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NASA NTRS2015

Advances in Astromaterials Curation: Supporting Future Sample Return Missions

NASA's Astromaterials, curated at the Johnson Space Center in Houston, are the most extensive, best-documented, and leastcontaminated extraterrestrial samples that are provided to the worldwide research community. These samples include lunar samples from the Apollo missions, meteorites collected over nearly 40 years of expeditions to Antarctica (providing samples of dozens of asteroid bodies, the Moon, and Mars), Genesis solar wind samples, cosmic dust collected by NASA's high altitude airplanes, Comet Wild 2 and interstellar dust samples from the Stardust mission, and asteroid samples from JAXA's Hayabusa mission. A full account of NASA's curation efforts for these collections is provided by Allen, et al [1]. On average, we annually allocate about 1500 individual samples from NASA's astromaterials collections to hundreds of researchers from around the world, including graduate students and post-doctoral scientists; our allocation rate has roughly doubled over the past 10 years. The curation protocols developed for the lunar samples returned from the Apollo missions remain relevant and are adapted to new and future missions. Several lessons from the Apollo missions, including the need for early involvement of curation scientists in mission planning [1], have been applied to all subsequent sample return campaigns. From the 2013 National Academy of Sciences report [2]: "Curation is the critical interface between sample return missions and laboratory research. Proper curation has maintained the scientific integrity and utility of the Apollo, Antarctic meteorite, and cosmic dust collections for decades. Each of these collections continues to yield important new science. In the past decade, new state-of-the-art curatorial facilities for the Genesis and Stardust missions were key to the scientific breakthroughs provided by these missions." The results speak for themselves: research on NASA's astromaterials result in hundreds of papers annually, yield fundamental discoveries about the evolution of the solar system (e.g. [3] and references contained therein), and serve the global scientific community as ground truth for current and planned missions such as NASA's Dawn mission to Vesta and Ceres, and the future OSIRIS REx mission to asteroid Bennu [1,3]

Evans, C. A.↗
NASA NTRS2016

Curating NASA's Past, Present, and Future Astromaterial Sample Collections

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (hereafter JSC curation) is responsible for curating all of NASA's extraterrestrial samples. JSC presently curates 9 different astromaterials collections in seven different clean-room suites: (1) Apollo Samples (ISO (International Standards Organization) class 6 + 7); (2) Antarctic Meteorites (ISO 6 + 7); (3) Cosmic Dust Particles (ISO 5); (4) Microparticle Impact Collection (ISO 7; formerly called Space-Exposed Hardware); (5) Genesis Solar Wind Atoms (ISO 4); (6) Stardust Comet Particles (ISO 5); (7) Stardust Interstellar Particles (ISO 5); (8) Hayabusa Asteroid Particles (ISO 5); (9) OSIRIS-REx Spacecraft Coupons and Witness Plates (ISO 7). Additional cleanrooms are currently being planned to house samples from two new collections, Hayabusa 2 (2021) and OSIRIS-REx (2023). In addition to the labs that house the samples, we maintain a wide variety of infra-structure facilities required to support the clean rooms: HEPA-filtered air-handling systems, ultrapure dry gaseous nitrogen systems, an ultrapure water system, and cleaning facilities to provide clean tools and equipment for the labs. We also have sample preparation facilities for making thin sections, microtome sections, and even focused ion-beam sections. We routinely monitor the cleanliness of our clean rooms and infrastructure systems, including measurements of inorganic or organic contamination, weekly airborne particle counts, compositional and isotopic monitoring of liquid N2 deliveries, and daily UPW system monitoring. In addition to the physical maintenance of the samples, we track within our databases the current and ever changing characteristics (weight, location, etc.) of more than 250,000 individually numbered samples across our various collections, as well as more than 100,000 images, and countless "analog" records that record the sample processing records of each individual sample. JSC Curation is co-located with JSC's Astromaterials Research Office, which houses a world-class suite of analytical instrumentation and scientists. We leverage these labs and personnel to better curate the samples. Part of the cu-ration process is planning for the future, and we refer to these planning efforts as "advanced curation". Advanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new types of collections as envi-sioned by NASA exploration goals. We are (and have been) planning for future cu-ration, including cold curation, extended curation of ices and volatiles, curation of samples with special chemical considerations such as perchlorate-rich samples, and curation of organically- and biologically-sensitive samples.

