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At least 37 records · Page 2

Heterogeneous fatigue damage in a nickel-based single-crystal superalloy unraveled using correlative 3D X-ray technology

Nickel-based single-crystal (Ni-SX) superalloys under cyclic stress are susceptible to cracking at stress-concentration sites, eventually leading to low-cycle fatigue (LCF) failure. LCF cracks typically originate from intrinsic defects (e.g., voids and carbides) within solidified dendrites. However, systematic quantitative experimental analyses of defect-mediated local damage remain limited. To thoroughly understand the microscopic origins and evolution of LCF damage, correlated 3D mapping of dendrites across various regions is essential. Here, in this study, macroscale micro-computed tomography (μ-CT) was initially used to capture internal interdendritic secondary cracks within bulk DD413 superalloy after LCF testing at 760 °C. Subsequently, a multimodal methodology combining synchrotron 3D microdiffraction (3D-μXRD), high-resolution μ-CT, and electron microscopy was established. This approach allowed precise localization of internal damage zones near interdendritic secondary cracks and detailed mapping of the 3D correlated distributions of dendrites, defects, and residual stress/strain fields within these zones at submicron spatial resolution. Finally, the same approach was applied to specimens subjected to interrupted loading at approximately 40 % of the fatigue life to uncover the early damage states of dendrites. The dendrite cores (DCs) and interdendritic regions (IDs) exhibit microscale heterogeneous mechanical responses: nearly defect-free DCs accumulate local irreversible slip along specific slip systems to generate slip bands, while the IDs containing various defects accommodate local microplasticity through the activation of multiple slip systems around these defects. The local tensile stress near defects in the IDs exceeds that in the DC slip band regions by more than threefold, leading to the generation of local damage zones within the IDs. Chain-like defect distributions facilitate the interconnection of these local zones into a continuous damage region, further elevating the overall tensile stress in the IDs. Additionally, geometrically necessary dislocations alone are insufficient as indicators of LCF damage; both the internal stress state and its magnitude must be considered. These experimental results provide critical data and insights for the development of multi-physics fatigue models.

Localized deformation↗

Microstructure-Based Estimation of Strength and Ductility Distributions for \(\alpha +\beta \) Titanium Alloys

Titanium alloys are processed to develop a wide range of microstructure configurations and therefore material properties. While these properties are typically measured experimentally, a framework for property prediction could greatly enhance alloy design and manufacturing. In this work, a microstructure-sensitive framework is presented for the prediction of strength and ductility as well as estimates of the bounds in variability for these properties. The framework explicitly considers distributions of microstructure via new approaches for instantiation of structure in synthetic samples. The parametric evaluation strategy, including the finite element simulation package FEpX, is used to create and test virtual polycrystalline samples to evaluate the variability bounds of mechanical properties in Ti-6Al-4V. Critical parameters for the property evaluation framework are provided by measurements of single crystal properties and advanced characterization of microstructure and slip system strengths in 2D and 3D. Property distributions for yield strength and ductility are presented, along with the validation and verification steps undertaken. Comparisons between strain localization and slip activity in virtual samples and in experimental grain-scale strain measurements are also discussed.

36 MATERIALS SCIENCE↗

Geological and vegetational applications of Shuttle Imaging Radar-B, Mineral County, Nevada

Multiple-incidence angle and multi-azimuth radar data were acquired from a Shuttle platform over test sites in Nevada in October 1984. An attempt was made to correlate these data with ground features for the purpose of evaluating the use of such data for geological and vegetational assessment. Standard ecological parameters with respect to the flora (community composition, dominance, and relative cover) were recorded in the field at the time of overflight. Although a total of 33 species representing 11 plant families were recognized, and plant cover ranged from 13 to 26 percent, radar data could not be used to separate plant communities. The signal return is more a function of abiotic conditions than vegetative characteristics. Illumination geometry plays an important role in the ability to detect strike-slip and dip-slip faults. Local incidence angle is the most important parameter, and SIR-B data takes with small incidence angles are superior for identifying certain styles of faulting. Look direction is critical for detecting faults with a dip-slip component. New structural features were not observed. Problems with radar antenna power and recording significantly affected data quality.

