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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2

Methods of analyzing microsize particulate aerosols and contaminants.

Methods for analyzing atmospheric aerosols and particulate contaminants from natural and industrial sources are briefly described. Their development was spurred by interest in cosmic dust investigations. These methods make it possible to analyze individual particles ranging in size from 0.01 to 1000 microns for elemental and mineralogical content. The described methods include transmission electron microscopy, scanning electron microscopy, electron probe microanalysis, X-ray diffraction, optical mineralogy, and density measurement.

Blanchard, M. B.↗

Design and fabrication of multigrid X-ray collimators

The paper considers the design and fabrication of multigrid collimators for use in X-ray astronomy. The most important collimator performance criteria are minimum off-band transmission or leakage, and maximum on-band transmission. Lockheed experience with multigrid collimator is summarized: (1) an Oda type with one-dimensional collimation of 1.7 arc minute FWHM and using only the central transmission band, (2) an Oda type with 2 arc minute one-dimensional collimation using up to 27 transmission bands, each separated by 42 arc min. and (3) a modified Parkinson type with two-dimensional collimation of 40 arc sec. Attention is given to grid materials, precision, plating, hole quality, and results of acceptance testing.

Acton, L. W.↗

A real-time electronic imaging system for solar X-ray observations from sounding rockets

A real-time imaging system for displaying the solar coronal soft X-ray emission, focussed by a grazing incidence telescope, is described. The design parameters of the system, which is to be used primarily as part of a real-time control system for a sounding rocket experiment, are identified. Their achievement with a system consisting of a microchannel plate, for the conversion of X-rays into visible light, and a slow-scan vidicon, for recording and transmission of the integrated images, is described in detail. The system has a quantum efficiency better than 8 deg above 8 A, a dynamic range of 1000 coupled with a sensitivity to single photoelectrons, and provides a spatial resolution of 15 arc seconds over a field of view of 40 x 40 square arc minutes. The incident radiation is filtered to eliminate wavelengths longer than 100 A. Each image contains 3.93 x 10 to the 5th bits of information and is transmitted to the ground where it is processed by a mini-computer and displayed in real-time on a standard TV monitor.

Davis, J. M.↗

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherends

Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.

X-ray computed tomography↗

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherents

Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.

bondline thickness↗

Optics and lasers

Report describes twenty-seven optical concepts developed for holographic viewing, spectral transmission, and film camera technology. Articles include developments in laser-Doppler systems, laser beam deflection controls, X-ray photography, and camera components.

Source record↗

Thermochemical Stability of Ca2Yb8(SiO4)6O2 Apatite in Presence of Molten Calcium-Magnesium-Aluminosilicate (CMAS)

Thermochemical stability of ytterbium silicon oxyapatite Ca 2 Yb 8 (SiO 4 ) 6 O 2 (CYbS) in the presence of molten calcium-magnesium aluminosilicate (CMAS) has been investigated at elevated temperatures for consideration as a thermal and environmental barrier coating (T/EBC) material. CYbS apatite powder was synthesized from the constituent oxides via a solid-state reaction method. Hot-pressed apatite substrates were exposed to molten CMAS at 1200, 1300, and 1400 °C for 1, 10, and 50 h. Development of phases in the interaction region of the heat-treated specimens was monitored using scanning electron microscopy, transmission electron microscopy, high-angle annular dark-field imaging, selected area electron diffraction, and energy dispersive x-ray spectroscopy. Monoclinic cyclosilicate Ca 3 Yb 2 (Si 3 O 9 ) 2 formed from interaction of CYbS apatite with CaO in the CMAS melt at the apatite-CMAS reaction front and continued to nucleate and grow within the residual CMAS in diffusion couples annealed for 1 to 50 h at 1200 °C as well as in those heat treated at 1300 °C for 1 h. Residual CMAS was depleted of Ca when cyclosilicate was present. Dendritic wollastonite (CaSiO3) was observed within the residual CMAS in couples annealed at 1200 and 1300 °C. Ingress of molten CMAS, because of its exponential decrease in viscosity, occurred through open pores and along the grain boundaries of the apatite substrates without any detectable chemical reaction at 1300 and 1400 °C. Results of this study indicate that Ca 2 Yb 8 (SiO 4 ) 6 O 2 apatite has the potential to mitigate the CMAS corrosion up to about 1200 °C but not at higher temperatures.

Narottam P Bansal↗

Initial results from the S-056 X-ray telescope on Skylab

The S-056 instrument on Skylab-ATM consists of a glancing incidence X-ray telescope with a camera, five X-ray filters, and two small proportional counters to monitor X-rays from the whole sun in the wavelength range from 2 to 18 A. The telescope reflectivity and filter transmissions limit the photographs to the wavelength ranges from 6 to 18 A and from 27 to 37 A. Hence, the instrument is most useful for the study of active regions and solar activity. Active regions usually have bright cores which often appear as linear features straddling the magnetic field neutral line. A large loop appearing on the west limb in connection with prominence activity on Aug. 13, 1973, was analyzed using proportional counter data and photographs. Crude spectral analysis indicates the loop temperature reached 6 million K and the density was enhanced to a few times that obtained from quiet coronal models. Over a hundred solar flares were photographed during the three Skylab missions. Illustrative examples are discussed for solar flares and other transient coronal phenomena.

