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Physical Background, Computations and Practical Issues of the Magnetohydrodynamic Pressure Drop in a Fusion Liquid Metal Blanket

In blankets of a fusion power reactor, liquid metal (LM) breeders, such as pure lithium or lead-lithium alloy, circulate in complex shape blanket conduits for power conversion and tritium breeding in the presence of a strong plasma-confining magnetic field. The interaction of the magnetic field with induced electric currents in the breeder results in various magnetohydrodynamic (MHD) effects on the flow. Of them, high MHD pressure losses in the LM breeder flows is one of the most important feasibility issues. To design new feasible LM breeding blankets or to improve the existing blanket concepts and designs, one needs to identify and characterize sources of high MHD pressure drop, to understand the underlying physics of MHD flows and to eventually define ways of mitigating high MHD pressure drop in the entire blanket and its sub-components. This article is a comprehensive review of earlier and recent studies of MHD pressure drop in LM blankets with a special focus on: (1) physics of LM MHD flows in typical blanket configurations, (2) development and testing of computational tools for LM MHD flows, (3) practical aspects associated with pumping of a conducting liquid breeder through a strong magnetic field, and (4) approaches to mitigation of the MHD pressure drop in a LM blanket.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

TRITIUM TRANSPORT MODELING AT THE PORE SCALE IN CERAMIC BEEDER MATERIALS USING TMAP8

Fusion reactors depend on the blanket material to breed and release tritium at the same rate or faster than it is consumed by the fusion reaction. Cellular ceramic breeders are dense materials that can maintain a high tritium breeding ratio while promoting tritium release thanks to highly connected pores. Assessing the tritium breeding capabilities of these materials requires a combination of extensive experimental and modeling efforts. In this work, we develop and calibrate a multiphysics model of tritium transport. This novel model accounts for ceramic and pore diffusion, trapping and detrapping, and several surface reactions at the pore surface. We perform a sensitivity analysis and calibrate the model by comparing its predictions against experimental measurements of deuterium absorption. The calibrated model is then used to model tritium absorption in samples with different pore microstructures to investigate the effect of pore interconnectivity on tritium absorption. The model is part of the development of the multiscale, multiphysics framework for tritium transport (i.e., the Tritium Migration Analysis Program [TMAP8]), which is itself built on top of the finite element multiphysics framework MOOSE. This study demonstrates some of TMAP8’s capabilities, and is the first step toward assessing the tritium breeding capabilities of ceramic breeder material designs.

08 HYDROGEN↗

MHD Analysis of Dual-Coolant Lead-Lithium Blanket for Spherical Tokamak Advanced Reactor

The tritium breeding blanket is vital for future fusion power plants, with the Spherical Tokamak Advanced Reactor (STAR) project highlighting the dual-coolant lead-lithium (DCLL) design. The DCLL blanket performs shielding, energy exhaust, and tritium breeding using a lead-lithium alloy , with lithium as the breeder and lead as the neutron multiplier. It also serves as the primary coolant, with helium providing supplemental cooling. Reduced-activation ferritic/martensitic steel is used for the blanket structure. Magnetohydrodynamic (MHD) phenomena influence the liquid metal flow in a magnetic field, affecting heat transfer in the breeder affected by energetic neutrons. Understanding key flow parameters in such conditions is critical for efficient DCLL design. This study uses three-dimensional thermofluid MHD analysis with ANSYS CFX software, modified at Princeton Plasma Physics Laboratory, to simulate high Hartmann flows. The neutronics code MCNP, coupled with plasma equilibrium, provides heat source distribution. In conclusion, we examine electromagnetic interactions in adjacent fluid domains and analyze the magnetic field’s impact on flow distribution in the inboard and outboard blanket layout, using detailed mesh generation for accurate results.