Borengasser, M. X.↗

Crustal Deformation and the Seismic Cycle Across the Kodiak Islands, Alaska

The Kodiak Islands are located approximately 120 to 250 km from the Alaska-Aleutian Trench - and are within the southern extent of the 1964 Prince William Sound (M(sub w) = 9.2) earthquake rupture zone. Here we report new campaign GPS results (1993-2001) from northern Kodiak Island. The rate and orientation of the horizontal velocities, relative to a fixed North America, range from 25.3 plus or minus 1.4 mm/yr at N32.9 deg. W plus or minus 2.5 to 8.5 plus or minus 1.0 mm/yr at N59.7 deg. W plus or minus 6.5 deg. In addition to the northern Kodiak data, we analyzed data from three southern Kodiak Island stations. The inland stations from both the northern and southern networks indicate a counterclockwise rotation of the velocity vectors. These results are consistent with the hypothesis that the difference between the Pacific-North American plate motion and the orientation of the down going slab would lead to 4-8 mm/yr of left-lateral slip above the unlocked, down-dip portion of the main thrust zone. The northern and southern Kodiak geodetic data are consistent with a model that includes the viscoelastic response to (1) a downgoing Pacific plate interface that is locked at shallow depths, (2) local coseismic slip in the 1964 earthquake, and (3) interseismic creep down dip from the seismogenic zone. Based on the pre-1964 and post-1944 earthquake history, as well as the pattern of interseismic earthquakes across the plate boundary zone, we hypothesize that in southern Kodiak some strain is released in moderate to large earthquakes between the occurrences of great earthquakes like the 1964 event.

Sauber, Jeanne↗

Stress-controlled fatigue of HfNbTaTiZr high-entropy alloy and associated deformation and fracture mechanisms

The stress-controlled fatigue tests are carried out at a stress ratio of 0.1 and a frequency of 10 Hz, and span both low-cycle and high-cycle regimes by varying the applied stress amplitudes. The high-cycle fatigue regime gives a fatigue strength of 497 MPa and a fatigue ratio of 0.44. At equivalent conditions, the alloy's fatigue strength is greater than all other high-entropy alloys (HEAs) with reported high-cycle fatigue data, dilute body-centered cubic alloys, and many structural alloys such as steels, titanium alloys, and aluminum alloys. Through in-depth analyses of crack-propagation trajectories, fracture-surface morphologies and deformation plasticity by means of various microstructural analysis techniques and theoretical frameworks, the alloy's remarkable fatigue resistance is attributed to delayed crack initiation in the high-cycle regime, which is achieved by retarding the formation of localized persistent slip bands, and its good resistance to crack propagation in the low-cycle regime, which is accomplished by intrinsic toughening backed up by extrinsic toughening. Additionally, the stochastic nature of the fatigue data is neatly captured with a 2-parameter Weibull model.

36 MATERIALS SCIENCE↗

Elastic-plastic deformation of a metal-matrix composite coupon with a center slot

A comprehensive experimental analysis of deformations of the surface of a metal-matrix specimen is reported. The specimen is a 6-ply 0 + or - 45 sub s boron-aluminum tensile coupon with a central slot. Moire interferometry is used for high-sensitivity whole-field measurements of in-plane displacements. Normal and shear strains are calculated from displacement gradients. Displacement fields are analyzed at various load levels from 15% to 95% of the failure load. Deformations of the boron fibers could be distinguished from those of the matrix. Highly localized plastic slip zones occur tangent to the ends of the slot. Shear strains and concurrent transverse compressive strains in the slip zones reach approximately 10% and 1%, respectively. Upon unloading, elastic recovery in surrounding regions causes a reverse plastic shear strain in the slip zone of about 4%. Longitudinal normal strains on the unslotted ligament peak at the slot boundary at about 1% strain. The strain concentration factor at the end of the slot decreases with load level and the advance of plasticity.

Post, D.↗

Deformation of a metal-matrix tensile coupon with a central slot - An experimental study

A metal-matrix specimen was investigated using high-sensitivity moire interferometry. In-plane displacement fields were analyzed at various load levels from 15 to 95 percent of the failure load. Normal and shear strains were determined from displacement gradients. Highly localized plastic slip zones occured in the ductile aluminum matrix tangent to the ends of the slot. Shear strains in the slip zone were an order of magnitude greater than the largest normal strains in the specimen. The shear-strain concentration factor rose dramatically with the onset of plastic slip and continued to rise gradually with load to 95 percent of the failure load. Upon unloading, shear strains in the slip zone remained precariously high.