Zeigler, R. A.↗
NASA NTRS2017

Research-Grade 3D Virtual Astromaterials Samples: Novel Visualization of NASA's Apollo Lunar Samples and Antarctic Meteorite Samples to Benefit Curation, Research, and Education

NASA's vast and growing collections of astromaterials are both scientifically and culturally significant, requiring unique preservation strategies that need to be recurrently updated to contemporary technological capabilities and increasing accessibility demands. New technologies have made it possible to advance documentation and visualization practices that can enhance conservation and curation protocols for NASA's Astromaterials Collections. Our interdisciplinary team has developed a method to create 3D Virtual Astromaterials Samples (VAS) of the existing collections of Apollo Lunar Samples and Antarctic Meteorites. Research-grade 3D VAS will virtually put these samples in the hands of researchers and educators worldwide, increasing accessibility and visibility of these significant collections. With new sample return missions on the horizon, it is of primary importance to develop advanced curation standards for documentation and visualization methodologies.

Blumenfeld, E. H.↗
NASA NTRS2018

Overview of the Digitization Workflow Post Image Acquisition of Apollo Lunar and Antarctic Meteorite Samples Using Agisoft Photoscan for the NASA 3D Astromaterials Virtual Samples Collection

The 3D Virtual Astromaterials Samples (3DVAS) collection is a multi-year funded project to create a digital database of sixty Apollo Lunar and Antarctic Meteorite samples following non-destructive documentation conservation protocols. After initial image processing, the photos are evaluated and processed using unique structure-from-motion photogrammetric techniques in a high performance modelling software designed to create a 3D model from 2D images: Agisoft Photoscan Pro. Agisoft Photoscan Pro uses image processing algorithms and techniques originating in computer vision to resolve 3D models for accurate and detailed visualization of a subject. The software provides a stepwise process that is tailored per model based on spatial and specular reflectance properties, for example. The process includes: photo alignment, creation of a dense point cloud, mesh, and finally texture. Photo alignment is dependent on model properties. The 3DVAS process requires a special rotation platform with calibrated photogrammetric targets, specific distance rotation protocols, and a contrasting background for alignment and scale accuracy. As a result of the photographic process, alignment will complete with two mirrored hemispheres that, in a sense, represent the 2D images overlapping to create a 3D model. Each dense point cloud is analyzed with provided statistical measures in a gradual selection process to eliminate outliers. The point cloud is reduced to include only data valuable to the final model. When a precise dense point cloud is achieved, a mesh and texture are applied. Each model is scaled with scale bar accuracies within 100 microns. Each sample has its own intimate process for modelling; there is no standard for the parameters required in the final creation of a high resolution model. By processing multiple samples, a skill is gained in practice to allow a close definition of the original sample and will result in the most detailed version of the sample shell. This process completes one-fifth of the 3DVAS protocol for providing accurate digital documentation. Each model shell is merged with X-ray Computed Tomography data to create a full volumetric sample. All 3DVAS data will be served on NASA's Astromaterials Acquisition and Curation website with an early subset of data available in 2019 and the 3D Virtual Astromaterials Samples Collection launch in 2020.

Thomas, Andi B.↗
NASA NTRSDate not supplied

The NASA Facility for Astromaterials Research at the Johnson Space Center – A National Laboratory for Planetary Research

The Astromaterials Research and Exploration Science (ARES) Division at the NASA Johnson Space Center houses a unique combination of laboratories, instruments, infrastructure, technical ex-pertise, and other assets for conducting broad-based world-class planetary research. These facilities have been accessed for decades by hundreds of external scientists, including faculty, post-docs, students, and interns, most at no cost and on a collaborative basis. With funding through NASA’s Planetary Science Enabling Facilities (PSEF) program, we have estab-lished the NASA Facility for Astromaterials Research (NFAR) to expand access to and enhance these labora-tories for a diverse and inclusive external user base, thus maximizing the science return from research funded by R&A programs in NASA’s Planetary Sci-ence Division (PSD). NFAR enables cutting edge planetary sample analyses, making new scientific dis-coveries possible, in addition to training the next-generation of planetary scientists. NFAR laboratories are co-located with JSC Curation that houses all NASA-controlled astromaterials collections, thus ena-bling direct access to both research and curation exper-tise, to facilitate specialized sample handling and anal-ysis of allocated samples (from JSC and other sample collections) to PIs, particularly those affiliated with institutions that historically have limited or no access to in-house analytical or experimental facilities.