DCLL↗

Investigation of Anchor Link Magnetohydrodynamic Effects in the Toroidally Symmetric Lead-Lithium (TSLL) Blanket Concept

This paper presents a comprehensive study on the magnetohydrodynamic (MHD) flow in a slotted channel with a cylindrical anchor link, which is an imperative component of the toroidally symmetric lead-lithium (TSLL) blanket concept. Following the validation of the MHD solver implemented in COMSOL and a proposed subtraction approach to compute the anchor link pressure drop, the effects of computational domain size on the pressure drop and velocity distribution are examined. The results show that the pressure drop associated with the anchor link and the maximum flow velocity follow an asymptotic trend as the domain width increases, with wall-induced pressure drop being more dominant than that of the anchor link. The velocity distribution analysis revealed the formation of an internal boundary layer extending along the magnetic field direction, which is a unique feature of the investigated MHD flow. An estimation of the total MHD pressure drop associated with the array of anchor links under the TSLL blanket conditions suggests ~0.3 MPa, which is significantly lower than the recommended maximum allowable blanket pressure drop of 2 MPa. In conclusion, this work offers valuable insights into the anchor link–associated MHD phenomena and serves as a foundation for further development of the TSLL blanket concept for future fusion reactors.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Construction of 3D MHD pressure drop correlation and flow characterization in the contraction region of a fusion blanket manifold

Inlet and outlet manifolds are typical components of liquid metal (LM) blanket designs of a fusion power reactor to be used to distribute the LM flow into breeding channels and collect it at the exit of the blanket. High pressure loss in the magnetohydrodynamic (MHD) flows featuring abrupt geometrical changes is one of the main feasibility issues of such designs. Recently, optimization studies were conducted to construct 3D MHD pressure drop correlations for a LM flow in an electrically insulating manifold with gradual expansion. Here, the 3D computational approach developed in that study is applied to the outlet manifold featuring gradual contraction. A systematic analysis was performed with a total number of 135 flow cases computed with COMSOL Multiphysics for Hartmann numbers 1000 < Ha < 10,000, Reynolds numbers 100 < Re < 12,000, and contraction angles 45° < θ < 75° for a fixed contraction ratio of 4. The effects of Ha, Re and θ on the flow recirculation, development length and the total pressure drop were carefully examined. A linear regression analysis was used to determine the power rule of pressure drop coefficient k related to Ha and Re, demonstrating a good match with the Ludford layer theory. Eventually, a correlation for the 3D MHD pressure drop coefficient was constructed as a function of Ha, Re and θ. Further, the results were compared against the inlet manifold. It was found that the flow in the inlet manifold exhibits larger recirculation zones. In the investigated range of Ha, Re and θ, the pressure drop coefficient k of the LM MHD flow in the gradual contraction is only slightly lower (< 8 %) than that in the gradual expansion.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Density Functional Theory Analysis of Candidate Tritium Permeation Barriers for Vanadium Alloys as a Fusion Structural Material

Vanadium alloys are being considered as a candidate structural material for the breeder blanket component of future fusion reactors due to their good thermal conductivity, low activation, and chemical compatibility with FLiBe. However, vanadium has a high hydrogen solubility, resulting in hydrogen diffusion and trapping in the vanadium structural alloy and lower than expected tritium breeding ratios. To mitigate the permeation of hydrogen into the structural alloy, a tritium permeation barrier will be coated onto the vanadium alloy. Multiple materials have been proposed as candidate tritium permeation barriers, but the extent to which each of these materials impacts hydrogen diffusion and trapping is still unknown. In this project, we perform atomic-scale calculations to narrow down the list of potential tritium permeation barrier candidates and to understand the mechanisms through which hydrogen diffusion is affected in these materials.

36 MATERIALS SCIENCE↗

SOFE2023 Presentation: "Tritium Safety and Sensitivity Analysis of Tritium Extraction eXperiment (TEX) PbLi Loop Using MELCOR-TMAP"

The efficient extraction of tritium from the breeder blanket (BB) in a fusion reactor is vital for maintaining the tritium economy for a sustainable and self-sufficient fusion power plant. The vacuum permeator (VP) design is one of several promising technology platforms for extracting tritium from the BB with the advantages of being capable of operating continuously at high temperatures with the aim of achieving high tritium extraction efficiencies. The Tritium Extraction eXperiment (TEX), under construction at the Safety and Tritium Applied Research (STAR) Facility at Idaho National Laboratory (INL), is designed to test the viability of VP technology by introducing atomic hydrogen (H, D, and T) from a source permeator (SP) into a forced convection lead lithium eutectic (PbLi) loop and determining the hydrogen extraction rates from the vanadium VP. Presented here is a computational analysis of the hydrogen inventory and permeation behavior in TEX using the hydrogen transport and accident analysis code MELCOR-TMAP developed at INL. The results of a sensitivity analysis based on MELCOR-TMAP simulations of hydrogen extraction efficiencies from the TEX test section using varying PbLi flow rates, hydrogen source rates from the SP, and material property uncertainties are also reported. Operation scenarios for TEX in consideration of the analyses based on results from MELCOR-TMAP are discussed.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Initial Neutronics Investigation of a Chlorine Salt-Based Breeder Blanket