Post, Daniel↗

Structural review of the Vredefort dome

The structure of the older-than-3.2-Ga Archean basement and Archean-to-Precambrian sedimentary/volcanic rocks (3.07 to ca. 2.2 Ga) in the center of the Witwatersrand Basin to the southwest of Johannesburg (South Africa) is dominated by the ca. 2.0-Ga megascopic Vredefort 'Dome' structure. The effect of the 'Vredefort event' is demonstrably large and is evident within a northerly arc of about 100 km radius around the granitic core of the structure. Northerly asymmetric overturning of the strata is observed within the first 17 km (strata is horizontal in the south), followed by a 40-km-wide rim synclinorium. Fold and fault structures (normal, reverse, and strike-slip) are locally as well as regionally concentrically arranged with respect to the northern and western sides of the structure. The unusual category of brittle deformation, the so-called 'shock deformation', observed in the collar strata has attracted worldwide attention over the past two decades. These deformation phenomena include the presence of coesite and stishovite, mylonites, and pseudotachylites, cataclasis at a microscopic scale, and the ubiquitous development of multiply striated joint surfaces (which include shatter cones, orthogonal, curviplanar, and conjugate fractures). The macroscopic to microscopic deformation features have led to the formulation of various hypotheses to account for the origin of the Vredefort structure: (1) tectonic hypotheses--deep crustal shear model, doming and N-directed thrust fault model, fold interference model, and diapir model; (2) the exogenous bolide impact hypothesis; and (3) the endogenous cryptoexplosion model.

Colliston, W. P.↗

Divergent evolution of slip banding in CrCoNi alloys

Abstract Metallic materials under high stress often exhibit deformation localization, manifesting as slip banding. Over seven decades ago, Frank and Read introduced the well-known model of dislocation multiplication at a source, explaining slip band formation. Here, we reveal two distinct types of slip bands (confined and extended) in compressed CrCoNi alloys through multi-scale testing and modeling from microscopic to atomic scales. The confined slip band, characterized by a thin glide zone, arises from the conventional process of repetitive full dislocation emissions at Frank–Read source. Contrary to the classical model, the extended band stems from slip-induced deactivation of dislocation sources, followed by consequent generation of new sources on adjacent planes, leading to rapid band thickening. Our findings provide insights into atomic-scale collective dislocation motion and microscopic deformation instability in advanced structural materials.

Science & Technology - Other Topics↗

The role of the gamma/gamma-prime eutectic and porosity on the tensile behavior of a single-crystal nickel-base superalloy

The microstructure of a single-crystal nickel-base superalloy, PWA 1480, has been varied by heat treatment and hot isostatic pressing in order to study the role of the gamma/gamma-prime eutectic and porosity on subsequent tensile behavior. The level of porosity was found not to affect any of the tensile properties, while the gamma/gamma-prime eutectic strongly influenced ductility. Eliminating the gamma/gamma-prime eutectic increased ductility which was attributed to the cleavage fracture of this constituent. It is proposed that such cleavage of the gamma/gamma-prime eutectic is initiated by the stress created from impinging slip bands, promoting shear localization, and final fracture along 111 slip planes. The precise nature of this fracture process is discussed, with emphasis on the role of the gamma/gamma-prime microstructure. The deformation structure of PWA 1480 was also studied, and while different in some respects from many other single-crystal superalloys, its fracture process appears to be similar.