J Filiberto↗
NASA NTRSDate not supplied

The Nasa Facility for Astromaterials Research at the Johnson Space Center – A National Laboratory for Planetary Research.

The Astromaterials Research and Exploration Science (ARES) Division at the NASA Johnson Space Center has established the NASA Facility for Astromaterials Research (NFAR) through the NASA Planetary Science Enabling Facilities program. NFAR is designed to provide access to our unique combination of laboratories, instruments, infrastructure, and technical expertise for conducting broad-based world-class planetary research. NFAR enables direct access to both research and curation expertise, to facilitate specialized sample handling and analysis of astromaterials and planetary analog materials. NFAR users from institutions that historically have limited access to or lack in-house analytical or experimental facilities are particularly encouraged to apply. We issue three calls for user proposals each year due the last day of April, July, and November. We award NFAR research projects to users in a competitive peer-reviewed proposal process. NASA-funded research in active PSD R&A proposals is prioritized along with requests from early-career/next-generation scientists, under-represented minorities, and those PIs from minority serving institutions. There is no cost to use the analytical facility, but researchers are required to be in person for analyses. Proposals to use NFAR labs are limited to < 5 pages and focus on the scientific purpose of the investigation and its relevance to NASA PSD, the labs to be accessed, and the time needed for the investigation. More information can be found at: https://ares.jsc.nasa.gov/research/nasa-facility-astromaterials-research/.

J. Filiberto↗
NASA NTRSDate not supplied

The NASA Facility for Astromaterials Research at the Johnson Space Center – A National Laboratory for Planetary Research

The Astromaterials Research and Exploration Science (ARES) Division at the NASA Johnson Space Center has established the NASA Facility for Astromaterials Research (NFAR) through the NASA Planetary Science Enabling Facilities program. NFAR is designed to provide access to our unique combination of laboratories, instruments, infrastructure, and technical expertise for conducting broad-based world-class planetary research. NFAR enables direct access to both research and curation expertise, to facilitate specialized sample handling and analysis of astromaterials and planetary analog materials. NFAR users from institutions that historically have limited access to or lack in-house analytical or experimental facilities are particularly encouraged to apply. We award NFAR research projects to users in a competitive peer-reviewed proposal process. Proposals to use NFAR labs are limited to <5 pages and focus on the scientific purpose of the investigation and its relevance to NASA Planetary Science Division (PSD) objectives, the labs to be accessed, and the time needed for the investigation. There is no deadline for proposals, and proposals will be reviewed on a rolling basis. NASA-funded research in active PSD R&A proposals is prioritized along with requests from early-career/next-generation scientists, under-represented minorities, and to Principal Investigators from minority-serving institutions. More information on the NFAR labs and preparing and submitting a proposal can be found at: https://ares.jsc.nasa.gov/research/nasa-facility-astromaterials-research/.

E. Rampe↗
NASA NTRS2024

The NASA Facility for Astromaterials Research at the Johnson Space Center – A National Laboratory for Planetary Research

The Astromaterials Research and Exploration Science (ARES) Division at the NASA Johnson Space Center houses a unique combination of laboratories, instruments, infrastructure, technical expertise, and other assets for conducting broad-based world-class planetary research. These facilities have been accessed for decades by hundreds of external scientists, including faculty, post-docs, students, and interns, most at no-cost and on a collaborative basis. With funding through NASA’s Planetary Science Enabling Facilities (PSEF) program, we have established the NASA Facility for Astromaterials Research (NFAR) to expand access to and enhance these laboratories for a diverse and inclusive external user base, focusing on training of the next generation of scientists and, thus, maximizing the science return from research funded by R&A programs in NASA’s Planetary Science Division (PSD). NFAR enables new planetary sample analyses, making new scientific discoveries possible, including training the next generation of planetary scientists. NFAR laboratories are co-located with JSC Curation that houses the NASA-controlled astromaterials collections, thus enabling direct access to both research and curation expertise, to facilitate specialized sample handling and analysis of allocated samples to sample PIs, particularly those affiliated with institutions that historically have limited access to or lack in-house analytical or experimental facilities.

