate resolution imaging spectroradiometer (MODIS) instrument. This includes internal and external requirements. Internal requirements include functional, operational, and data processing as well as performance, quality, safety, and security engineering requirements. External requirements include those imposed by data archive and distribution systems (DADS); scheduling, control, monitoring, and accounting (SCMA); product management (PM) system; MODIS log; and product generation system (PGS). Implementation constraints and requirements for adapting the software to the physical environment are also included.

Masuoka, Edward↗