Tritium breeding blankets within D-T-fueled fusion reactors contain lithium compounds and typically require neutron multiplier materials to achieve a tritium breeding ratio (TBR) consistent with self-sustaining operation. Liquid breeder blankets have some advantages over solid blankets, and previous blanket studies have investigated liquid metal as well as liquid salt–based blankets. Liquid salts have reduced magnetohydrodynamic effects as compared to liquid metals, but typically have a lower TBR. Recently, advanced fission reactor concepts have considered chloride-based salts in their design, and there is a significant amount of research work occurring to study these salts. Chloride salts have previously been considered for fusion reactors, but studies have typically found lower breeding ratios than for fluoride salts, such as 2(LiF)-BeF 2 (flibe) so they have not been further developed. In this work, we use a one-dimensional cylindrical radiation transport model of a conceptual tokamak fusion reactor to investigate the neutronics feasibility of using a chloride salt–based blanket that uses chlorine enriched in 37 Cl, which has both a low capture cross section and a substantial (n,2n) cross section. It is found that chloride salts (LiCl mixed with BeCl 2 and/or PbCl 2 ) can potentially achieve a ~3% to 5% higher TBR than fluoride molten salts, notably flibe, in the absence of a solid multiplier. Including a solid multiplier, however, does narrow this advantage, with TBRs estimated within ~1% of flibe with a 2-cm Be multiplier. Chloride salts can also reach lower melting points than flibe, potentially improving the scope for the use of reduced activation ferritic-martensitic steel as a structural material. There is substantial uncertainty in the calculations driven by limited thermochemical data for the Cl salts, plus cross-section uncertainties. The production of 36 Cl through 35 Cl(n,g) and 37 Cl(n,2n) has the potential to challenge the waste disposal rating of the blanket. Calculations indicate that, while this is not an immediate showstopper, this case depends upon the exact waste disposal rating criteria used for 36 Cl. Further work could reduce these uncertainties with improved thermochemical data, higher-fidelity modeling for downselected salts, and more refined waste disposal calculations and regulatory guidance. Lastly, it must be recognized that, as for all molten salts, corrosion and chemistry can present appreciable technical challenges that require further assessment in developing a practical blanket concept, and also that the enrichment of chlorine presents an additional technical and supply chain challenge.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Design and Assessments of Liquid Metal Systems for a Fusion Power Reactor

This three-year research program at UCLA builds on the Fusion Engineering System Study (FESS) and has the major goal of identifying and accessing the most critical MHD/Mass & Heat Transfer phenomena associated with LM MHD flows in fusion breeding/cooling applications. The computed results and their analyses provide a strong basis to overcome present design limitations and will eventually lead to feasible, more effective solutions for LM systems of a fusion power reactor, such as breeding blankets and LM plasma facing components (PFCs). The project focuses on three research thrusts: Identification and characterization of the most important generic issues common to LM breeders (hereinafter called “Blanket”: ~47% of the resources); Design, implementation and assessments of two LM breeding-blanket concepts, DCLL and HCLL, for particular fusion devices, such as the US Fusion Nuclear Science Facility (FNSF) or the Fusion Pilot Plant (FPP) (hereinafter called “System Studies”: ~40% of the resources); Design and analysis of LM (Li) divertor concepts for FNSF or FPP, including scoping and detailed 2D and 3D computations (hereinafter called “LM PFC”: ~13% of the resources).

