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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Zircon age-temperature-compositional spectra in plutonic rocks

We present that geochronology can resolve dispersed zircon dates in plutonic rocks when magma cooling time scales exceed the temporal precision of individual U-Pb analyses; such age heterogeneity may indicate protracted crystallization between the temperatures of zircon saturation (T sat ) and rock solidification (T solid ). Diffusive growth models predict asymmetric distributions of zircon dates and crystallization temperatures in a cooling magma, with volumetrically abundant old, hot crystallization at T sat decreasing continuously to volumetrically minor young, cold crystallization at T solid . We present integrated geochronological and geochemical data from Bergell Intrusion tonalites (Central Alps, Europe) that document zircon compositional change over hundreds of thousands of years at the hand-sample scale, indicating melt compositional evolution during solidification. Ti-in-zircon thermometry, crystallization simulation using MELTS software, and U-Pb dates produce zircon mass-temperature-time distributions that are in excellent agreement with zircon growth models. In conclusion, these findings provide the first quantitative validation of longstanding expectations from zircon saturation theory by direct geochronological investigation, underscoring zircon’s capacity to quantify supersolidus cooling rates in magmas and resolve dynamic differentiation histories in the plutonic rock record.

58 GEOSCIENCES↗
DOE OSTI2022

Tuscaloosa Marine Shale: Seal or Source? Petrophysical Comparative Study of Wells in SE Louisiana and SW Mississippi

The Tuscaloosa Marine Shale (TMS) is a versatile Late Cretaceous shale formation present in central and SE Louisiana and SW Mississippi, which drew attention because of the various roles played within the Tuscaloosa Group. In this paper, it is debated whether the Tuscaloosa Marine Shale can act as a source, reservoir, or seal all throughout the shale play or only in certain areas. Well log and core data from Adams County, Mississippi, are compared to data from East Feliciana Parish in Louisiana. Conclusions were drawn based on the results of well log analysis, X-ray Diffraction (XRD), porosity–permeability measurements, programmed pyrolysis, and fracture analysis. It was shown that the Tuscaloosa Marine Shale interval in SE Louisiana consists of important amounts of calcite, exhibits multiple natural fractures, has porosity values as high as 9.3%, and shows a TOC content of up to 2.8 wt%. On the other hand, samples from a well at the Cranfield field, MS, are characterized by considerably lower TOC values of around 0.88 wt%, porosities between 0.33% and 4%, and no serious fracturing. The formation demonstrates better reservoir and source potential in SE Louisiana and reliable CO2 sealing capacity in SW Mississippi. The analysis presented in this paper represents a holistic approach to the characterization of shale formations, is applicable to other plays around the world, and can be used as an integral part of CO2 sequestration or hydraulic fracturing programs.

04 OIL SHALES AND TAR SANDS↗
NASA NTRS1977

Shock metamorphism of lunar and terrestrial basalts

Lonar Crater (India) basalt and lunar basalt 75035 were shock loaded under controlled laboratory conditions up to 1000 kbar, generally in a CO/CO2 (1:1) environment evacuated to 10 to the minus seventh power torr. The Kieffer et al. (1976) classification scheme of progressive shock metamorphism is found to apply to lunar basalts. The major shock features of the five classes that span the range 0 to 1000 kbar are described. Only three out of 152 basalt specimens show shock effects in their natural state as severe as Class 2 features. The scarcity of shocked basalt hand samples in contrast to the abundance of shock-produced agglutinates and homogeneous glass spheres in the lunar regolith indicates the dominant role of micrometeorite impact in the evolution of the lunar regolith. The overall glass content in asteroidal and Mercurian regoliths is considered.

Schaal, R. B.↗
NASA NTRS1989

The Tsarev meteorite - Petrology and bidirectional reflectance spectra of a shock-blackened L chondrite

The Tsarev meteorite is a highly shocked black L5 ordinary chondrite. Meteorites of this class may have been subjected to regolith processes on or near the surface of ordinary chondrite bodies. The study of their optical alteration can provide valuable support in the spectral search for ordinary chondrite parent bodies. Although Tsarev is very dark in a cut-surface hand sample, it is characterized by subtle variations in apparent darkness, called in this work grey and black areas. Both areas are substantially optically altered from normal ordinary chondrites and are characterized by a much lower albedo and strongly suppressed absorption features. Although both areas are altered, they show differences in albedo and the strength of absorption features. Particulate samples from the black area have a slightly higher albedo and stronger absorption features, while the particulate samples from the grey area show a systematic suppression of spectral features and albedo. Chemical, mineralogical, and spectral analyses suggest that the spectral differences can be the result of one or a combination of several factors, including shock effects on the crystallographic structure of the minerals and differences in the size, distribution, and amount of metal and troilite grains.