Walston, W. S.↗

The effects of free surfaces on deformation twinning in HCP metals

Deformation twinning is a predominant mode of plastic deformation for hexagonal close packed metals, like Mg and Ti. The heterogenous microstructure and the local stresses associated with twinning play a key role in their mechanical response and fracture. Surface analyses, like electron microscopy, are frequently employed to spatially map microstructure and micromechanical fields in order to study twinning behavior. However, these measurements are inherently influenced by the vicinity of the free surface. In this work, an elasto-visco-plastic fast-Fourier-transform (EVP-FFT) polycrystal modeling approach is employed to investigate the effects of free surfaces on twin development before and after loading. We compare calculated micromechanical fields on free surfaces with those calculated inside the bulk and, in some cases, experimental surface measurements. The results indicate that the creation of free surfaces can promote twin propagation and growth and can influence twin morphology by causing a twin lamella to become larger, more blunted and irregular. The structure along the twin boundaries are also affected, due to the higher driving stresses that extend prismatic-basal and basal-prismatic facets. Furthermore, free surfaces invoke different slip activities in the twin and the surrounding parent crystal by enhancing basal, prismatic and pyramidal slip in some localized regions, while reducing slip in others. We demonstrate that the simulated free-surface effects lead to better qualitative and quantitative agreement with experimental measurements from scanning electron microscopy and digital image correlation.

36 MATERIALS SCIENCE↗

Investigation of the fracture mechanism of Ti-5Al-2.5Sn at cryogenic temperatures

Fractography and metallographic sectioning were used to investigate the influence of microstructure on the fracture mechanism and fracture toughness (KIC) of normal interstitial and extra low interstitial (ELI) Ti-5Al-25Sn at 20 K (-423 F) and 77 K (-320 F). Plates of each grade were mill annealed at 815 C followed by either air or furnace cooling. These variations in composition and cooling rate resulted in differences in the volume fraction and internal structure of the dispersed beta phase and in the ordering of the alpha matrix. The ELI alloys were tougher than the normal interstitial plates. KIC of the furnace-cooled ELI plate was 25% lower than that of the air-cooled ELI material. Variations in cooling rate had no influence of KIC of the normal interstitial alloys. Fractography showed that a large portion of the fracture surfaces were covered with elongated dimples. Metallographic sections of specimens deformed at 77 K showed that these features form at the intersections of slip bands or deformation twins with grain or twin boundaries. Ordering and higher interstitial levels increase the local strain in slip bands resulting in void nucleation at lower macroscopic strains and lower KIC values.

Van Stone, R. H.↗

Maximum strength and dislocation patterning in multi–principal element alloys

Multi–principal element alloys (MPEAs) containing three or more components in high concentrations render a tunable chemical short-range order (SRO). Leveraging large-scale atomistic simulations, we probe the limit of Hall-Petch strengthening and deformation mechanisms in a model CrCoNi alloy and unravel chemical ordering effects. The presence of SRO appreciably increases the maximum strength and lowers the propensity for faulting and structure transformation, accompanied by intensification of planar slip and strain localization. Deformation grains exhibit notably different microstructures and dislocation patterns that prominently depend on their crystallographic orientation and the number of active slip planes. Grain of single-planar slip attains the highest volume fraction of deformation-induced structure transformation, and grain with double-slip planes develops the densest dislocation network. These results advancing the fundamental understanding of deformation mechanisms and dislocation patterning in MPEAs suggest a mechanistic strategy for tuning mechanical behavior through simultaneously tailoring grain texture and local chemical order.

36 MATERIALS SCIENCE↗

A quantitative study of stress fields ahead of a slip band blocked by a grain boundary in unalloyed magnesium

Stress localization ahead of a slip band blocked by a grain boundary is measured for three different grain boundaries in unalloyed Mg using high-resolution electron backscatter diffraction (HR-EBSD). The results are compared with a theoretical dislocation pile-up model, from which slip system resistance and micro-Hall–Petch coefficients for different grain boundary types are deduced. The results indicate that grain boundary character plays a crucial role in determining micro-Hall–Petch coefficients, which can be used to strengthen classical crystal plasticity constitutive models to make predictions linked to the effect of grain boundary strengthening.

42 ENGINEERING↗

Vibration characteristics of mistuned shrouded blade assemblies

An investigation of the mode localization phenomenon associated with mistuning is presented for shrouded blade assemblies. The calculations are based on a generic finite element model, which permits modeling of arbitrary mistuning and both slipping and nonslipping shroud interfaces. The results presented indicate that interactions occur between mistuning and slip effects, with maximum mode localization occurring when the shrouds slip freely. Certain modes are found to be very sensitive to shroud slip, and in some cases completely change character when slip occurs. Mode localization is most pronounced in the predominantly bending modes, and varies considerably from mode to mode. As the ratio of interblade coupling strength to mistuning strength is increased, the effect of mistuning is observed to decrease significantly. This result has important implications for the flutter problem, since it suggests that the stabilization effect available from mistuning is significantly less for a shrouded rotor as compared to an unshrouded rotor.