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Conceptual Design for a Blanket Tritium Extraction Test Stand

Future fusion reactors must be able to breed the tritium they will consume. Several breeding and tritium extraction technologies are under investigation internationally. PbLi is of particular interest as a breeder material. A new forced convection PbLi loop, the Tritium Extraction eXperiment (TEX), is being designed and constructed to investigate tritium extraction from PbLi. Specifically, TEX will serve to investigate the extraction efficiency of various vacuum permeator membranes and configurations. The major components of the loop include a moving magnet pump, reverse permeator, furnace test section, analysis chamber, supply tank, and plenum. As significant hazards are present in such experiments, safety is an integral focus of the experimental design.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Extension of OpenMC for Fixed Source Transmutation Calculations

This report documents work performed under a Strategic Partnership Project between Argonne National Laboratory (ANL) and the United Kingdom Atomic Energy Authority (UKAEA). The overall goal of this project is to extend OpenMC [1], a community-developed Monte Carlo particle transport code, to be able to perform fixed-source transmutation calculations. In fission and fusion reactors, the high flux of energetic neutrons causes materials within the reactor to “transmute,” or undergo a nuclear reaction that results in the addition/removal of neutrons and protons from the nucleus of an atom. If subjected to these reactions for long enough, the overall composition and physical properties of the material itself begin to change as a result of transmutation. Such a feature is vital for predicting the decrease in tritium production rate within a breeder blanket during the lifetime of a fusion reactor. OpenMC is capable of simulating neutron transport in fission/fusion systems, thereby allowing it to estimate the flux that causes transmutation. It is also capable of solving the transmutation equations, which determine how the composition of a material changes over time due to neutron irradiation and radioactive decay. However, solving the transmutation equations was previously only possible when the source of neutrons came from a fission system. In a fusion system, the source of neutrons is typically determined by a separate code and then given as an input to the particle transport simulation. This is known as a fixed source calculation. Through this project, we have extended OpenMC to solve the transmutation equations for a fixed source calculation. Evaluating the change in material compositions due to transmutation and its effect on physical properties is of key importance to a range of engineering analyses for fission and fusion systems. For example, in a fusion reactor, estimating the dose rate at different physical locations resulting from irradiated materials in the reactor allows designers to ensure that workers are not exposed to doses beyond applicable regulations. In order to properly dispose of irradiated materials, designers also need to estimate the radiotoxicity, which again relies on knowledge of the material composition at some future time. The specific tasks for this project that were agreed to between ANL and UKAEA were as follows: 1. Make changes and additions in the openmc.deplete and related modules in OpenMC to support transmutation calculations following a fixed source transport simulation. 2. Make necessary changes to OpenMC to model transmutation due to an arbitrary set of reactions needed for fusion applications. Use this new capability to generate a depletion chain file based on the TENDL nuclear data library. 3. Improve the openmc.deplete module in OpenMC to keep track of gases produced as a by-product of nuclear reactions during transmutation calculations. 4. Validate the new capabilities by carrying out fixed-source transmutation calculations on a suitable benchmark problem using OpenMC and a comparable Monte Carlo neutron transport code.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

The Maintainable Fusion Pilot Plant

The US fusion community has coalesced around the goal of building an FPP as described by the National Academies of Science, Engineering, and Medicine (NASEM). In addition to demonstrating the viability of the technologies necessary to operate such a plant, including demonstration of net energy and electricity production, NASEM found that a “fusion pilot plant will need to demonstrate the ability to efficiently perform remote maintenance and replacement in support of the design of a power plant, taking into account details of the consequences of the fusion environment, such as material activation and tritium retention in components.” Current designs of fusion demonstration reactors do usually foresee a regular exchange of their first wall modules, including the tritium breeding blankets. In the European Power Plant Conceptual Studies, it is assumed that a fusion reactor will need to change its divertor every 2 years and its first wall blanket module every 5 to 6 years to reach acceptable availability. Underlying this capability are remote-handling technologies to keep the outage for the exchange of these components short. There are many uncertainties in the remote-handling schemes, and most schemes are at a preconceptual level at best. In addition, the exchange of these components would either produce an enormous rad-waste stream or would require an enormous refurbishment activity with huge cost-prohibitive hot-cells. Past Fusion Nuclear Science Facility (FNSF) preconceptual studies have led to hot cell dimensions of an unbelievable size, likely costing tens of billions of dollars. Already at The Way (previously International Thermonuclear Experimental Reactor, ITER), hot-cells have become cost-prohibitive, demanding redesigns of the ITER first wall to reduce the toxic rad-waste/inventory. In this in-situ PFC repair project, a concept for a long-life, maintainable first wall module concept is developed and tested. This first wall concept relies on innovative remote handling to repair the first wall modules in-situ, avoiding costly refurbishments outside of the tokamak vessel. This approach was highlighted in the Fusion Energy Sciences Advisory Committee (FESAC) report on Transformative Enabling Capabilities for Efficient Advance Toward Fusion Energy. In general, the damage of the first wall armor is due to particle and radiation exposures. Load conditions vary from one fusion reactor design to another. In tokamaks, first wall Plasma Facing Components (PFCs) are exposed to far-Scrape-Off-Layer plasma fluxes, electromagnetic radiation, energetic CX neutrals, and potentially runaway electron beams. Protecting the first wall to the worst-case load conditions would require the design of a very thick first wall armor. Transient heat and particle fluxes due to disruptions or edge localized modes can lead to excessive heat loads resulting potentially in melting PFCs down to the cooling channel. Catastrophic events like these need to be avoided by appropriate disruption mitigation systems. However, failure of these systems will still put a first wall at an unacceptable risk. Hence, a first wall design needs to accommodate the occasional transient heat loads by introducing sacrificial limiters, which will absorb these transients.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

