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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
NASA NTRS2004

Alignment and Performance of the Infrared Multi-Object Spectrometer

The Infrared Multi-Object Spectrometer (IRMOS) is a principle investigator class instrument for the Kitt Peak National Observatory 4 and 2.1 meter telescopes. IRMOS is a near-IR (0.8 - 2.5 micron) spectrometer with low-to mid-resolving power (R = 300 - 3000). IRMOS produces simultaneous spectra of approximately 100 objects in its 2.8 x 2.0 arc-min field of view (4 m telescope) using a commercial Micro Electro-Mechanical Systems (MEMS) micro-mirror array (MMA) from Texas Instruments. The IRMOS optical design consists of two imaging subsystems. The focal reducer images the focal plane of the telescope onto the MMA field stop, and the spectrograph images the MMA onto the detector. We describe ambient breadboard subsystem alignment and imaging performance of each stage independently, and ambient imaging performance of the fully assembled instrument. Interferometric measurements of subsystem wavefront error serve as a qualitative alignment guide, and are accomplished using a commercial, modified Twyman-Green laser unequal path interferometer. Image testing provides verification of the optomechanical alignment method and a measurement of near-angle scattered light due to mirror small-scale surface error. Image testing is performed at multiple field points. A mercury-argon pencil lamp provides a spectral line at 546.1 nanometers, a blackbody source provides a line at 1550 nanometers, and a CCD camera and IR camera are used as detectors. We use commercial optical modeling software to predict the point-spread function and its effect on instrument slit transmission and resolution. Our breadboard and instrument level test results validate this prediction. We conclude with an instrument performance prediction for cryogenic operation and first light in late 2003.

Connelly, Joseph A.↗
NASA NTRS2001

Thermal Infrared Spectral Band Detection Limits for Unidentified Surface Materials

Infrared emission spectra recorded by airborne or satellite spectrometers can be searched for spectral features to determine the composition of rocks on planetary surfaces. Surface materials are identified by detections of characteristic spectral bands. We show how to define whether to accept an observed spectral feature as a detection when the target material is unknown. We also use remotely sensed spectra measured by the Thermal Emission Spectrometer (TES) and the Spatially Enhanced Broadband Array Spectrograph System to illustrate the importance of instrument parameters and surface properties on band detection limits and how the variation in signal-to-noise ratio with wavelength affects the bands that are most detectable for a given instrument. The spectrometer's sampling interval, spectral resolution, signal-to-noise ratio as a function of wavelength, and the sample's surface properties influence whether the instrument can detect a spectral feature exhibited by a material. As an example, in the 6-13 micrometer wavelength region, massive carbonates exhibit two bands: a very strong, broad feature at approximately 6.5 micrometers and a less intense, sharper band at approximately 11.25 micrometers. Although the 6.5-micrometer band is stronger and broader in laboratory-measured spectra, the 11.25-micrometer band will cause a more detectable feature in TES spectra.

Kirkland, Laurel E.↗
NASA NTRS2004

Multifunction Imaging and Spectroscopic Instrument

A proposed optoelectronic instrument would perform several different spectroscopic and imaging functions that, heretofore, have been performed by separate instruments. The functions would be reflectance, fluorescence, and Raman spectroscopies; variable-color confocal imaging at two different resolutions; and wide-field color imaging. The instrument was conceived for use in examination of minerals on remote planets. It could also be used on Earth to characterize material specimens. The conceptual design of the instrument emphasizes compactness and economy, to be achieved largely through sharing of components among subsystems that perform different imaging and spectrometric functions. The input optics for the various functions would be mounted in a single optical head. With the exception of a targeting lens, the input optics would all be aimed at the same spot on a specimen, thereby both (1) eliminating the need to reposition the specimen to perform different imaging and/or spectroscopic observations and (2) ensuring that data from such observations can be correlated with respect to known positions on the specimen. The figure schematically depicts the principal components and subsystems of the instrument. The targeting lens would collect light into a multimode optical fiber, which would guide the light through a fiber-selection switch to a reflection/ fluorescence spectrometer. The switch would have four positions, enabling selection of spectrometer input from the targeting lens, from either of one or two multimode optical fibers coming from a reflectance/fluorescence- microspectrometer optical head, or from a dark calibration position (no fiber). The switch would be the only moving part within the instrument.

