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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Sound Speed as a Candidate for Internal Temperature Monitoring During Solid Phase Processing of Materials

Internal temperature is an important parameter for understanding the solid phase processing (SPP) of materials and improving feedback control of these processes. Friction stir processes, shear assisted processing and extrusion (ShAPE ™ ), and ultrahigh velocity (UHV) cold spray are examples of such processes. Simple thermal models based on temperatures measured at the boundary of the deforming body cannot capture the dynamic nature of temperature generation within the deforming solid. One possibly way of understanding internal temperature is by measuring sound speed, which varies as a function of temperature for materials and directing ultrasonic wave propagation through selected material volumes of interest. In this project, longitudinal wave speed is estimated for aluminum 6061. Piezoelectric materials bonded to a specimen provided data from which longitudinal wave speed was estimated. A discussion evaluated the linear relationship of wave speed versus temperature and postulated how wave speed measurements could be used to estimate the internal temperature of selected material volumes for feedback during SPP of materials. Instrumentation, data and analysis, and a discussion are reviewed.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Hugoniot, sound speed, and phase transitions of single-crystal sapphire for pressures 0.2–2.1 TPa

Sapphire (Al 2 O 3 ) is a major constituent of the Earth's mantle and has significant contributions to the field of high-pressure physics. Constraining its Hugoniot over a wide pressure range and identifying the location of shock-driven phase transitions allows for development of a multiphase equation of state and enables its use as an impedance-matching standard in shock physics experiments. In this paper we present measurements of the principal Hugoniot and sound velocity from direct impact experiments using magnetically launched flyers on the Z machine at Sandia National Laboratories. The Hugoniot was constrained for pressures from 0.2–2.1 TPa and a four-segment piecewise linear shock-velocity–particle-velocity fit was determined. First-principles molecular dynamics simulations were conducted and agree well with the experimental Hugoniot. Sound-speed measurements identified the onset of melt between 450 and 530 GPa, and the Hugoniot fit refined the onset to 525 ± 13 GPa. A phase diagram which incorporates literature diamond-anvil cell data and melting measurements is presented.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2024

Speed of Sound Measurements of R-1130(E) and an Azeotropic Blend of R-1336mzz(Z)/1130(E)

Sound speed data measured using a dual-path pulse-echo instrument are reported for pure trans-1,2-dichloroethene (R-1130(E)) and an azeotropic blend of cis-1,1,1,4,4,4-hexafluorobutene (R-1336mzz(Z)) and R-1130(E) with a composition of 74.8 mass % R-1336mzz(Z) with the balance being R-1130(E). The azeotropic blend of R-1336mzz(Z)/1130(E) is classified as R-514A in ANSI/ASHRAE standard 34. Liquid phase speed of sound data are reported from just above the saturation pressure of pure R-1130(E) or the bubble point pressure of R-514A to a maximum pressure of 26.7 MPa. The relative combined expanded uncertainty in the speed of sound varies from 0.032 % to 0.148 % with the greatest deviations occurring at the lowest sound speeds. At present, no reference Helmholtz-energy-explicit equation of state (EOS) is available for R-1130(E). Therefore, the reported data for pure R-1130(E) are compared to an extended corresponding states (ECS) model. Deviations between the pure R-1130(E) sound speed data and the ECS model were found to be consistently negative ranging between − 4.1 % and − 3.5 %. The R-514A data are compared to a multifluid model inclusive of the established reference Helmholtz-energy-explicit EOS for R-1336mzz(Z) and ECS model for R-1130(E) with estimated binary interaction parameters. Deviations between the experimental speed of sound data and the multifluid model were also found to be consistently negative. However, deviations from the multifluid model were found to be as great as − 17.1 %. The large deviations from the ECS model and multifluid model underscore the need for a robust Helmholtz-energy-explicit EOS for R-1130(E).

42 ENGINEERING↗
DOE OSTI2025

Sound Speeds of Solids from Ultrasonic Pulse Receiver Measurements

A common method of determining elastic material properties is utilizing an ultrasonic pulse receiver. This is a non-destructive test (NDT) causing no plastic deformation of the material. It requires a pulse generator, oscilloscope, and two transducers to measure the sound velocity of a material. Both longitudinal and shear sound velocities may be obtained by utilizing the appropriate transducer. Acoustic nondestructive testing methods are often used in manufacturing certification processes and for material defect detection in industry. These methods can also be utilized to directly measure the elastic moduli of a material without damaging the material. Overall, it is a low-cost experiment with minimal preparation, and is easy to use.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Sound speed and refractive index of amorphous CaSiO3 upon pressure cycling to 40 GPa