Britt, D. T.↗
NASA NTRS1993

Heterogeneity in small aliquots of Apolllo 15 olivine-normative basalt: Implications for breccia clast studies

Most of the recent advances in lunar petrology are the direct result of breccia pull-apart studies, which have identified a wide array of new highland and mare basalt rock types that occur only as clasts within the breccias. These rocks show that the lunar crust is far more complex than suspected previously, and that processes such as magma mixing and wall-rock assimilation were important in its petrogenesis. These studies are based on the implicit assumption that the breccia clasts, which range in size from a few mm to several cm across, are representative of the parent rock from which they were derived. In many cases, the aliquot allocated for analysis may be only a few grain diameters across. While this problem is most acute for coarse-grained highland rocks, it can also cause considerable uncertainty in the analysis of mare basalt clasts. Similar problems arise with small aliquots of individual hand samples. Our study of sample heterogeneity in 9 samples of Apollo 15 olivine normative basalt (ONB) which exhibit a range in average grain size from coarse to fine are reported. Seven of these samples have not been analyzed previously, one has been analyzed by INAA only, and one has been analyzed by XRF+INAA. Our goal is to assess the effects of small aliquot size on the bulk chemistry of large mare basalt samples, and to extend this assessment to analyses of small breccia clasts.

Lindstrom, Marilyn M.↗
NASA NTRS1994

A phyllosilicate-sulfide vein in Kaidun

A fragment of a carbonaceous chondrite (#53.12, maximal dimension about 2 mm) containing a phyllosilicate-sulfide vein was found during an inspection of small pieces of the Kaidun meteorite. Phyllosilicate veins are apparently rare in carbonaceous chondrites and have so far only been reported from the Y82162 CI chondrite. In hand sample the vein was visible on two perpendicular faces. The polished section prepared from one side displays a complex structure. A single vein, 150 microns in width, bifurcates, and each branch narrows toward a large rounded object (RO). The section contains abundant ROs, most of them less than or equal to 100 microns in diameter. The vein has sharp contacts to the surrounding matrix, whereas the RO contacts are diffuse. The phyllosilicate in the main vein has a massive texture along the contact, which becomes platy toward the vein center where the crystals protrude into an open space. The texture of the largest RO resembles that of a barred olivine (BO) chondrule. Some of the smaller ROs also texturally resemble chondrules. The BO chondrule contains rounded sulfide-silicate objects and small metal grains covered by oxides. Phyllosilicates of the main vein consist mainly of serpentine. The phyllosilicate near the contact with the matrix has low contents of minor elements and a high Mg/Fe ratio. The composition changes in a regular manner toward the center: Al, Na, Ca, Ni, and S increase, indicating increasing amounts of sulfates admixed. The phyllosilicate vein could only have formed after a substantial rock was formed. Mechanical stress probably opened a crack that was subsequently filled by phyllosilicate, pyrrhotite, and finally by a (Fe,Mg)-sulfate. The source of the matter mobilized to form the vein could have been within the rock itself or outside. No compositional or mineralogical zoning is apparent at the vein-rock contacts. The nature of the transporting agent (liquid H2O or vapor) must also remain an enigma. M. Zolensky has recently observed similar phyllosilicate-filled veins in dark, wet clasts in the Al Rais CR chondrite.

Ivanov, A. V.↗
NASA NTRS2009

Covariant C and O Isotope Trends in Arctic Carbonate Crusts and ALH 84001: Potential Biomarker or Indicator of Cryogenic Formation Environment?