Mouroulis, Pantazis↗
NASA NTRS2011

The Detector Subsystem for the SXS Instrument on the Astro-H Observatory

The Soft X-ray Spectrometer (SXS) instrument on the Astro-H observatory is based on a 36 pixel x-ray calorimeter array cooled to 50 mK in a sophisticated spaceflight cryostat. The SXS is a true spatial-spectral instrument, where each spatially discrete pixel functions as a high-resolution spectrometer. Here we discuss the SXS detector subsystem that includes the detector array, the anticoincidence detector, the first stage amplifiers, the thermal and mechanical staging of the detector, and the cryogenic bias electronics. The design of the SXS detector subsystem has significant heritage from the Suzaku/XRS instrument but has some important modifications that increase performance margins and simplify the focal plane assembly. Notable improvements include x-ray absorbers with significantly lower heat capacity, improved load resistors, improved thermometry, and a decreased sensitivity to thermal radiation. These modifications have yielded an energy resolution of 3.5-4.0 eV FWHM at 6 keV for representative devices in the laboratory, giving considerable margin against the 7 eV instrument requirement. We expect similar performance in flight

Porter, Frederick↗
NASA NTRS1995

The JPL Field Emission Spectrometer

The Jet Propulsion Laboratory (JPL) Field Emission Spectrometer (FES) was built by Designs and Prototypes based on a set of functional requirements supplied by JPL. The instrument has a spectral resolution of 6 wavenumbers (wn) and can acquire spectra from either the Mid Infrared (3-5 mu m) or the Thermal Infrared (8-12 pm) depending on whether the InSb or HgCdTe detector is installed respectively. The instrument consists of an optical head system unit and battery. The optical head which is tripod mounted includes the interferometer and detector dewar assembly. Wavelength calibration of the interferometer is achieved using a Helium-Neon laser diode. The dewar needs replenishing with liquid Nitrogen approximately every four hours. The system unit includes the controls for operation and the computer used for acquiring viewing and processing spectra. Radiometric calibration is achieved with an external temperature-controlled blackbody that mounts on the fore-optics of the instrument. The blackbody can be set at 5 C increments between 10 and 55 C. The instrument is compact and weighs about 33 kg. Both the wavelength calibration and radiometric calibration of the instrument have been evaluated. The wavelength calibration was checked by comparison of the position of water features in a spectrum of the sky with their position in the output from a high resolution atmospheric model. The results indicatethat the features in the sky spectrum are within 6-8 wn of their position ill the model spectrum. The radiometric calibration was checked by first calibrating the instrument using the external blackbody supplied with the instrument and then measuring the radiance from another external blackbody at a series of temperatures. The temperatures of these radiance spectra were then recovered by inventing Planck's law and the recovered temperatures compared lo the measured blackbody temperature. These results indicate that radiometric calibration is good to 0.5 C over the range of temperatures 10 to 55 C. The results also indicate that the instrument drifts slowly over time and should be recalibrated every 20 to 30 minutes in the field to ensure good radiometric fidelity. The instrument has now been extensively tested in the field in the United States and Australia. These in situ field measurements are being used to validate emissivity spectra recovered from the Thermal Infrared Multispectral Scanner (TIMS) and also the Australian CO2 Laser. The availability of in situ measurements is proving crucial to validation of the spectra derived from the airborne instruments since many natural surfaces cannot be easily transported back to the laboratory.