Mckenzie, D. L.↗

Determination of volume fraction in multiphase systems using incomplete pole figures

The determination of the volume fraction of a second phase in a multiphase sample by X-ray diffraction becomes more difficult if the diffracting planes have a preferred orientation. Lopata and Kula have described a method of treating this problem using complete pole figures for each of the phases. With some samples, it is not always possible or convenient to obtain data over the full hemisphere. Equations and an example are given which require X-ray data over a limited range of approximately 0 to 75 deg. This can be obtained by reflection without a specially cut sample or transmission data. A series of Legendre polynomials are fitted to data collected while spinning the sample about its normal. An extrapolation is made possible by introducing two conditions on the end points which must be satisfied if the extrapolation functions are to be valid.

Houska, C. R.↗

Effects of diffraction in multiple-grid telescopes for X-ray astronomy

Diffraction effects in modern designs for grid collimator telescopes (assumed to have roughly a 100-micron grid period) are apparent at wavelengths longer than 1 A and are dominant at wavelengths longer than 10 A. In collimators with many grids spaced far apart the effects of diffracation are to reduce strongly the peak transmission of the collimator at longer wavelengths and to broaden it by about the amount expected from Fraunhofer diffraction through a slit the size of the grid openings. Comparisons between two-collimator measurements and the present calculations show reasonable agreement; it is therefore concluded that the present single-collimator calculation gives a good representation of their diffraction-limited angular response.

Lindsey, C. A.↗

Transmission ultrasonography

Review of the results of the application of an advanced signal-processing technique, called time delay spectrometry, in obtaining soft tissue transmission images by transmission ultrasonography, both in vivo and in vitro. The presented results include amplitude ultrasound pictures and phase ultrasound pictures obtained by this technique. While amplitude ultrasonographs of tissue are closely analogous to X-ray pictures in that differential absorption is imaged, phase ultrasonographs represent an entirely new source of information based on differential time of propagation. Thus, a new source of information is made available for detailed analysis.

Heyser, R. C.↗

An exploratory study of the microstructure of mullite fibers

Mullite fibers of three compositions, ranging from SiO2-rich to Al2O3-rich, were investigated by a number of transmission electron microscopy (TEM) techniques. The fibers were examined in the as-received condition and after subjecting them to thermal exposures as high as 142 C. The investigative techniques used included direct TEM of microtomed sections of mounted fibers and TEM of replicas of polished, chemically etched, and cathodically etched fibers. In addition, X-ray diffraction line broadening analyses was used for determining average crystallite size. A preliminary description of the microstructure of mullite fibers is given.

Santoro, G. J.↗

A versatile Mossbauer spectrometer and its applications in vibration measurement

A Fe-57 Mossbauer spectrometer, equally efficient in transmission and reflection geometries, is described. The radiation detector consists of a 1.524- by 5.08 by 5.08-cm rectangular NaI(Tl) crystal with a hole 1.524 cm in diameter. The front and back faces of the crystal are covered with beryllium windows 0.0127 cm thick and 3.81 cm in diameter. The energy of the radiation accepted for counting ranges from 6.3 keV conversion X-rays to the 14.4 keV reemitted gamma rays. The spectrometer was used to measure various types of low frequency (10 Hz) and low amplitude (0.254 mm) periodic motion of steel specimens.

Singh, J. J.↗

A focusing collector for long wavelength X-ray astronomy.

Rocket studies of the low-energy X-ray sky conducted so far suffer from serious experimental problems. Therefore, an apparatus was design ed to overcome the outstanding experimental problems. The instrument developed was successfully flown in an Aerobee-170 rocket. The new device utilizes a grazing incidence paraboloid as an energy concentrator and low-pass filter. The effective bandpass of the instrument from 100 to 280 eV is determined by the combination of the counter window transmission and the mirror reflectivity.

Yentis, D. J.↗

Coded aperture imaging with uniformly redundant arrays

The paper discusses uniformly redundant arrays (URA) as applied to coded aperture imaging. The URA system offers the high-transmission characteristics of random arrays as well as a flat sidelobe advantage. The high-transmission yields the imaging of very low-intensity sources and the flat sidelobes provide the suppression of inherent noise which obscures low-contrast sources. Simulations have shown that the URA with shot and background noise produces a better reconstructed object than random arrays without shot or background noise. The URA also offers an arrangement which involves a mosaic of basic URA patterns forming a circular correlation of the object on the picture plane. Thus the information needed to reconstruct the object is contained in an area equal to that of the basic aperture pattern. This smaller required detector is important in applications including X-ray astronomy.

Fenimore, E. E.↗

Imaging slitless spectrometer for X-ray astronomy

Imaging slitless spectrometer, a combination of an X ray transmission /or reflection/ grating and image-forming X ray telescope, is capable of obtaining simultaneous spatial and spectral information about celestial X ray sources.

Gursky, H.↗

Microscopic observations of X-ray and gamma-ray induced decomposition of ammonium perchlorate crystals

The X-ray and gamma-ray induced decomposition of ammonium perchlorate was studied by optical, transmission, and scanning electron microscopy. This material is a commonly used oxidizer in solid propellents which could be employed in deep-space probes, and where they will be subjected to a variety of radiations for as long as ten years. In some respects the radiation-induced damage closely resembles the effects produced by thermal decomposition, but in other respects the results differ markedly. Similar radiation and thermal effects include the following: (1) irregular or ill-defined circular etch pits are formed in both cases; (2) approximately the same size pits are produced; (3) the pit density is similar; (4) the c face is considerably more reactive than the m face; and (5) most importantly, many of the etch pits are aligned in crystallographic directions which are the same for thermal or radiolytic decomposition. Thus, dislocations play an important role in the radiolytic decomposition process.

Herley, P. J.↗