J. I. Simon↗
NASA NTRS2010

Comparison of the Mineralogy of Comet Wild 2 Coma Grains to Other Astromaterials

We propose that Kuiper Belt samples (in this case comet coma grains from the Jupiter family comet Wild 2) are recognizably different from the bulk of materials in outer belt asteroids, because of their different formation positions and times in the early solar system. We believe this despite similarities found between some Wild 2 grains and components of carbonaceous chondrites (i.e. some CAI and chondrules). Kuiper Belt samples must preserve measurable mineralogical and compositional evidence of formation at unique positions and times in the early solar nebula, and these formational differences must have imparted recognizable special characteristics. We hypothesize that these characteristics include: (1) Unique major element compositional ranges of common astromaterial minerals, especially olivine and pyroxene; (2) Unique minor element compositions of major silicate phases, especially olivine and low-Ca pyroxene; (3) Degree and effects of radiation processing -- including amorphous rims, metal coatings, and Glass with Embedded Metal and Sulfides (GEMS); (4) Presence of abundant presolar silicate grains as recognized by anomalous oxygen in silicates; (5) Oxidation state of the mineral assemblage. We are working our way through all available Wild 2 samples, selecting 1-2 non-consecutive viable TEM grids from each possible extracted Wild 2 grain. We especially prefer TEM grids from grains for which complete mineralogical details have not been published (which is to say the majority of the extracted grains). We are performing a basic mineralogic survey by E-beam techniques, to establish the essential features of the extracted Wild 2 grains. We are making a particular effort to carefully and accurately measure minor elements of olivine and pyroxene, as these minerals are widespread in astromaterials, and comparisons of their compositions will serve to place the Wild 2 silicates in contact with asteroids, meteorites and chondritic interplanetary dust particles processing. We are also making a special effort to search for mineralogical products of aqueous alteration, since their presence would reveal that Wild 2 was once internally heated, a result with dramatic implications for models of early solar system primitive bodies. Thus far carbonates are the only potential evidence for aqueous alteration for Wild 2.

Frank, David↗
NASA NTRS2013

Robotic Sample Manipulator for Handling Astromaterials Inside the Geolab Microgravity Glovebox

Future human and robotic sample return missions will require isolation containment systems with strict protocols and procedures for reducing inorganic and organic contamination. Robotic handling and manipulation of astromaterials may be required for preliminary examination inside such an isolation containment system. In addition, examination of astromaterials in microgravity will require constant contact to secure samples during manipulation. The National Space Grant Foundation exploration habitat (XHab) academic innovative challenge 2012 administered through the NASA advanced exploration systems (AES) deep space habitat (DSH) project awarded funding to the University of Bridgeport team to develop an engineering design for tools to facilitate holding and handling geological samples for analysis in a microgravity glovebox environment. The Bridgeport XHab team developed a robotic arm system with a three-finger gripper that could manipulate geologic samples within the existing GeoLab glovebox integrated into NASA's DSH called the GeoLab Robotic Sample Manipulator (see fig. 1 and 2). This hardware was deployed and tested during the 2012 DSH mission operations tests [1].

