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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRS1980

Spectroscopic determination of the in-situ composition of epoxy matrices in glass fiber reinforced composites

Computerized infrared analysis is applied to the characterization of a glass-reinforced crosslinked polyester. The method of factor analysis determines the number of independent components which constitute the polymeric matrix. Subsequently, the spectra of those components are fitted by a least-squares criterion to spectra of the multicomponent matrix, or, if the glass spectrum is included as an additional component, to the spectra of composites. The least-squares coefficients yield the matrix composition in terms of the initial reactant composition and the extent of crosslinking.

Antoon, M. K.↗

NASA NTRS1981

Spectroscopic determination of the in-situ composition of epoxy matrices in glass-fiber-reinforced composites

Antoon, M. K.↗

NASA NTRS1982

Estimation of bearing contact angle in-situ by X-ray kinematography

The mounted, preloaded contact angle of the structural bearings in the assembled design mechanical assembly was measured. A modification of the Turns method is presented, based upon the clarity and definition of moving parts achieved with X-ray technique and cinematic display. Contact angle is estimated by counting the number of bearings passing a given point as a function of number of turns of the shaft. Ball and pitch diameter variations are discussed. Ball train and shaft angle uncertainties are also discussed.

Fowler, P. H.↗

NASA NTRS1982

Forward scattering and backscattering of solar radiation by the stratospheric limb after Mount St. Helens eruption

Stratospheric limb radiance profiles versus altitude of closest approach of the line of sight to the Earth's surface have been measured before and after the Mount St. Helens eruptions by means of photographs taken from a Sun-oriented balloon gondola floating above 35 km altitude over France. Preliminary data were reported for flights in October 1979 and in May and June 1980. The radiance integrated along the line of sight as in-situ radiance (R) can be derived taking into account absorption by ozone and air. The onion peeling inversion method was used to derive the vertical radiance (R) profiles respectively. The values of R were determined in the solar azimuth. The solar elevation angles are chosen larger for the backscattering observation than for the forward scattering observation to deal with as similar illumination conditions as possible despite the Earth's sphericity.

Ackerman, M.↗

NASA NTRS1973

Static penetration resistance of soils

Model test results were used to define the failure mechanism associated with the static penetration resistance of cohesionless and low-cohesion soils. Knowledge of this mechanism has permitted the development of a new analytical method for calculating the ultimate penetration resistance which explicitly accounts for penetrometer base apex angle and roughness, soil friction angle, and the ratio of penetration depth to base width. Curves relating the bearing capacity factors to the soil friction angle are presented for failure in general shear. Strength parameters and penetrometer interaction properties of a fine sand were determined and used as the basis for prediction of the penetration resistance encountered by wedge, cone, and flat-ended penetrometers of different surface roughness using the proposed analytical method. Because of the close agreement between predicted values and values measured in laboratory tests, it appears possible to deduce in-situ soil strength parameters and their variation with depth from the results of static penetration tests.

Durgunoglu, H. T.↗

NASA NTRS1983

Breakdown of organic insulators

Solar cells and their associated electrical interconnects and leads were encapsulated in transparent elastomeric materials. Their purpose in a photovoltaic module, one of the most important for these elastomeric encapsulation materials, is to function as electrical insulation. This includes internal insulation between adjacent solar cells, between other encapsulated electrical parts, and between the total internal electrical circuitry and external metal frames, grounded areas, and module surfaces. Catastrophic electrical breakdown of the encapsulant insulation materials or electrical current through these materials or module edges to external locations can lead to module failure and can create hazards to humans. Electrical insulation stability, advanced elastomeric encapsulation materials are developed which are intended to be intrinsically free of in-situ ionic impurities, have ultralow water absorption, be weather-stable (UV, oxygen), and have high mechanical flexibility. Efforts to develop a method of assessing the life potential of organic insulation materials in photovoltaic modules are described.

Cuddihy, E. F.↗

NASA NTRS1973

Joint Conference on Sensing of Environmental Pollutants, 2nd, Washington, D.C., December 10-12, 1973, Proceedings

Subjects considered are related to the remote passive sensing of atmosphere pollutants, the extension of laboratory measurement techniques for field use, instrument quality and measurement standardization, the remote active sensing of atmospheric pollutants, stationary source sensing, and air quality standards and measurement accuracy. Aspects of radiological, electromagnetic, and acoustic pollution monitoring are discussed together with new methods in particulate analysis, the measurement of meteorological variables that impact on atmospheric pollutants, and the impact of meteorological parameters on pollution analysis. The in-situ sensing of acoustic chemical and biological pollutants is reported along with global scale pollution monitoring and the remote sensing of water pollutants. Individual items are announced in this issue.