Abstract Brillouin spectroscopy at room temperature and pressures up to 40 GPa documents nearly identical elasticity and refractive index of amorphous CaSiO3 created by two different methods: temperature-quenching the melt at ambient pressure and pressure-amorphizing crystalline wollastonite at room temperature. We find reproducible hysteresis of 0 to 8% on pressure cycling that is small relative to the 30 to 60% changes in shear and longitudinal wave velocities over this pressure range. Together with observed changes in refractive index and previous results from Raman spectroscopy, these measurements reveal a continuous and reversible change in atomic packing induced by pressure. Unlike many other silicate glasses, amorphous CaSiO3 exhibits highly reproducible properties, behaving smoothly and reversibly under pressure cycling and possessing similar structure and elasticity regardless of synthesis paths for the starting material, which suggests that the amorphous solid may mimic the liquid over the pressure range investigated.

Geochemistry & Geophysics↗
DOE OSTI2024

Speed of sound in methane under conditions of planetary interiors

We present direct observations of acoustic waves in warm dense matter. We analyze wave-number- and energy-resolved x-ray spectra taken from warm dense methane created by laser heating a cryogenic liquid jet. X-ray diffraction and inelastic free-electron scattering yield sample conditions of 0.3 ± 0.1 eV and 0.8 ± 0.1 g/ cm − 3 , corresponding to a pressure of ∼ 13 GPa. Inelastic x-ray scattering was used to observe the collective oscillations of the ions. With a highly improved energy resolution of ∼ 50 meV, we could clearly distinguish the Brillouin peaks from the quasielastic Rayleigh feature. Data at different wave numbers were utilized to derive a sound speed of 5.9 ± 0.5 km/s, marking a high-temperature data point for methane and demonstrating consistency with Birch's law in this parameter regime. Published by the American Physical Society 2024

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2022

Speed of Sound Measurements of Binary Mixtures of Difluoromethane (R-32) with 2,3,3,3-Tetrafluoropropene (R-1234yf) or trans-1,3,3,3-Tetrafluoropropene (R-1234ze(E)) Refrigerants

In this article, sound speed data measured using a dual-path pulse-echo instrument are reported for binary mixtures of difluoromethane (R-32) with 2,3,3,3-tetrafluoropropene (R-1234yf) or trans-1,3,3,3-tetrafluoropropene (R-1234ze(E)). The sound speed is reported at two compositions for each binary mixture of approximately (0.33/67) and (0.67/0.33) mole fraction at temperatures between 230 K and 345 K. Data are reported from pressures slightly above the bubble point to 12 MPa for R-32/1234yf mixtures to avoid potential polymerization reactions and to 53 MPa for the R-32/1234ze(E) mixtures. The mean uncertainty of the sound speed data are less than 0.1% of the measured value where uncertainties at individual state points range from 0.04% to 0.5% of the measured value as the conditions approach the mixture critical region. The reported data are compared to available Helmholtz-energy-explicit EOS included in REFPROP and all systems studied have average absolute deviations greater than 2%. The comparisons show that further adjustments to the mixture models are needed to provide a reasonable representation of the data within its experimental uncertainty.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Speed of Sound Measurements of Binary Mixtures of 1,1-Difluoroethylene (R-1132a) + Propane and Derived Speed of Sound of Pure R-1132a

Speed of sound data, measured using a dual-path pulse-echo instrument, are reported for three binary mixtures of 1,1-difluoroethylene (R-1132a) with propane at temperatures ranging from 230 to 345 K and pressures ranging from slightly above the bubble curve to a maximum pressure of 50 MPa. Significant attenuation of the pulse-echo signals was observed for measurements on pure R-1132a. Therefore, the R-1132a sample was doped with propane at mole fractions ranging from 0.0274 to 0.0887 and the propane + R-1132a mixture data was used to derive sound speeds for pure R-1132a. The data were compared to a preliminary equation of state for R-1132a, and deviations ranged from 2 % to 8 %. This demonstrates that the preliminary R-1132a EoS needs to be refit to better represent the speed of sound.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Speed of Sound Measurements of Binary Mixtures of Hydrofluorocarbons [Pentafluoroethane (R-125), 1,1-Difluoroethane (R-152a), or 1,1,1,2,3,3,3-Heptafluoropropane (R-227ea)] with Hydrofluoroolefins [2,3,3,3-Tetrafluoropropene (R-1234yf) or trans-1,3,3,3-Tetrafluoropropene (R-1234ze(E))]