Bell, Mary S.↗
NASA NTRS2013

Nondestructive Analysis of Astromaterials by Micro-CT and Micro-XRF Analysis for PET Examination

An integral part of any sample return mission is the initial description and classification of returned samples by the preliminary examination team (PET). The goal of the PET is to characterize and classify returned samples and make this information available to the larger research community who then conduct more in-depth studies on the samples. The PET tries to minimize the impact their work has on the sample suite, which has in the past limited the PET work to largely visual, nonquantitative measurements (e.g., optical microscopy). More modern techniques can also be utilized by a PET to nondestructively characterize astromaterials in much more rigorous way. Here we discuss our recent investigations into the applications of micro-CT and micro-XRF analyses with Apollo samples and ANSMET meteorites and assess the usefulness of these techniques in future PET. Results: The application of micro computerized tomography (micro-CT) to astromaterials is not a new concept. The technique involves scanning samples with high-energy x-rays and constructing 3-dimensional images of the density of materials within the sample. The technique can routinely measure large samples (up to approx. 2700 cu cm) with a small individual voxel size (approx. 30 cu m), and has the sensitivity to distinguish the major rock forming minerals and identify clast populations within brecciated samples. We have recently run a test sample of a terrestrial breccia with a carbonate matrix and multiple igneous clast lithologies. The test results are promising and we will soon analyze a approx. 600 g piece of Apollo sample 14321 to map out the clast population within the sample. Benchtop micro x-ray fluorescence (micro-XRF) instruments can rapidly scan large areas (approx. 100 sq cm) with a small pixel size (approx. 25 microns) and measure the (semi) quantitative composition of largely unprepared surfaces for all elements between Be and U, often with sensitivity on the order of a approx. 100 ppm. Our recent testing of meteorite and Apollo samples on micro-XRF instruments has shown that they can easily detect small zircons and phosphates (approx. 10 m), distinguish different clast lithologies within breccias, and identify different lithologies within small rock fragments (2-4 mm soil Apollo soil fragments).

Zeigler, R. A.↗
NASA NTRS2014

High-Resolution Imaged-Based 3D Reconstruction Combined with X-Ray CT Data Enables Comprehensive Non-Destructive Documentation and Targeted Research of Astromaterials

Providing web-based data of complex and sensitive astromaterials (including meteorites and lunar samples) in novel formats enhances existing preliminary examination data on these samples and supports targeted sample requests and analyses. We have developed and tested a rigorous protocol for collecting highly detailed imagery of meteorites and complex lunar samples in non-contaminating environments. These data are reduced to create interactive 3D models of the samples. We intend to provide these data as they are acquired on NASA's Astromaterials Acquisition and Curation website at http://curator.jsc.nasa.gov/.

Blumenfeld, E. H.↗
NASA NTRS2014

Astromaterials Research Office (KR) Overview

The fundamental goal of our research is to understand the origin and evolution of the solar system, particularly the terrestrial, "rocky" bodies. Our research involves analysis of, and experiments on, astromaterials in order to understand their nature, sources, and processes of formation. Our state-of-the-art analytical laboratories include four electron microbeam laboratories for mineral analysis, four spectroscopy laboratories for chemical and mineralogical analysis, and four mass spectrometry laboratories for isotopic analysis. Other facilities include the experimental impact laboratory and both 1-atm gas mixing and high-pressure experimental petrology laboratories. Recent research has emphasized a diverse range of topics, including: Study of the solar system's primitive materials, such as carbonaceous chondrites and interplanetary dust; Study of early solar system chronology using short-lived radioisotopes and early nebular processes through detailed geochemical and isotopic characterizations; Study of large-scale planetary differentiation and evolution via siderophile and incompatible trace element partitioning, magma ocean crystallization simulations, and isotopic systematics; Study of the petrogenesis of Martian meteorites through petrographic, isotopic, chemical, and experimental melting and crystallization studies; Interpretation of remote sensing data, especially from current robotic lunar and Mars missions, and study of terrestrial analog materials; Study of the role of organic geochemical processes in the evolution of astromaterials and the extent to which they constrain the potential for habitability and the origin of life.

Draper, David S.↗
NASA NTRS2016

Engaging Students, Teachers, and the Public with NASA Astromaterials Research and Exploration Science (ARES) Assets

Engaging students, teachers, and the public with NASA Astromaterials Research and Exploration Science (ARES) assets, including Science, Technology, Engineering and Mathematics (STEM) experts and NASA curation astromaterial samples, provides an extraordinary opportunity to connect citizens with authentic aspects unique to our nation's space program. Effective engagement can occur through both virtual connections such as webcasts and in-person connections at educator workshops and public outreach events. Access to NASA ARES assets combined with adaptable resources and techniques that engage and promote scientific thinking helps translate the science and research being facilitated through NASA exploration, elicits a curiosity that aims to carry over even after a given engagement, and prepares our next generation of scientific explorers.

