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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2

Development of Oxidation Resistant Coatings on GRCop-84 Substrates by Cold Spray Process

GRCop-84, a Cu-CR-Nb alloy, has been developed for rocket engine liner applications. For maximum life additional oxidation protection is required to prevent blanching. NiCrAlY was identified as a suitable coating, and efforts were initiated to develop suitable coating techniques. Cold spray is one technique under consideration. Efforts at ASB Industries to produce dense, adherent coatings are detailed. The work culminated in the production of samples for testing at NASA Glenn Research Center.

Karthikeyan, J.↗

Fabrication technology: A compilation

Devices and techniques are presented for cutting, shaping, and forming metals. Metal fabrication and coating techniques are discussed. Patent information is presented.

Source record↗

Protective coatings for columbium applied in the field.

The various aspects of field repair of columbium alloy panels with protective coatings designed as part of the Space Shuttle thermal protection system are examined. The field repair of the coatings is accomplished by employing ceramic cement repairs, and reapplying the fused slurry silicide coating. Techniques are described which improve the practicality of these repairs by employing torch heating. The repair coating quality is demonstrated by testing which simulates flight temperature, pressure, stress and acoustic vibration conditions as a function of time. Conclusions on the present status of field repair coatings are presented and recommendations are given for appropriate future activities relative to the use on an operational Space Shuttle system.

Carter, J.↗

Preparation and Characterization of Space Durable Polymer Nanocomposite Films from Functionalized Carbon Nanotubes

Low color, flexible, space durable polyimide films with inherent, robust electrical conductivity have been under investigation as part of a continuing materials development activity for future NASA space missions involving Gossamer structures. Electrical conductivity is needed in these films to dissipate electrostatic charge build-up that occurs due to the orbital environment. One method of imparting conductivity is through the use of single walled carbon nanotubes (SWNTs). However, the incompatibility and insolubility of the SWNTs severely hampers their dispersion in polymeric matrices. In an attempt to improve their dispersability, SWNTs were functionalized by the reaction with an alkyl hydrazone. After this functionalization, the SWNTs were soluble in select solvents and dispersed more readily in the polymer matrix. The functionalized SWNTs were characterized by Raman spectroscopy and thermogravimetric analysis (TGA). The functionalized nanotubes were dispersed in the bulk of the films using a solution technique. The functionalized nanotubes were also applied to the surface of polyimide films using a spray coating technique. The resultant polyimide nanocomposite films were evaluated for nanotube dispersion, electrical conductivity, mechanical, and optical properties and compared with previously prepared polyimide-SWNT samples to assess the effects of SWNT functionalization.

Delozier, D. M.↗

Fogging technique used to coat magnesium with plastic

Cleaning process and a fogging technique facilitate the application of a plastic coating to magnesium plates. The cleaning process removes general organic and inorganic surface impurities, oils and greases, and oxides and carbonates from the magnesium surfaces. The fogging technique produces a thin-filmlike coating in a clean room atmosphere.

Mroz, T. S.↗

Solventless LARC-160 Polyimide Matrix Resin

The addition polyimide, LARC-160, which was originally synthesized from low cost liquid monomers as a laminating resin in ethanol, was prepared as a solventless, high viscosity, neat liquid resin. The resin was processed by hot-melt coating techniques into graphite prepreg with excellent tack and drape. Comparable data on graphite reinforced laminates made from solvent-coated and various hot-melt coated prepreg were generated. LARC-160, because of its liquid nature, can be easily autoclave processed to produce low void laminates. Liquid chromatographic fingerprints indicate good reaction control on resin scale ups. Minor changes in monomer ratios were also made to improve the thermal aging performance of graphite laminates.

Stclair, T. L.↗

The scratch test - Different critical load determination techniques

Different critical load determination techniques such as microscopy, acoustic emission, normal, tangential, and lateral forces used for scratch test evaluation of complex or multilayer coatings are investigated. The applicability of the scratch test to newly developed coating techniques, systems, and applications is discussed. Among the methods based on the use of a physical measurement, acoustic emission detection is the most effective. The dynamics ratio between the signals below and above the critical load for the acoustic emission (much greater than 100) is well above that obtained with the normal, tangential, and lateral forces. The present commercial instruments are limited in load application performance. A scratch tester able to apply accurate loads as low as 0.01 N would probably overcome most of the actual limitations and would be expected to extend the scratch testing technique to different application fields such as optics and microelectronics.

Sekler, J.↗

SP-100 high-temperature advanced radiator development

The development of an advanced radiator concept design meeting SP-100 thermoelectric requirements is reported. Carbon-carbon heat pipes are used to produce this lightweight, high-performance radiator. Two feasibility problems had to be solved to enable the design: the production of a carbon-carbon heat pipe tube with integral fins, and the development of a coating that protects the carbon-carbon substrate from 875-K potassium working fluid. Carbon-carbon tubes with integral fins were successfully produced using a T-300 fiber, an angle interlocking weave architecture, and pitch densification. A barrier coating to protect the inside diameter of these tubes which employed the CVD of niobium over a thin rhenium interlayer was developed. The rhenium interlayer proved to be critical to the success of this coating technique by providing a gradation in the coefficient of thermal expansion, carrying a portion of the induced stress load, improving coating adhesion, and providing a partial carbon diffusion barrier.