Hook, Simon J.↗
NASA NTRS1999

GPS Altimetry

The advent of satellite altimetry has greatly improved our ability to observe global ocean circulation. However, the swath of a single, nadir-viewing satellite altimeter is only a few km and the track spacing is several hundred km to resolve the two-dimensional structure of ocean eddies. Our goal is to increase spatial and temporal coverage by monitoring Global Positioning System (GPS) signals reflected from the ocean. A constellation of spacecraft would each carry a GPS receiver capable of recording 8 reflections simultaneously. The reflections are well distributed in azimuth and elevation and can be tracked continuously while the satellite is in view, and another is then acquired, as illustrated below. The diagram depicts a new approach at altimetry measurements where ocean surface reflected GPS signals are simultaneously tracked and processed in a GPS flight receiver in space. The reflected GPS signals from the ocean must be compared precisely with the direct GPS signals in order to infer the characteristics of the ocean from the combined data set. Understanding the features and accuracy of GPS altimetry measurement is crucial to establishing its suitability for oceanography. Preliminary work has enabled us to theoretically model the signal output of the correlator for a variety of system parameters such as wind speed (sea roughness), receiver height, incidence angle, receiver range and Doppler filter bandwidth and antenna gain. Expected signal-to-noise ratio has been estimated from which we have inferred, to a first approximation, the basic receiver gain requirements for a space-based altimeter and the expected range raw error. In 1998, work on a different task led to the extraction of the first reflected GPS signal observed from a spaceborne receiver during the 1995 Space Transportation System-68 (STS-68) Shuttle Radar Laboratory-2 (SRL-2) high resolution synthetic aperture radar mission. Good comparisons with our signal models have been obtained. Having established that only modest signal-to-noise ratios are obtainable unless very high gain antennas are used, we expect that single measurements might not provide an estimate of sea state parameters as accurate as that obtainable with traditional remote sensing instruments, if costs are limited. Therefore spatial and temporal averaging of many measurements is required. Since the receiving satellite tracks do not repeat, measurements in a given area will be used to refine the local solution as a function of time, and will define the spatial resolution. In order to make this instrument viable in space, we need to detect and process many scattered signals. In 1998 we made a first step at understanding what configurations of antenna gain and orientations capture the largest number of viable signals to be used in the subsequent spatial/temporal averaging process. Additional information is contained in the original.

Lichten, Stephen M.↗
DOE OSTI2023

Relativistic ultrafast electron diffraction at high repetition rates

The ability to resolve the dynamics of matter on its native temporal and spatial scales constitutes a key challenge and convergent theme across chemistry, biology, and materials science. The last couple of decades have witnessed ultrafast electron diffraction (UED) emerge as one of the forefront techniques with the sensitivity to resolve atomic motions. Increasingly sophisticated UED instruments are being developed that are aimed at increasing the beam brightness in order to observe structural signatures, but so far they have been limited to low average current beams. Here, we present the technical design and capabilities of the HiRES (High Repetition-rate Electron Scattering) instrument, which blends relativistic electrons and high repetition rates to achieve orders of magnitude improvement in average beam current compared to the existing state-of-the-art instruments. The setup utilizes a novel electron source to deliver femtosecond duration electron pulses at up to MHz repetition rates for UED experiments. Instrument response function of sub-500 fs is demonstrated with < 100 fs time resolution targeted in future. We provide example cases of diffraction measurements on solid-state and gas-phase samples, including both micro- and nanodiffraction (featuring 100 nm beam size) modes, which showcase the potential of the instrument for novel UED experiments.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2025

Instrumentation and methods for efficient time-resolved X-ray crystallography of biomolecular systems with sub-10 ms time resolution

Time-resolved X-ray crystallography has great promise to illuminate structure–function relations and key steps of enzymatic reactions with atomic resolution. The dominant methods for chemically-initiated reactions require complex instrumentation at the X-ray beamline, significant effort to operate and maintain this instrumentation, and enormous numbers (∼10 5 –10 9 ) of crystals per time point. We describe instrumentation and methods that enable high-throughput time-resolved study of biomolecular systems using standard crystallography sample supports and mail-in X-ray data collection at standard high-throughput cryocrystallography synchrotron beamlines. The instrumentation allows rapid reaction initiation by mixing of crystals and substrate/ligand solution, rapid capture of structural states via thermal quenching with no pre-cooling perturbations, and yields time resolutions in the single-millisecond range, comparable to the best achieved by any non-photo-initiated method in both crystallography and cryo-electron microscopy. Our approach to reaction initiation has the advantages of simplicity, robustness, low cost, adaptability to diverse ligand solutions and small minimum volume requirements, making it well suited to routine laboratory use and to high-throughput screening. We report the detailed characterization of instrument performance, present structures of binding of N -acetylglucosamine to lysozyme at time points from 8 ms to 2 s determined using only one crystal per time point, and discuss additional improvements that will push time resolution toward 1 ms.