Graff, P. V.↗
NASA NTRS2017

Using Virtual and In-Person Engagement Opportunities to Connect K-12 Students, Teachers, and the Public With NASA Astromaterials Research and Exploration Science Assets

Engaging K-12 students, teachers, and the public with NASA Astromaterials Research and Exploration Science (ARES) assets provides an extraordinary opportunity to connect audiences with authentic aspects unique to our nation's space program. NASA ARES has effectively engaged audiences with 1) Science, Technology, Engineering and Mathematics (STEM) experts, 2) NASA specialized facilities, and 3) NASA astromaterial samples through both virtual and in-person engagement opportunities. These engagement opportunities help connect local and national audiences with STEM role models, promote the exciting work being facilitated through NASA's Science Mission Directorate, and expose our next generation of scientific explorers to science they may be inspired to pursue as a future STEM career.

Graff, P.↗
NASA NTRS2018

Perserving Samples and Their Scientific Integrity - Insights into MSR from the Astromaterials Acquisition and Curation Office at NASA Johnson Space Center

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (JSC), in Houston, TX (henceforth Curation Office) manages the curation of all past, present, and future extraterrestrial samples returned by NASA missions and shared collections from international partners, preserving their integrity for future scientific study while providing the samples to the international community in a fair and unbiased way. The Curation Office also curates flight and non-flight reference materials and other materials from spacecraft assembly of sample return missions that would have the potential to cross-contaminate a present or future NASA astromaterials collection. These materials are primarily collected during the assembly, test, and launch operations (ATLO) phase and after flight during the recovery and curation phase. In addition, the Curation Office curates non-flight, flight-like, and flown witness plates for sample return missions. These reference materials and witness plates provide the scientific community with the fundamental ability to reconstruct the contamination/alteration history of the sample collection through the course of the mission, with the overall goal of strengthening the scientific conclusions drawn from the study of returned materials.

Harrington, A. D.↗
NASA NTRS2018

The Astromaterials X-Ray Computed Tomography Laboratory at Johnson Space Center

The Astromaterials Acquisition and Cura-tion Office at NASA's Johnson Space Center (hereafter JSC curation) is the past, present, and future home of all of NASA's astromaterials sample collections. JSC curation currently houses all or part of nine different sample collections. Our primary goals are to maintain the long-term integrity of the samples and ensure that the samples are distributed for scientific study in a fair, timely, and responsible manner, thus maximizing the return on each sample. Part of the curation process is planning for the future, thus we also perform funda-mental research in advanced curation initiatives. Ad-vanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new types of sample collections, or getting new results from existing sample collections [1]. As part of these ad-vanced curation efforts we are augmenting our analyti-cal facilities.

Zeigler, R. A.↗
NASA NTRS2019

Generating Excitement and Increasing Awaressness of NASA Planetary Science and Astromaterials Assets

Students, educators, the public, and the scientific community are so often inspired by NASA science and exploration. Millions have joined NASA during live mission event broadcasts and also follow NASA on social media. Exploration of worlds in our solar system enable the scientific community to obtain and analyze data that provide clues to better understand the history and evolution of our solar system. Missions that collect and return samples to Earth from a target solar system body provide scientists with samples they can research and analyze in their laboratories. For those who are not planetary scientists, they may not understand the significance of these samples and/or the importance of sample return missions. The Astromaterials Research and Exploration Science (ARES) Science Engagement team, through work supported by NASA’s Science Mission Directorate (SMD) Science Education Cooperative Agreement Notice NNH15ZDA004C, provides access to samples from NASA’s Astromaterials Collections through NASA sponsored exhibits at educator and scientific conferences, NASA relevant public outreach events, and collaborations with other Science Activation Teams supported by the SMD Cooperative Agreement Notice. The goal of this work is to generate excitement while enhancing knowledge and awareness of NASA’s unique assets, thus highlighting NASA planetary science and exploration.

Graff, P. V.↗