In this article, speed of sound data measured using a dual-path pulse-echo instrument are reported for three binary refrigerant mixtures, R-125/1234yf, R-1234yf/152a, and R-1234ze(E)/227ea, at compositions of (0.33/0.67) and (0.67/0.33) mole fraction. The speed of sound was studied at temperatures ranging from 230 K to 345 K from pressures slightly above the bubble point curve up to 20 MPa for the mixtures containing R-1234yf and 49 MPa for the R-1234ze(E)/227ea mixtures. The relative combined expanded speed of sound uncertainty ranged from 0.039 % to 0.317 % with a mean uncertainty over all state points of less than 0.10 %. The reported data are compared to the most recent mixture models in REFPROP for each blend studied. Comparisons of available mixture models for the R-125/1234yf and R-1234yf/152a blends exhibit average absolute deviation values ranging from 0.10 % to 0.27 %, and the average absolute deviations for R-1234ze(E)/227ea blends range from 0.62 % to 0.94 %. The comparisons show that only minor adjustments are required to the R-125/1234yf and R-1234yf/152a mixture models to represent the speed of sound data within its uncertainty. However, significant adjustments are needed to improve the current mixture models for the R-1234ze(E)/227ea blend. Deficiencies with the R-1234ze(E)/227ea mixture model are not unexpected since it (1) utilizes a pure-fluid EOS R-1234ze(E) that has been shown to inaccurately represent R-1234ze(E) speed of sound values and (2) uses binary interaction parameters for the chemically similar mixture of R-1234yf/227ea.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Strong gravity extruding peaks in speed of sound profiles of massive neutron stars

The speed of sound squared (SSS) s 2 in massive neutron stars (NSs) characterizes not only the stiffness of supradense neutron-rich matter within but also equivalently properties of the curved geometry due to the strong-field gravity and matter-geometry coupling. A peaked density or radius profile of s 2 has been predicted for massive NSs using various NS equation of state (EOS) models. However, the nature, cause, location and size of the peak in s 2 profiles are still very EOS model dependent. In this work, we investigate systematically s 2 profiles in massive NSs in a new approach that is independent of the nuclear EOS model and without any presumption about the NS structure and/or composition. In terms of the small quantities (reduced radius, the energy density and pressure scaled by their central values), we perform double-element perturbative expansions in solving perturbatively the scaled Tolman-Oppenheimer-Volkoff (TOV) equations and analyzing s 2 profiles from the Newtonian limit to the general relativistic (GR) case. The GR term in the TOV equations plays a twofold role: it compresses NS matter and modifies the pressure/energy density ratio from small values in Newtonian stars showing no s 2 peak to large ones for massive NSs possessing a peak in their s 2 profiles, and eventually takes away the peak in extremely compact/massive NSs approaching the causality limit. In particular, the peaked behavior in s 2 is expected to emerge near the center of massive NSs like PSR J⁢0740+6620, while a sharp phase transition is unlikely to occur there. Furthermore, these features revealed from our analyses are universal as they are intrinsic properties of the GR stellar structure equations independent of the still very uncertain EOS of supradense neutron-rich matter in NSs.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2021

Insights on the peak in the speed of sound of ultradense matter

In this work we investigate the minimal physical requirements needed for generating a speed of sound that surpasses its asymptotic conformal limit. It is shown that a peak in the speed of sound of homogeneous matter naturally emerges in the transition from a phase with broken chiral symmetry to one with a gapped Fermi surface. We argue that this could be relevant for understanding the peak in the speed of sound displayed by some of the current models for cold ultradense matter. A minimal model implementation of this mechanism is presented, based on the spontaneous breakdown of an approximate particle-antiparticle symmetry, and its thermodynamic properties are determined.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2024

Analytical insights into the interplay of momentum, multiplicity, and the speed of sound in heavy-ion collisions

We introduce a minimal model of ultracentral heavy-ion collisions to study the relation between the speed of sound of the produced plasma and the final particles' energy and multiplicity. We discuss how the particles' multiplicity N tot and average energy E tot / N tot is related to the speed of sound c s by c s 2 = d ln ( E tot / N tot ) / d ln N tot if the fluid is inviscid, its speed of sound is constant and all final particles can be measured. We show that finite rapidity cuts on the particles' multiplicity N and energy E introduce corrections between c s 2 and d ln ( E / N ) / d ln N that depend on the system's lifetime. We study analytically these deviations with the Gubser hydrodynamic solution, finding that, for ultrarelativistic bosons, they scale as the ratio of the freeze-out temperature T FO over the maximum initial temperature of the fluid T 0 ; the nonthermodynamic aspect of these corrections is highlighted through their dependence on the system's initial conditions. Published by the American Physical Society 2024

Physics↗