Bendiksen, O. O.↗

Focal depths and fault plane solutions of earthquakes and active tectonics of the Himalaya

Synthetic seismograms were compared with long-period body waves for nine earthquakes with epicenters in the Himalayan arc to determine depths of foci and to improve fault plane solutions. Focal depths are shallow (10-20 km). Inferred slip vectors are locally perpendicular to the mountain range; they plunge very gently (about 10 deg) in the eastern sections of the range and more steeply (about 25 deg) in western sections. Assuming India to be a rigid plate, the radially oriented slip vectors imply that southern Tibet extends at about half the rate of underthrusting in the Himalaya and therefore probably at about 5-10 mm/yr. The shallow depths and gentle dips of the fault planes, at least for the events in the eastern half of the range, are consistent with coherent underthrusting of the Indian plate beneath, at least, the Lesser Himalaya. The steeper dips of fault planes in the western part of the arc might reflect deformation of the overriding thrust plate or simply a steepening of the main underthrusting zone beneath the Greater Himalaya.

Baranowski, J.↗

Variability of near-fault seismic risk to reinforced concrete buildings based on high-resolution physics-based ground motion simulations

Broadband physics-based simulated earthquake ground motions are utilized to characterize the regional-scale seismic risk to modern reinforced concrete (RC) structures. A highly dense dataset of ground motions covering a 100-km urn:x-wiley:00988847:media:eqe3413:eqe3413-math-0001 40-km domain was generated using kinematic fault rupture models with varying rupture characteristics to represent shallow crustal earthquakes and resolved up to frequencies of 5 Hz. Over 40,000 nonlinear response history simulations of short- and mid-rise RC special moment frame buildings were conducted using simulation models that are capable of representing nonlinear behavior and component deterioration effects. The spatial variability of structural risk within a single earthquake scenario and between different rupture scenarios is examined, and the regions of strongest directivity effects and highest structural demands are identified. The structural demands may vary by factor of up to 8.0 at very short distances from the fault, and the large dispersion in the demands decreases significantly beyond a distance of 15 km. The interstory drift and member rotation demands are substantially impacted by important features of the geological structure and the characteristics of the rupture scenarios, particularly the presence of localized high-slip regions. The frequency characteristics of the structures are found to play an important role in determining the effects of near-fault ground motions on the structural response and expected damage. The results of this study suggest that the simulated ground motions, particularly those generated using the hybrid rupture approach, may offer reasonable structural risk estimates for low-frequency structures and conservative estimates for high-frequency structures.

58 GEOSCIENCES↗

A stochastic solver based on the residence time algorithm for crystal plasticity models

Abstract The deformation of crystalline materials by dislocation motion takes place in discrete amounts determined by the Burgers vector. Dislocations may move individually or in bundles, potentially giving rise to intermittent slip. This confers plastic deformation with a certain degree of variability that can be interpreted as being caused by stochastic fluctuations in dislocation behavior. However, crystal plasticity (CP) models are almost always formulated in a continuum sense, assuming that fluctuations average out over large material volumes and/or cancel out due to multi-slip contributions. Nevertheless, plastic fluctuations are known to be important in confined volumes at or below the micron scale, at high temperatures, and under low strain rate/stress deformation conditions. Here, we develop a stochastic solver for CP models based on the residence-time algorithm that naturally captures plastic fluctuations by sampling among the set of active slip systems in the crystal. The method solves the evolution equations of explicit CP formulations, which are recast as stochastic ordinary differential equations and integrated discretely in time. The stochastic CP model is numerically stable by design and naturally breaks the symmetry of plastic slip by sampling among the active plastic shear rates with the correct probability. This can lead to phenomena such as intermittent slip or plastic localization without adding external symmetry-breaking operations to the model. The method is applied to body-centered cubic tungsten single crystals under a variety of temperatures, loading orientations, and imposed strain rates.

42 ENGINEERING↗