This work seeks to use the chemical, isotopic, and mineralogical characteristics of secondary carbonate minerals produced during brief aqueous events to identify the conditions of the aqueous environment in which they formed. Liquid water near the surface of Mars is subject to either rapid freezing and/or evaporation. These processes are also active on Earth, and produce secondary minerals that have complex chemical, mineralogical, and isotopic textures and compositions that can include covariant relationships between Delta C-13 (sub VPDB) and delta O-18 (sub VSMOW). The extremely well studied four billion year old carbonates preserved in martian meteorite ALH 84001 also show covariant delta C-13 and delta O-18 compositions, but these variations are manifested on a micro-scale in a single thin section while the variation observed so far in terrestrial carbonates is seen between different hand samples.

Socki, Richard A.↗
NASA NTRS2011

The Regolith of 4 Vesta: Perspectives from Howardite Meteorites and Dawn Mission Observations

4 Vesta is the largest asteroid with a basaltic surface, the only surviving differentiated asteroid recording igneous processes from the earliest phase of solar system history. The Dawn spacecraft is in orbit about Vesta pursuing a campaign of high resolution imaging and visible and infrared spectrometry of the surface; compositional mapping by gamma-ray and neutron spectrometry will follow. Vesta is heavily cratered with a surface covered by impact debris, a regolith. One important goal of the Dawn mission is to develop an understanding of regolith processes that are affecting this surface debris. Regolith characteristics are a record of interaction with the environment (e.g., impactors, dust, solar wind, galactic cosmic-rays) and give evidence of surface processes (down-gravity movement, etc.). Regolith mineralogy and composition reflect the local bedrock, with influences from regional and global mixing. Understanding regolith processes will aid in determining the lithology of underlying crust. Vesta is most likely the parent asteroid of the howardite, eucrite and diogenite meteorites. Eucrites are intrusive and extrusive mafic rocks composed mostly of ferroan low-Ca clinopyroxene and calcic plagioclase, while diogenites are cumulate magnesian orthopyroxenites. Magmatism occurred within a few million years of the formation of the solar system and then ceased. Impacts into the igneous crust produced the howardites - polymict breccias composed of mineral and lithic debris derived mostly from eucrites and diogenites. Some howardites are true regolith breccias formed by lithification of extensively impact-gardened surface debris. However, howardites have a number of significant petrologic and compositional differences from mature lunar regolith breccias and soils reflecting the different environment around Vesta compared to that at 1 AU. The most significant differences are the higher impactor flux with a lower mean impact velocity and the lower gravity. As a result, regolith processes on Vesta differ in detail from those on the Moon. Laboratory study of howardites and orbital investigation of Vesta will allow for development of robust models of regolith formation on hand sample to multi-kilometer scales.

Mittlefehldt, David W.↗
NASA NTRS2014

Alteration of Sedimentary Clasts in Martian Meteorite Northwest Africa 7034

The martian meteorite Northwest Africa (NWA) 7034 and pairings represent the first brecciated hand sample available for study from the martian surface [1]. Detailed investigations of NWA 7034 have revealed substantial lithologic diversity among the clasts [2-3], making NWA 7034 a polymict breccia. NWA 7034 consists of igneous clasts, impact-melt clasts, and "sedimentary" clasts represented by prior generations of brecciated material. In the present study we conduct a detailed textural and geochemical analysis of the sedimentary clasts.

McCubbin, F. M.↗
NASA NTRS2015

Updates on Pairing Issues with the US Antarctic Meteorite Collection

The US Antarctic meteorite program has re-covered >21,000 meteorites since 1976, with thousands of those recovered from several icefields over multiple seasons, some-times spanning over a decade [1]. Pairing is assigned as best as possible at the time of classification, based on information from the field team, macro-scale hand sample features in the lab, and petrography, but later focused studies can reveal details that suggest re-evaluation of pairing groups. As a result, pairing groups are revealed over time, and must be continuously updated. Here we examine a few groups with known issues and give an update on some of the larger or more significant pairing groups.