Rovang, Richard D.↗

Shock interference peak heating measurements using phase change coatings

The phase change coating technique is used to obtain peak heating measurements in shock interference flow regions with high surface shear and heating. This technique provides heat transfer coefficients which are determined by measuring the time for a point on the surface to reach the phase change temperature of the thin fusible coating. Measurements were conducted on a 5.08-cm diameter hemisphere-cylinder made of silica based epoxy at Mach 6 for free stream Reynolds numbers of 3.3 to 25.6 million per meter. A sketch of the shock interference pattern produced by a flat plate shock generator is included. Heating data obtained on a 5.08-cm diameter stainless steel hemispherical model instrumented with thermocouples is presented for the purpose of comparing the phase change technique with the thermocouple-calorimeter technique.

Keyes, J. W.↗

Aluminized alloy boosts turbine blade life

Description of an aluminized alloy coating technique that involves first the application of a ductile, oxidation-resistant overlay, such as NiCrAl, which is then partially aluminized. The duplex protective system has performance advantages over conventional aluminide coatings in that it provides higher-temperature hot corrosion resistance over a longer service life.

Gedwill, M. A.↗

Vacuum Sputtered and Ion-Plated Coatings for Wear and Corrosion Protection

The plasma or ion-assisted coating techniques such as sputtering and ion plating are discussed in view of wear and corrosion protection. The basic processes and the unique features of the technique are discussed in regard to the synthesis and development of high reliability wear and corrosion resistant films. The ions of the plasma which transfer energy, momentum, and charge to the substrate and the growing films can be beneficially used. As a result, coating adherence and cohesion is improved. Favorable morphological growth such as high density and porosity-free films can be developed, and residual stresses can be reduced.

Spalvins, T.↗

Space optics: Imaging X-ray optics workshop; Proceedings of the Seminar, Huntsville, Ala., May 22-24, 1979

The papers in this volume are broadly based and represent a comprehensive summary of past achievements, new designs, techniques and future plans in space optics. The design, construction, testing and use of grazing incidence optics have played an integral role in the advance of X-ray astronomy. Topics of interest include a cosmic X-ray telescope for ARIES rocket observations, quest for ultrahigh resolution in X-ray optics, optical coating techniques for Wolter-type substrates, astronomical applications of grazing incidence telescopes with polynomial surfaces, and a paraboloidal X-ray telescope mirror for solar coronal spectroscopy.

Weisskopf, M.↗

New techniques for far-infrared filters.

The techniques considered make it possible to construct high performance low-pass wide-band, and medium-band filters at wavelengths in the range from 25 to 300 micrometers. Short wavelength rejection without appreciable loss at long wavelengths is achieved by means of small particle scattering. Spectral definition in the far infrared is obtained by cooling one or more crystalline materials to liquid-He or liquid-nitrogen temperatures. The problem of reflection losses at the various surfaces is solved by a new antireflection coating technique.

Armstrong, K. R.↗

Thin wing corrections for phase-change heat-transfer data.

Since no methods are available for determining the magnitude of the errors incurred when the semiinfinite slab assumption is violated, a computer program was developed to calculate the heat-transfer coefficients to both sides of a finite, one-dimensional slab subject to the boundary conditions ascribed to the phase-change coating technique. The results have been correlated in the form of correction factors to the semiinfinite slab solutions in terms of parameters normally used with the technique.

Hunt, J. L.↗

Hypersonic aerothermal characteristics of a manned low finenes ratio shuttle booster

An investigation of a winged booster model having canards and an ascent configuration comprised of the booster mounted in tandem with an orbiter model has been conducted at Mach 10.2 in the continuous flow hypersonic tunnel. Longitudinal and lateral directional force characteristics were obtained over angle of attack ranges of -12 deg to 60 deg for the booster and -11 deg to 11 deg for the ascent configuration. Interference heating effects on the booster using the phase-change coating technique were determined at 0 deg angle of attack. Some oil flow photographs of the isolated booster and orbiter and ascent configuration are also presented.

Bernot, P. T.↗

Effect of wing sweep, angle of attack, Reynolds number, and wing root fillet on the interference heating to the wing windward surface of an entry vehicle configuration

The phase-change-coating technique was used to study the interference heating to the windward surface of 14 deg, 25 deg, and 50 deg swept wings of an entry vehicle configuration. One wing root of each model was faired to the fuselage with a fillet. Tests were made at Mach 8 at angles of attack of 0 deg, 20 deg, 40 deg, and 60 deg and at free-stream Reynolds numbers based on model length of 0.47 and 1.7 million. Bow shock impingement heating was found to increase in magnitude and affected area with increasing angle of attack until at a higher angle of attack it decreases; this angle of attack is lower for a 50 deg swept wing. Wing root interference heating was found to increase with angle of attack up to 40 deg and then to remain approximately constant. Consequently, wing root interference heating becomes the major type of interference heating at large angles of attack, and this occurs at a lower angle of attack for the highest sweep angle. A wing leading-edge root fillet reduces the peak in wing root interference heating near the leading edge, and increasing Reynolds number increases the level of interference heating.

Clark, L. E.↗

Heat transfer tests of the NASA-MSC space shuttle configuration at the Langley Research Center Mach 8 Variable Density Facility

The experimental investigations performed on the NASA-Manned Spacecraft Center Space Shuttle orbiter and booster configurations at a Mach 8 variable density facility are presented. The test program was a series of aerothermodynamic wind tunnel tests that were run over a range of angles of attack, yaw angles, and Reynolds numbers. Objectives of the test program were to obtain heat transfer data over the NASA-Manned Spacecraft Center Space Shuttle orbiter, booster, and launch configurations for a range of angles of attack from - 20 to + 30 deg, yaw angles of 0 and + or - 6 deg, and Reynolds numbers of 0.6, 2.0, and 3.7 x one million. The phase-change coating technique was used to obtain heat transfer data. Information received from these tests will be instrumental in performing thermal protection systems studies and vehicle aerodynamic design.

Connor, L. E.↗