MHD flow in liquid metal blankets: Major design issues, MHD guidelines and numerical analysis

The design of breeding blankets represents the major challenge for fusion reactor engineering because of performance requirements and severe operating conditions in terms of heat load and neutron flux. Liquid metal alloys such as lead-lithium, due to their lithium content, can be used to breed tritium, one of the plasma fuel components, and owing to their high thermal conductivity, they may serve as coolants. On the other hand, there are technical issues related to the fact that the liquid metals are electrically conducting and interact with the plasma-confining magnetic field. Induced electric currents and generated electromagnetic forces affect velocity and pressure distribution in the blankets. Magnetohydrodynamic (MHD) flows for fusion applications have been often investigated in simplified geometries, such as pipes, ducts, bends, with focus on their fundamental features. These analyses are essential, since results remain valid as background for the development of blanket designs, even when a concept is dismissed. However, the conceptual study of fusion blankets requires to take into account the global multiple effects, that arise when the full system is considered. Progress made in fusion-related MHD research results from combined numerical and experimental activities. In this paper we review and summarize features of 2D and 3D MHD flows that are typical in liquid metal blankets, together with available correlations for MHD pressure losses. This knowledge can provide simple design MHD guidelines that support a preliminary estimate of MHD effects in a blanket concept, in terms of pressure drop and flow distribution.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Effects of HFIR neutron irradiation on fracture toughness properties of standard and Ni-doped F82H

F82H is the Japanese reference reduced-activation ferritic-martensitic (RAFM) steel for fusion blanket applications. The harsh environment of a fusion reactor, such as neutron irradiation and He/H damage, can result in significant degradation of F82H fracture toughness. Therefore, understanding the fracture toughness behavior of F82H in the fusion environment is critical to ensure the long-term safe operation of the fusion reactor. Here, we summarize seven irradiation campaigns of the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL) covering five variants of F82H steels, including F82H IEA, F82H Mod3, F82H doped with 1.4% natural Ni, F82H doped with 1.4% 58 Ni, and F82H doped with 1.4% 60 Ni. The irradiation temperatures covered the range from 220 °C to 530 °C and the neutron irradiation dose spanned 4 dpa to 70 dpa. The effects of neutron irradiation temperature, dose, materials composition, Ni doping, and He production on F82H fracture toughness are discussed. Our results showed that irradiation embrittlement monotonically decreased with increasing irradiation temperature until 400 °C for F82H IEA and F82H Mod3. F82H Mod3 showed better fracture toughness than F82H IEA both before and after neutron irradiation. We determined that 1.4% Ni alloying can be applied to F82H for simulating He effect in a fission reactor without jeopardizing the fracture toughness of the material. However, more studies are needed to understand the effect of high dose (>20 dpa) and He production on F82H fracture toughness.

