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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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267 records · Page 2

Behaviors of Lunar Regolith Simulant Under Varying Gravitational Conditions

Understanding the behavior of regolith in varying gravity conditions is critical for space exploration and future missions. In this work, the gravity-driven hopper flow of lunar regolith simulant in different gravitational accelerations (terrestrial, lunar) is first observed experimentally. Numerical simulations (DEM) are then developed to understand the role which cohesive inter-particle forces play in such gravity-driven flow, using the theoretical framework of granular Bond number. Qualitative comparison between a terrestrial experiment and numerical simulation validated this framework. Following that, we numerically studied the dynamic behavior under varying gravitational conditions (from terrestrial to lunar to asteroid gravitational accelerations). We find that this behavior is extremely sensitive to the interplay of the gravity conditions and the attractive/cohesive forces among particles. The numerical and experimental results show that the complex interaction of these forces can drastically change the dynamics of the material producing effects relevant for variable gravity applications.

Soft Matter

Battery Failure Databank

The Battery Failure Databank contains thermal runaway results gathered from nearly 300 small format fractional thermal runaway calorimetry (S-FTRC) experiments. A majority of these experiments were conducted at synchrotron facilities where high-speed x-ray videography was conducted of the cell while tested inside of the S-FTRC. The databank is a two-component system which consists of a Microsoft ExcelTM spreadsheet which provides S-FTRC results in tabular format and a radiographic video library containing the high-speed x-ray videos. Overall, the databank provides thermal results from S-FTRC experiments conducted on a mixture of commercially available lithium-ion (Li-ion) cells and specialized Li-ion test cells with varying cell format (18650, 21700, and D-cell) and trigger mechanism (heaters, heaters plus internal short circuiting device, and nail penetration). The radiography video component provides insight into the initiation and propagation of TR in the cells, in addition to consequences of TR measured by the FTRC. Fractions of mass ejected for the cell types are separated into regimes based on the different failure modes of the cells, such as purely venting, partial ejection, and total ejection. With knowledge of the rate and characterization of the internal degradation of the cells during TR, and the amounts of mass ejected and unrecovered, the extent of TR, and therefore the mitigation of TR, is revealed relative to cell types and failure modes.

Lithium-ion battery

Lunar Electrical Conductivity, Permeability and Temperature From Apollo Magnetometer Experiments

Magnetometers have been deployed at four Apollo sites on the Moon to measure remanent and induced lunar magnetic fields. Measurements from this network of instruments have been used to calculate the electrical conductivity, temperature, magnetic permeability, and iron abundance of the lunar interior. The measured lunar remanent fields range from 3 gammas (γ) minimum at the Apollo 15 site to 327 γ maximum at the Apollo 16 site. Simultaneous magnetic field and solar plasma pressure measurements show that the remanent fields at the Apollo 12 and 16 sites interact with, and are compressed by, the solar wind. Remanent fields at Apollo 12 and Apollo 16 are increased 16 γ and 32 γ, respectively, by a solar plasma bulk pressure increase of 1.5 x 10 -7 dynes/cm 2 . Global lunar fields due to eddy currents, induced in the lunar interior by magnetic transients, have been analyzed to calculate an electrical conductivity profile for the Moon. From nightside magnetometer data in the solar wind it has been found that deeper than 170 km into the Moon the conductivity rises from 3 x 10 -4 mhos/m to 10 -2 mhos/m at 1000-km depth. Recent analysis of data obtained in the geomagnetic tail, in regions free of complicating plasma effects, yields results consistent with nightside values. Conductivity profiles have been used to calculate the lunar temperature for an assumed lunar material of olivine. In the outer layer (~ 170 km thick) the temperature rises to 110° C, after which it gradually increases with depth to 1500° C at a depth of ~ 1000 km. Simultaneous measurements by magnetometers on the lunar surface and in orbit around the moon are used to construct a whole-moon hysteresis curve, from which the global lunar magnetic permeability is determined to be μ = 1.012 ± 0.006. The corresponding global induced dipole moment is 2 x 10 18 gauss-cm 3 for typical inducing fields of 10 -4 gauss in the lunar environment. Lunar free iron abundance corresponding to the global permeability is determined to be 2.5 ± 2.0 wt. %. Total iron abundance (sum of iron in the ferromagnetic and paramagnetic states) is calculated for two assumed compositional models of the lunar interior. For a free iron/orthopyroxene lunar composition the total iron content is calculated to be 12.8 ± 1.0 wt. %; for a free iron/olivine composition, total iron content is 5.5 ± 1.2 wt. %. Other lunar models with an iron core and with a shallow iron-rich layer are also discussed in light of the measured global lunar permeability. Velocities and thicknesses of the Earth's magnetopause and bow shock have been estimated from simultaneous magnetometer measurements. Average speeds are determined to be about 50 km/s for the magnetopause and 70 km/s for the bow shock, although there are large variations in the measurement for any particular boundary crossing. Corresponding measured boundary thicknesses average about 2300 km for the magnetopause and 1400 km for the bow shock.