Source record↗

NASA NTRS1978

Remote in-situ elemental analysis systems for underwater application

The systems approach, theoretical measurement calculations, and preliminary measurements to be used in monitoring and mapping pollutants (such as traces of heavy metals) in the Chesapeake Bay are discussed. A neutron gamma-ray method is under development for demonstrating the system. The excitation source to be used is a machine accelerator using a deuterium/tritium reaction to produce 14-MeV neutrons. The neutrons excite characteristic gamma ray emission from the neutron irradiated surface. The discrete line emission produced can be used to infer both qualitative and quantitative elemental composition. A data preprocessor will accumulate, digitize, store, format, and prepare the data for transmission which can be accomplished by telephone, microwave, and possibly satellite link to central processors.

Trombka, J. I.↗

NASA NTRS2026

Extrusion-based Additive Manufacturing of Regolith-Filled Shape Memory Vitrimer Composite for Lunar Construction

The National Aeronautics and Space Administration (NASA) is visiting the moon again. This time, the objective is to explore establishing a permanent lunar base. To achieve both longterm human habitation on the moon and future deep space travel, it is crucial to make the most of the in-situ resources and build autonomous systems on the moon to support the construction of a lunar habitat. NASA’s In-situ Resource Utilization (ISRU) program aims to minimize the need to ship heavy prefabricated structures, reducing cost and enhancing sustainability. Here, we developed an economical extrusion method for printing lunar regolith-based composites using shape memory vitrimer as a binder. A rheological study is conducted to determine the extrudability of the composite with different regolith weight percentages. Several characterizations were conducted on the composites. The as-printed composites exhibited compressive and flexural strengths of 73.32 MPa and 156.59 MPa, respectively, and good impact tolerance. The composite maintained 57.92% of its mechanical properties even after the second crack healing cycle. The composites also exhibit shape fixity ratio of 90.02% and shape recovery ratio of 83.46%. The simple synthesis method, sustainability, and good thermomechanical properties make the 3D printed composite an ideal material for lunar construction applications.

Kingsley Yeboah Gyabaah↗

NASA NTRS1972

Experimental approaches to well controlled studies of thin-film nucleation and growth.

Particular features and the performance of two experimental systems are described for quantitative studies of thin-film nucleation and growth processes including epitaxial depositions. System I consists of a modified LEED-Auger instrument combined with high-resolution electron microscopy. System II is a UHV electron microscope adapted for in-situ deposition studies. The two systems complement each other ideally, and the combined use of both can result in a comprehensive investigation of vapor deposition processes not obtainable with any other known method.

Poppa, H.↗

NASA NTRS1974

Recent improvements in our knowledge of neutral atmosphere structure from satellite drag measurements

Observational results on the density in the thermosphere and lower exosphere (i.e., within the altitude range from about 150 to about 1000 km) are discussed in this paper. Most observational results on total gas density were obtained from orbital drag and more recently also from in-situ drag analysis. The primary parameter measured is atmospheric density, with temperature as a secondary structural parameter deduced with the help of theory and/or atmospheric models. Both the merits and shortcomings of the drag analysis method are outlined in view of a comparison of temperature deduced from total density and kinetic gas temperature measured by incoherent scatter. Recent improvements of our knowledge of the known density variations are presented.

Roemer, M.↗

NASA NTRS1978

Laboratory studies of in vivo fluorescence of phytoplankton

A lidar system is developed that uses four selected excitation wavelengths to induce chlorophyll 'a' fluorescence which is indicative of both the concentration and diversity of phytoplankton. The operating principles of the system and the results of measurements of phytoplankton fluorescence in a controlled laboratory environment are presented. A comparative study of results from lidar fluorosensor laboratory tank tests using representative species of phytoplankton in single and multispecies cultures from each of four color groups reveals that (1) there is good correlation between the fluorescence of chlorophyll 'a' remotely simulated and detected by the lidar system and in-situ measurements using four similar excitation wavelengths in a flow-through fluorometer; (2) good correlation exists between the total chlorophyll 'a' calculated from lidar-fluorosensor data and measurements obtained by the Strickland-Parsons method; and (3) the lidar fluorosensor can provide an index of population diversity.

Brown, C. A., Jr.↗

NASA NTRS1971

In-situ measurement of objective lens data of a high-resolution electron microscope.

Bragg-reflex images of small individual crystallites in the size range of 20-100 A diameter with known crystallographic orientation were used in a transmission electron microscope to determine in-situ: (a) the relationship between objective lens current (or accelerating voltage) changes in discrete steps and corresponding defocus, (b) the spherical aberration coefficient, and (c) the axial chromatic aberration coefficient of the objective lens. The accuracy of the described method is better than 5%. The same specimen can advantageously be used to properly aline the illuminating beam with respect to the optical axis.

Heinemann, K.↗

NASA NTRS1983

Surface studies with (clean) supported metal particles and clusters

Small particles are ideal for combined studies with surface analytical and electron microscopy/diffraction methods. In this way crystallography, microstructure, morphology, physical stability, and electronic structure can be correlated directly with chemical reactivity. Various integrated experimental approaches for conducting model studies with UHV-evaporated particles have been successfully developed; they entail the use of TPD, AES, XPS, and work function measurements on one hand and standard TEM/TED, in-situ TEM/TED, and in-situ STED/TEM techniques on the other hand. The essential features of four particular experimental approaches are discussed and a selection of representative results is presented to illustrate the potential usefulness of such studies in the field of catalysis.