Righter, K.↗
NASA NTRS2017

Basalt Weathering in a Cold and Icy Climate: Three Sisters, Oregon as an Analog for Early Mars

There is abundant evidence for liquid water on early Mars, but the debate remains whether early Mars was warm and wet or cold and icy with punctuated periods of melting. To further investigate the hypothesis of a cold and icy early Mars, we collected rocks and sediments from the Collier and Diller glacial valleys in the Three Sisters volcanic complex in Oregon. We analyzed rocks and sediments with X-ray diffraction (XRD), scanning and transmission electron microscopies with energy dispersive spectroscopy (SEM, TEM, EDS), and visible, short-wave infrared (VSWIR) and thermal-IR (TIR) spectroscopies to characterize chemical weathering and sediment transport through the valleys. Here, we focus on the composition and mineralogy of the weathering products and how they compare to those identified on the martian surface. Phyllosilicates (smectite), zeolites, and poorly crystalline phases were discovered in pro- and supra-glacial sediments, whereas Si-rich regelation films were found on hand samples and boulders in the proglacial valleys. Most phyllosilicates and zeolites are likely detrital, originating from hydrothermally altered units on North Sister. TEM-EDS analyses of the <2 um size fraction of glacial flour samples demonstrate a variety of poorly crystalline (i.e., no long-range crystallographic order) phases: iron oxides, devitrified volcanic glass, and Fe-Si-Al phases. The CheMin XRD on the Curiosity rover in Gale crater has identified significant amounts of X-ray amorphous materials in all samples measured to date. The amorphous component is likely a combination of silicates, iron oxides, and sulfates. Although we have not yet observed amorphous sulfate in the samples from Three Sisters, the variety of poorly crystalline weathering products found at this site is consistent with the variable composition of the X-ray amorphous component identified by CheMin. We suggest that these amorphous phases on Mars could have formed in a similarly cold and icy environment.

Rampe, E. B.↗
DOE OSTI2017

Geothermal Exploration of Mount Baker Hot Springs Through Ground-Based Magnetic and Gravity Surveys

The Washington State Division of Geology and Earth Resources (WDGER), together with the USGS, Altarock Energy Inc., Colorado College, Temple University, Innovate Geothermal Ltd., University of British Columbia, and Western Washington University(WWU), conducted phase two of a geothermal play fairway exploration at three plays (Mount Baker, Mount St. Helens seismic zone, and Wind River valley) along the Washington Cascade Range. The Mount Baker (MB) play is an ideal location for further investigation as a potential geothermal resource due to the presence of thermal features, young volcanic centers, existing geothermal leases, accessibility, and its proximity to existing transmission lines at the Baker Lake Dam. The goal of phase II exploration at all three plays is to collect geologic and geophysical data to help constrain spatial changes in subsurface lithology and structures that may be associated with the geothermal systems. Furthermore, this paper discusses the geothermal potential of the southeast flank of Mount Baker, WA by interpreting newly collected ground-based gravity and magnetic data. The Mount Baker play was surveyed from July-September, 2016 by the USGS, WDGER, and WWU. Results of a detailed magnetic and gravity surveys of the region surrounding the Baker hot springs, the primary surface expression of the hydrothermal system, are presented here. Gravity data were collected at 495 stations in the study area amounting to an area of roughly 150 square km. Approximately 93 km of line magnetometer data were collected within the study area, over a dozen magnetic susceptibility measurements were taken at 50 locations and about 50 hand samples were collected for density measurements. Preliminary data and modeling suggest pronounced magnetic anomalies trending NE/SW, generally in line with previously mapped lineaments identified in LiDAR. We present a series of preliminary two-dimensional forward models of the gravity and magnetic data as well as a 3D inversion model of magnetic susceptibility and interpret these models in terms of the structural controls influencing the Baker hot springs and hydrothermal system.