P Dyal

Development and application of a 3-D geometry/mass model for LDEF satellite ionizing radiation assessments

A computer model of the three dimensional geometry and material distributions for the LDEF spacecraft, experiment trays, and, for selected trays, the components of experiments within a tray was developed for use in ionizing radiation assessments. The model is being applied to provide 3-D shielding distributions around radiation dosimeters to aid in data interpretation, particularly in assessing the directional properties of the radiation exposure. Also, the model has been interfaced with radiation transport codes for 3-D dosimetry response predictions and for calculations related to determining the accuracy of trapped proton and cosmic ray environment models. The methodology is described used in developing the 3-D LDEF model and the level of detail incorporated. Currently, the trays modeled in detail are F2, F8, and H12 and H3. Applications of the model which are discussed include the 3-D shielding distributions around various dosimeters, the influence of shielding on dosimetry responses, and comparisons of dose predictions based on the present 3-D model vs those from 1-D geometry model approximations used in initial estimates.

B. L. Colborn

Protein Crystal Growth Results From the United States Microgravity Laboratory-1 Mission

Protein crystal growth experiments have been performed by this laboratory on 18 Space Shuttle missions since April, 1985. In addition, a number of microgravity experiments also have been performed and reported by other investigators. These Space Shuttle missions have been used to grow crystals of a variety of proteins using vapor diffusion, liquid diffusion, and temperature-induced crystallization techniques. The United States Microgravity Laboratory - 1 mission (USML-1, June 25 - July 9, 1992) was a Spacelab mission dedicated to experiments involved in materials processing. New protein crystal growth hardware was developed to allow in orbit examination of initial crystal growth results, the knowledge from which was used on subsequent days to prepare new crystal growth experiments. In addition, new seeding hardware and techniques were tested as well as techniques that would prepare crystals for analysis by x-ray diffraction, a capability projected for the planned Space Station. Hardware that was specifically developed for the USML-1 mission will be discussed along with the experimental results from this mission.

L J Delucas

Lunar and Planetary X-Ray Diffraction Program: Progress Report of Research and Instrument Development, July 1964 to March 1965

The Lunar and Planetary X-Ray Diffraction Program consists of three concurrent efforts aimed at rapid development of a first-generation flight-instrument system, evaluation of potential advances in diffractometer components for a possible second-generation instrument, and full investigation of the capabilities and limitations of rock analysis by X-ray diffraction. More complete descriptions of each of these studies are given below; the papers which follow are grouped according to these subjects in Sections II through V.