36 MATERIALS SCIENCE↗

Computational Fluid Dynamics Analysis of the Molten Salt Tritium Transport Experiment Test Section

Tritium, a radionuclide produced through neutron capture by lithium and other elements (beryllium and fluoride) in molten salts, presents unique challenges to radionuclide release. This is true for both fusion energy breeder blankets and molten salt fission reactors. The fundamental understanding of tritium transport is crucial to the safe design and operation of these reactors. The Molten Salt Tritium Transport Experiment (MSTTE), currently under construction at Idaho National Laboratory, aims to investigate tritium transport phenomena using a forced-convection fluoride salt loop. This loop is designed to study various transport mechanisms, such as permeation through metals and gas-liquid interactions, and is intended to support future research on tritium extraction units. A critical aspect of the MSTTE loop design is ensuring a fully developed velocity profile before the fluid reaches the permeation test section where measurements are made. This study employs computational fluid dynamics to model the salt flow behavior within the MSTTE permeation test section. A realizable k-ε turbulent model with enhanced wall treatment is used to simulate the single-phase, vertical upward flow of molten salt FLiNaK under isothermal conditions. The simulation results indicated flow distortion and underdeveloped profiles at all planned flow rates within the test section due to the 85-deg sharp bend. To address this issue, a reduced diameter with a reducer and expander and a flow conditioner are investigated to achieve fully developed flow. The analysis showed that the flow conditioner successfully corrected the flow profile, achieving fully developed behavior at a flow rate of 50 liters per minute (LPM). In conclusion, this research enhances our understanding of flow dynamics in molten salt systems and contributes to optimizing tritium transport control technologies.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Blanket Modeling with Tritium Accountancy using MELCOR-Fusion

Fusion devices require a "blanket" of materials that generate tritium during production to provide the source of tritium for the fusion device. We use MELCOR for fusion to demonstrate a blanket model of an ARC-class reactor with a liquid immersion blanket. We discuss major sources of uncertainty and describe ongoing experimental efforts to reduce the uncertainty.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

History, present status, and future directions of vanadium alloys for fusion reactors

Since the need for low-activation fusion reactor materials was recognized in the mid-1980s, vanadium alloys have been researched and developed as promising candidates for blanket structural materials. Vanadium alloys are non-ferromagnetic and ductile materials and thus have advantages different from other candidates. However, since vanadium alloys are still at a premature industrial stage, research and development have been carried out not only on issues specific to fusion reactors but also on those related to industrial materials. Blankets using vanadium alloys as structural materials and liquid Li as a tritium breeder and coolant (self-cooled V/Li blankets) have unique characteristics, and research and development of issues specific to V/Li blankets have been conducted in conjunction with the development of vanadium alloys. In this paper, the progress of this research and development is reviewed, and the remaining issues are pointed out. As a result, the future direction of vanadium alloy research and development is discussed, considering recent changes in the environment surrounding fusion energy.

Liquid Li blanket↗

Influence of fatigue precracking and specimen size on Master Curve fracture toughness measurements of EUROFER97 and F82H steels

EUROFER97 and F82H steels are two leading reduced-activation ferritic-martensitic (RAFM) steels for fusion first wall and blanket applications. Exposure to the harsh environment of fusion reactors can result in severe degradation of fracture toughness. Thus, the post-irradiation evaluation of fracture toughness is critical for understanding the material behavior. Due to the space constraints of irradiation facilities and challenges in controlling a uniform irradiation condition for large size specimens, the development of small specimen test techniques (SSTT) is indispensable to evaluate the performance of irradiated materials. In this study, we evaluated specimen size effects on the Master Curve fracture toughness of EUROFER97 and F82H steels. A wide variety of specimens, including 0.5 T compact tension (C(T)) specimens, 0.16 T mini-compact tension (miniC(T)) specimens, and 1.65 mm miniature bend bar specimens, were tested. The testing methodology was based on the Master Curve method in the ASTM E1921 standard. No specimen size effect was observed in 0.5 T C(T) and 0.16 T miniC(T) specimens on the Master Curve reference temperature T0, while 1.65 mm miniature bend bar specimens yielded a higher T 0Q . A strong effect of fatigue precracking on T 0 for 0.5 T C(T) and 0.16 T miniC(T) specimens was observed, such that testing on specimens with skewed fatigue precrack fronts resulted in lower T 0 than for specimens with ASTM standard qualified straight fatigue precrack fronts. The results highlight the importance of experimental quality control in developing SSTT for Master Curve fracture toughness testing. Lastly, we also evaluated and provided recommendations on the minimum number of specimens needed for each specimen type for yielding reliable T 0Q values.

36 MATERIALS SCIENCE↗