Geophysics↗
NASA NTRS2010

Automated Desalting Apparatus

Because salt and metals can mask the signature of a variety of organic molecules (like amino acids) in any given sample, an automated system to purify complex field samples has been created for the analytical techniques of electrospray ionization/ mass spectroscopy (ESI/MS), capillary electrophoresis (CE), and biological assays where unique identification requires at least some processing of complex samples. This development allows for automated sample preparation in the laboratory and analysis of complex samples in the field with multiple types of analytical instruments. Rather than using tedious, exacting protocols for desalting samples by hand, this innovation, called the Automated Sample Processing System (ASPS), takes analytes that have been extracted through high-temperature solvent extraction and introduces them into the desalting column. After 20 minutes, the eluent is produced. This clear liquid can then be directly analyzed by the techniques listed above. The current apparatus including the computer and power supplies is sturdy, has an approximate mass of 10 kg, and a volume of about 20 20 20 cm, and is undergoing further miniaturization. This system currently targets amino acids. For these molecules, a slurry of 1 g cation exchange resin in deionized water is packed into a column of the apparatus. Initial generation of the resin is done by flowing sequentially 2.3 bed volumes of 2N NaOH and 2N HCl (1 mL each) to rinse the resin, followed by .5 mL of deionized water. This makes the pH of the resin near neutral, and eliminates cross sample contamination. Afterward, 2.3 mL of extracted sample is then loaded into the column onto the top of the resin bed. Because the column is packed tightly, the sample can be applied without disturbing the resin bed. This is a vital step needed to ensure that the analytes adhere to the resin. After the sample is drained, oxalic acid (1 mL, pH 1.6-1.8, adjusted with NH4OH) is pumped into the column. Oxalic acid works as a chelating reagent to bring out metal ions, such as calcium and iron, which would otherwise interfere with amino acid analysis. After oxalic acid, 1 mL 0.01 N HCl and 1 mL deionized water is used to sequentially rinse the resin. Finally, the amino acids attached to the resin, and the analytes are eluted using 2.5 M NH4OH (1 mL), and the NH4OH eluent is collected in a vial for analysis.

Spencer, Maegan K.↗
NASA NTRS1996

Experimental Modification of Rat Pituitary Prolactin Cell Function During and After Spaceflight

Experimental modification of rat pituitary prolactin cell function during and after spaceflight. This study was done to evaluate the effects of microgravity on prolactin (PRL) cells of the male rat pituitary gland. We used the identical passive closed-vial cell culture system that was described for the culture of growth hormone cells (W C. Hymer, R. E. Grindeland, T. Salada, P. Nye, E. Grossman, and R Lane). After an 8-day spaceflight, all flight media (containing released PRL), as well as extracts (containing intracellular PRL), contained significantly lower amounts of immunoreactive PRL than their corresponding ground control samples. On the other hand, these same samples, when assessed for their biological activities by two different in vitro lymphocyte assays, yielded disparate results that may reflect posttranslational modifications to the hormone molecule. Other data showed that: (1) the apparent molecular weights of released PRL molecules were not altered by microgravity; but (2) the region from which the PRL cells came (dorsal or ventral) made a significant difference in the amount and activity of PRL released from the flight cells. Because there is much current interest in the role that PRL may play in the regulation of the immune system and because changes in both cellular and humoral immunity accompany spaceflight, this study could help define future microgravity research in this area.

Hymer, W. C.↗
DOE OSTI2023

Determining the Effects of Neutron Irradiation on the Structural Integrity of Additively Manufactured Heat Exchangers for Very Small Modular Reactor Applications, DOE Final Report (Project # 19-16980)