PETROLOGY

Next-Generation Hard X-ray Missions: SuperHERO and HEROIX

High-energy X-ray observations have transformed our understanding of astrophysical systems where non-thermal processes dominate, from shock-accelerated particles in supernova remnants to relativistic jets and hot coronae in active galactic nuclei. NuSTAR’s pioneering focusing images of the hard X-ray sky have demonstrated the immense scientific potential of this band, while also highlighting how limited angular resolution constrains our ability to fully characterize complex physical processes in faint extended sources and resolving faint sources in crowded sky regions. In this presentation, I will discuss a pathway to overcome these challenges through NASA Marshall Space Flight Center’s replicated NiCo full-shell X-ray mirror technology. Specifically, I will discuss the SuperHERO hard X-ray telescope to achieve better than 10-arcsecond half-power diameter (HPD) angular resolution on a balloon flight observing the Crab Nebula, and the High EneRgy Observatory for Imaging X-rays (HEROIX) Medium-Class Mission concept to achieve an integrated effective area of 570 cm2 at 30 keV with 5 arcsec HPD angular resolution.

AGN

High EneRgy Observatory for Imaging X-rays (HEROIX) Mission Concept

The High EneRgy Observatory for Imaging X-rays (HEROIX) is a next-generation broadband X-ray space telescope concept under development as a Medium-Class Explorer mission. Building on more than three decades of replicated NiCo shell technology at NASA’s Marshall Space Flight Center, HEROIX will deliver 5 arcsecond half-power-diameter imaging resolution in the hard X-ray band. The observatory will incorporate four co-aligned telescopes with advanced multilayer coatings, extending the bandpass into the hard X-ray regime and providing an integrated effective area of 380 cm² at 30 keV. A suite of focal plane detectors will enable imaging capability throughout its 1–80 keV bandpass. This combination of angular resolution and high-energy coverage will open new windows into non-thermal processes in extreme astrophysical environments. HEROIXwill deliver transformative science, advancing the astrophysics community’s understanding of supernova physics, the X-ray binary population of the Galactic Center, accretion-driven galaxy evolution, and the origin of the Cosmic X-ray Background.

Nick Thomas

X-Ray Polarization From the Atoll 4U 1735−44 Suggests a Low Inclination

X-ray polarimetry is a new tool capable of probing the geometry of accretion onto weakly magnetized neutron stars. Here we present the first X-ray spectro-polarimetric results from coordinated observations of the atoll source 4U 1735−44, conducted with the Imaging X-ray Polarimetry Explorer (IXPE), NICER, and NuSTAR . Over the 2–8 keV energy range, we obtained a marginal detection of polarization with the polarization degree of 1.4% ± 0.7% and polarization angle of −29◦ ± 14◦, corresponding to a 3σ upper limit on the polarization degree of 3.5%. The best-fit model to describe the spectrum comprises a thermal component associated with the accretion disk, a Comptonized black body component, and a relativistic reflection component. From the reflection model, we infer a disk inclination of ∼40◦. The spectroscopic and polarimetric properties of 4U 1735−44 are consistent with those observed in other atoll sources studied by IXPE, with its low polarization likely due to its low inclination

X-rays: binaries

X-Ray Polarization of Z-Type Neutron Star Low-Mass X-Ray Binaries II. Spectropolarimetric Analysis

IXPE has provided for the first time detailed energy- and time-resolved X-ray polarimetry of Z-type neutron star low-mass X-ray binaries (NS-LMXBs) as they move along their color-color diagrams (CCDs). These sources can reach the highest polarization observed for NS-LXMBs in the 2–8 keV range when they move along the horizontal branch. In a previous paper, we characterized the spectral state of a sample of Z-sources using the CCD and estimated the polarization with model-independent analysis. Here, we present detailed spectropolarimetric analysis for each source on each branch using data from IXPE, NICER, and NuSTAR. The continuum X-ray emission of all the sources is well described with a combination of thermal accretion disk emission plus a harder Comptonized component. In addition, reflection features, in particular the relativistically broadened Fe Kα line, are observed for our sources, except GX 5–1. For most of the sources and branches, the main contribution to the X-ray emission and polarization is due to Comptonization: moving from the horizontal branch (HB) to the normal branch (NB), the polarization degree (PD) in the 2–8 keV band varies from about 6% to 3–4%, while the PD is loosely constrained in the flaring branch (FB), due to the shorter exposures. These PD values are significantly higher than theoretical expectations for typical spreading or boundary layer configurations. The polarization of the disk is generally lower (below 3%) but still higher than predictions for an electron scattering-dominated, plane-parallel atmosphere above the disk observed at the corresponding inclination. Moreover, the polarization angle (PA) of the disk seems to be significantly misaligned and not perpendicular to that of Comptonization. We find no correlation between the polarization signal and the inclination, nor with the contribution of reflected photons throughout the Z-track.