Poppa, H. R.↗

NASA NTRS1979

Ocean Chlorophyll Studies from a U-2 Aircraft Platform

Chlorophyll gradient maps of large ocean areas were generated from U-2 ocean color scanner data obtained over test sites in the Pacific and Atlantic Oceans. The delineation of oceanic features using the upward radiant intensity relies on an analysis method which presupposes that radiation backscattered from the atmosphere and ocean surface can be properly modeled using a measurement made at 778 nm. An estimation of the chlorophyll concentration was performed by properly ratioing radiances measured at 472 nm and 548 nm after removing the atmospheric effects. The correlation between the remotely sensed data and in-situ surface chlorophyll measurements was validated in two sets of data. The results show that the correlation between the in-situ measured chlorophyll and the derived quantity is a negative exponential function and the correlation coefficient was calculated to be -0.965.

Kim, H. H.↗

NASA NTRS1979

Proposed methods for the reconstruction of the Pioneer/Venus probe entry trajectories

In connection with the Pioneer Venus Project, an orbiter and an array of atmospheric probes are sent to Venus in separate launches during 1978. The four probes, which are transported to the planet on an instrumented Bus are released approximately 20 days prior to encounters. There are three identical small probes and a large probe. Each is designed to make in-situ atmospheric measurements. One of the principal scientific objectives of the Pioneer Venus (P/V) multiprobe mission is the determination of the structure and composition of the Venusian atmosphere down to the planet surface. To enhance the science return it is of paramount importance to be able to accurately determine the spacecraft entry trajectories. In addition to the in-situ spacecraft measurements, earth-based Doppler data are available. The process felt to be most applicable for the P/V multiprobe entry trajectory reconstruction is considered, with emphasis placed on the highly dynamic upper entry segment of the trajectory.

Findlay, J. T.↗

NASA NTRSDate not supplied

Evaluating Crystallinity in Thermoplastic Composites for Aerospace Applications

Polymer matrix composites (PMCs) offer many benefits for the aerospace industry due to their potential for weight reduction when compared to metal or ceramic based materials. Most PMCs currently in flight use thermoset matrices, however, thermoplastic resins are being explored as alternatives due to their ability to be remelted, which is of particular interest due to the potential for in-situ repair and faster production. Most thermoplastic resins are semicrystalline polymers. The properties of semicrystalline thermoplastics are directly influenced by their crystallinity, which can vary due to many factors including thermal treatments, environmental conditions, and mechanical deformation. Within thermoplastic PMC parts, crystallinity gradients can arise due to variations in part geometry, across part thicknesses, and along bonded joints. Monitoring the crystallinity of thermoplastic composites is key to ensuring these materials meet the high demands required for aerospace. Several different analytical techniques exist that can be used to characterize the bulk crystallinity of thermoplastic materials. However, many existing methods lack the specificity required to identify the subtle variations in crystallinity that may play a significant role in the performance and durability of PMC parts. Because of this, a significant amount of work is still required to fully characterize and understand the crystallinity profiles of thermoplastic PMCs and the resulting impact to material properties. This talk discusses the use of multiple techniques such as Differential Scanning Calorimetry, Polarized Light Optical Microscopy, and Fourier-Transform Infrared Spectroscopy to characterize the crystallinity in carbon fiber/thermoplastic composites. Samples of different crystallinity profiles were manufactured using various cooling procedures. This work aims to provide the fundamental data necessary to understand the effects of crystallinity on thermoplastic PMCs, which is key to advancing their use in aerospace applications.

Thermoplastics↗

NASA NTRS1981

Configuration of Jupiter's magnetic tail and equatorial current sheet

Recent research reports by Behannon et al. (1981) and Connerney et al. (1981) are summarized. It is noted that the analysis made of the detailed neutral sheet crossings by the minimum variance method shows a consistent result with regard to the orientation of the neutral sheet in the magnetic tail as a two-dimensional surface rocking back and forth about the Jupiter sun-line as the rotation of the planet leads to a precession of the tilted dipole magnetic axis. The occurrence of neutral sheet crossings is found not to be consistent with any of the axially symmetric theoretical models proposed earlier on the basis of the 1974 Pioneer 10 observations. It is noted that a simple nonaxially symmetric model has been developed on the basis of the Voyager results which indicates the strong control upon orientation by the interaction of the solar wind with the Jovian magnetosphere. The model is described as simple because it improves the fit of theory to observation but uses fewer parameters. A quantitative model of the magnetodisc equatorial current sheet has been developed for the inner magnetosphere region which matches well the in-situ magnetic field observations.

Ness, N. F.↗