Auburn University (AU) teamed with the University of Missouri Research Reactor (MURR) and Kansas State University (KSU) to determine how to best use laser-powder bed fusion (L-PBF) additive manufacturing (AM) methods for generating radiation resistant nickel-based superalloys, Inconel alloy 625 and 718, for special purpose reactor (SPR) or very small modular reactor (vSMR) heat-exchangers (HeXs). Compact, conformal, and durable HeXs that are tolerant of extreme environments are needed for supporting the technical maturity of next-generation, portable compact reactors. AM is an enabler for realizing this new wave of HeXs – providing a means to make customizable hot and cold stream architectures with novel flow path geometries (e.g., tortuous channels with non-uniform, asymmetric cross-sections) and reduced layer-to-layer contact resistance (i.e., no separate bonding procedure required). AM further enables a more time/cost efficient means for fabricating SPRs by reducing the number of suppliers required for HeX assembly and allowing for on-site HeX fabrication. The project aim has been to better understand how neutron irradiation affects the microstructure and properties of additively manufactured nickel-based superalloys, to accelerate their safe, reliable use in the modular reactor industry. The major objective was to qualify/quantify the microstructure and microhardness of nickel-based superalloys (including Inconel 718 and 625) additively manufactured via the L-PBF process in the neutron-dosed (irradiated) and non-irradiated states over a course of 3 years. Effects of build orientation during L-PBF and post-AM heat treatments on neutron resistance, microstructure and mechanical properties were also investigated. Neutron damage mechanisms via hardening were characterized. This project combined subject-matter experts in AM, mechanical/microstructure metallic part characterization, and neutron irradiation, as well as unique assets and capabilities at AU and MURR at MU, to ensure project results translated to effectively addressing known gaps in nuclear science and engineering. Parts were fabricated using L-PBF systems readily available at AU. Specimens were then irradiated using MURR facilities; a manipulator equipped hot cell was also used to measure material hardness after dosing. MURR, a 10 MW, light-water nuclear reactor, is the largest, highest powered, highest-flux university owned research reactor in the U.S. The major findings in this project provide evidence that AM can serve as an alternative way to build structural components for future advanced small modular reactors using advanced materials like Inconel 625 (IN625) or Inconel 718 (IN718). After full spectrum neutron irradiation, vertically as-built AM IN625 samples were observed to display better resistance towards radiation-induced-hardening defects relative to traditionally machined metals. A Vickers microhardness tester, using settings of 1 kgf and dwell time of 15 seconds per indentation, was used to measure hardness in this study. The as-built, vertically printed samples experienced 1.2% of radiation hardening vs. 5.25% radiation hardening observed in wrought IN625. Another set of IN625 and IN718 samples were exposed to fast neutron irradiation. It was observed that IN718 showed more resistance towards radiation hardening compared to IN625 samples indicating IN718 had a better performance. Results showed that the IN718 samples experienced less change (-2.5 to 3.24 %) in microhardness. On the other hand, IN625 samples underwent more (0.9 to 7.21%) change in microhardness after fast neutron irradiation. AM IN625 samples were irradiated using an ion (proton) beam in cyclotron. The mechanical properties of AM samples post irradiation were compared with wrought samples. The irradiated region on the samples were tested using nano-hardness indention. It was observed that the beam current and time used in this study generated an annealing effect and thus reduced the hardness of the samples. The sum of the project results provide precious insight into how one may minimize radiation hardening in AM materials while maintaining material property constraints. Results should assist engineers in selecting an appropriate heat treatment for AM nickel-based superalloys for increased radiation resistance. Results should increase confidence levels for adopting AM for building nuclear reactor components which perform the same or better than conventionally manufactured components. Fast neutron irradiation testing provided an accelerated means of obtaining radiation effects without making materials radioactive and difficult to handle.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
NASA NTRS2008

Effects of hand soldering MIL-PRF 55365 tantalum capacitors

Different values of MIL-PRF-55365 tantalum capacitors were subjected to three different types of soldering conditions— Convection Reflow, JPL Standard Hand Soldering, and Optimized Hand Soldering. The electrical parameters for a large number of capacitors of each value were measured before and after thermal soldering stress. The results indicate that tantalum capacitors subjected to convection reflow conditions experience detectable changes in electrical parameters; capacitors subjected to hand solder conditions show reduced changes in electrical parameters when compared to the reflow samples. Optimized hand solder conditions are shown to have a minimal effect on electrical parameters.

Sheldon, Douglas↗
NASA NTRS1974

The application of large numbers of pleasure boats to collect synoptic sea-truth for ERTS-1 overpasses

The author has identified the following significant results. In order to interpret and annotate current circulation and suspended sediment concentration maps derived from ERTS-1 digital tapes, the University of Delaware has been collecting water samples and other data from boats and helicopters. In order to increase the number of samples at the exact time of the ERTS-1 pass over Delaware Bay, pleasure craft were organized to obtain samples of the entire test site. On the ERTS-1 pass of July second, scientists were stationed at three public boat launches along the Bay to hand out sampling packets to interested boaters. The packets contained two litre sampling bottles, a map, data card, and a pen. The boaters were asked to fill the two bottles between 11 and 11:15 a.m., mark their location on the map, and fill out the data card. Forty-nine packets were handed out of which 40 were returned (82%). Only four of the 40 were not in the alloted time range. This gave 36 real time data points covering approximately 30 nautical miles. The samples are being analyzed for sediment concentration, particle size, and salinity. Participating boaters will receive a copy of an ERTS image of the Delaware Bay and a summary report of the project. Because of the success of the project, future use of pleasure boaters is being planned.

Klemas, V.↗