accretion

Toward Large Field-of-view X-ray Spectrometers with Magnetic Microcalorimeters

A future X-ray telescope mission like Lynx, a X-ray flagship mission concept, requires a large field of view, high energy resolution, and high spatial resolution. The Magnetic Microcalorimeter (MMC) detectors we are developing for such a mission feature a 5-arcminute field of view, approximately 100,000 pixels, each spanning 0.5–1 arcsecond. These detectors require the readout of 8,000 sensors. Three different array types have been designed to meet scientific goals, two of which utilize thermal multiplexing to reduce the number of readout channels in a scheme called “Hydra.” We are currently fabricating detectors on a recently completed buried wiring wafer with connections to every sensor. The sensors are read out using a microwave multiplexer (μMUX) with flux ramp modulation. A single μMUX can read out approximately 1,000 sensors with only two feed lines. We will report on the test of the first two-dimensional μMUX chip, consisting of 78 resonators. μMUX chips that pass screening will be directly bonded to MMC array chips using indium bump bonding. In parallel, we have tested a kinetic inductance traveling wave parametric amplifier (KI-TWPA) to amplify signals at low temperatures. The KI-TWPA exhibits extremely low internal noise, approaching the standard quantum limit. Since the energy resolution of an MMC is primarily limited by the readout system, the KI-TWPA is an ideal amplifier for MMCs with μMUX readout. We recently measured the readout noise of a μMUX with a KI-TWPA, demonstrating its capability for reading out MMC arrays. We present the design and fabrication of the latest MMC detectors, along with its readout performance.

Magntic Microcalorimeters

SuperHERO X-ray Telescope Balloon Mission

The SuperHERO hard X-ray telescope will observe extended sources at unprecedented imaging resolution, revealing the origins of non-thermal emission in extreme astrophysical environments. Employing NASA Marshall Space Flight Center’s replicated NiCo full-shell X-ray mirror technology to achieve better than 10-arcsecond half-power diameter (HPD) angular resolution on a balloon platform, SuperHERO consists of seven identical, co-aligned telescopes with a combined effective area of 45 cm² at 30 keV. SuperHERO was selected in the APRA 2023 call as a five-year mission, with an inaugural two-day flight scheduled from Fort Sumner, New Mexico, in the fall of 2028. For its initial target, SuperHERO will observe the Crab pulsar wind nebula, localizing hard X-ray emission. Mission development is currently underway, with updates and status to be provided in this presentation.

Nick Thomas

X-Ray Absorption Spectroscopy in High Temperature Oxidation of Metals and Alloys

An experimental technique is described that allows for the joint study of the kinetics and of the oxide structure during the high temperature oxidation of metal surfaces. Oxygen is supplied at the metal through an electrochemical oxygen pump and the oxygen pressure, at the metal surface, is measured during oxidation by a YSZ (yttria stabilized zirconia) oxygen sensor. XAS (x-ray absorption spectroscopy) is performed in fluorescence mode at the cation K edge and after each oxidation step. An appropriate analysis of the XAS spectra could provide information on both the oxidation kinetics and oxide structure. Experimental data on the high temperature oxidation of nickel, cobalt, and Fe(64%)Ni(36%) alloy, at low oxygen pressure, are reported and analyzed according to the proposed data reduction. These results indicate the presented technique to be particularly suitable for studying the hot corrosion of oxide film too thick for common surface spectroscopy (AUGER, ESCA) and too thin for conventional thermogravimetric technique.

Daniele Gozzi

Optimization of X-ray Absorbers for High-Resolution TES Detectors in NewATHENA X-IFU

NewATHENA’s X-ray Integral Field Unit (X-IFU) uses a large-format array of Transition Edge Sensor (TES) microcalorimeters coupled with absorbers made of gold and bismuth providing 4 eV FWHM resolution up to 7 keV in the 0.2- 12 keV band. X-ray absorbers must be thick enough for photon absorption, maintain low heat capacity for energy resolution, and have good thermalization properties. The X-IFU requires total Quantum Efficiency (QE) of 96%, 87%, and 63% at 1, 7, and 9.5 keV, respectively. Optimal thicknesses are 1.05 µm gold and 5.5 µm bismuth to achieve 0.731 pJ/K at 90 mK and 87% QE at 7 keV. While typical TES absorbers are 3-4 µm thick, producing the required 5.5 µm Bi absorbers via standard electroplating creates enlarged grains and surface roughness. The increased roughness and grain size variability produced with our standard recipe have resulted in instances of 1) low energy spectral tails 2) spectral broadening of the energy resolution and 3) thermal shorts between pixels when a large grain bridges the gap between absorbers. In this study, we have introduced a new fabrication process and altered the morphology of the thick Bi through changes in the electroplating process. The process changes are intended to address all three issues as well as reduce particulate contamination observed on the finished detector arrays.

Absorber

The HEROIX Broadband X-Ray Space Telescope Mission Concept

The High EneRgy Observatory for Imaging X-rays (HEROIX) Medium-Class Mission concept envisions a next-generation broadband X-ray observatory designed to meet the astrophysics community’s need for high-angular-resolution studies of the Cosmic X-ray Background. Building on the science legacy of NASA’s NuSTAR mission and more than 30 years of advances in replicated NiCo shell technology at NASA Marshall, HEROIX proposes a space observatory comprising four co-aligned telescopes achieving 5 arcsecond half-power diameter (HPD) angular resolution. This capability, approached by the resolution demonstrated in the FOXSI-4 sounding rocket mission and under development through the SuperHERO balloon mission, will be extended to energies up to 80 keV through multilayer coatings. Marshall’s inhouse precision optics manufacturing enables an integrated effective area of 380 cm² at 30 keV, which, combined with high-resolution optics, opens new windows into extreme astrophysical non-thermal processes.

Nick Thomas

Polarized Resonant Soft X-ray Scattering (P-RSoXS) as a New Technique for Characterizing Amorphous Astromaterials

In the coming years, samples will be returned from several asteroids, the lunar surface, and the first material returned directly from the Martian surface. Previous in-situ and remote studies indicate these samples will contain abundant amorphous or weakly crystalline materials. However, detailed characterization and quantification of these amorphous materials remains challenging. Conventional techniques, including electron microscopy and X-ray diffraction, provide important information on material structure, but are generally limited to crystalline materials. Polarized resonant soft X-ray scattering (P-RSoXS) is a synchrotron-based X-ray scattering technique that has been used to characterize and quantify weakly crystalline systems, including soft materials. This research aims to translate this technique to geologic and extraterrestrial materials, building off the knowledge of using P-RSoXS to interrogate soft materials. P-RSoXS is well-suited to interrogate geologic materials, which are often multiphase, heterogeneous systems with crystalline and amorphous components, and domain sizes on the order of tens of nanometers. It is anticipated that future work will help reveal new chemical and structural information in geologic materials. Maturation of this preliminary work to develop P-RSoXS to characterize astromaterial-relevant samples will provide new understanding of the secondary processes responsible for the development of amorphous astromaterials and further elucidate our knowledge of the geologic history and past alteration processes.

Joshua H Litofsky