Indergaard, John A. (ORCID:000000022367699X)↗
NASA NTRS1975

An evolution of X-ray astronomy instrumentation

This paper describes the growth of X-ray astronomy instrumentation from simple, single function, instruments performing survey measurements with crude spectral, spatial and temporal resolution to complex, multiple detector, instruments capable of observing selected phenomena and sources with extremely fine resolution. Examples of solar X-ray instrumentation that are discussed include OSO-IV, Apollo Telescope Mount and proposed Solar Maximum Mission instruments. Stellar X-ray instrumentation examples include UHURU, Astronomy Netherlands Satellite and HEAO-B instruments. Design details are provided and instrument parameters are compared to illustrate the evolutionary process.

Jagoda, N.↗
NASA NTRS2001

An Assessment of the Ability of Potential Space-Borne Instruments to Resolve Spatial and Temporal Variability of Atmospheric Carbon Dioxide

Mounting concern regarding the possibility that increasing carbon dioxide concentrations will initiate climate change has stimulated interest in the feasibility of measuring CO2 mixing ratios from satellites. Currently, the most comprehensive set of atmospheric CO2 data is from the NOAA CMDL cooperative air sampling network, consisting of more than 40 sites where flasks of air are collected approximately weekly. Sporadic observations in the troposphere and stratosphere from airborne in situ and flask samplers are also available. Although the surface network is extensive, there is a dearth of data in the Southern Hemisphere and most of the stations were intentionally placed in remote areas, far from major sources. Sufficiently precise satellite observations with adequate spatial and temporal resolution would substantially increase our knowledge of the atmospheric CO2 distribution and would undoubtedly lead to improved understanding of the global carbon budget. We use a 3-D chemical transport model to investigate the ability of potential satellite instruments with a variety of orbits, horizontal resolution and vertical weighting functions to capture the variation in the modeled CO2 fields. The model is driven by analyzed winds from the Goddard Data Assimilation Office. Simulated CO2 fields are compared with existing surface and aircraft data, and the effects of the model convection scheme and representation of the planetary boundary layer are considered.

Andrews, Arlyn E.↗
NASA NTRS2002

An Assessment of the Ability of Potential Satellite Instruments to Resolve Spatial and Temporal Variability of Atmospheric CO2

Sufficiently precise satellite observations with adequate spatial and temporal resolution would substantially increase our knowledge of the atmospheric CO2 distribution and would undoubtedly lead to reduced uncertainty in estimates of the global carbon budget. An overview of possible strategies for measuring CO2 from space will be presented, including IR and nearby measurements, active sensors and broad band and narrow band passive sensors. The ability of potential satellite instruments with a variety of orbits, horizontal resolution and vertical weighting functions to capture the variation in atmospheric CO2 mixing ratios will be illustrated using a combination of surface data, aircraft data and model results.

Andrews, A.↗
NASA NTRS2001

An Assessment of the Ability of Potential Spaceborne Instruments to Resolve Spatial and Temporal Variability of Atmospheric Carbon Dioxide

Mounting concern regarding the possibility that increasing carbon dioxide concentrations will initiate climate change has stimulated interest in the feasibility of measuring CO2 mixing ratios from satellites. Currently, the most comprehensive set of atmospheric CO2 data is from the NOAA CMDL cooperative air sampling network, consisting of more than 40 sites where flasks of air are collected approximately weekly. Sporadic observations in the troposphere and stratosphere from airborne in situ and flask samplers are also available. Although the surface network is extensive, there is a dearth of data in the Southern Hemisphere and most of the stations were intentionally placed in remote areas, far from major sources. Sufficiently precise satellite observations with adequate spatial and temporal resolution would substantially increase our knowledge of the atmospheric CO2 distribution and would undoubtedly lead to improved understanding of the global carbon budget. We use a 3-D chemical transport model to investigate the ability of potential satellite instruments with a variety of orbits, horizontal resolution and vertical weighting functions to capture the variation in the modeled CO2 fields. The model is driven by analyzed winds from the Goddard Data Assimilation Office. Simulated CO2 fields are compared with existing surface and aircraft data, and the effects of the model convection scheme and representation of the planetary boundary layer are considered.

Andrews, Arlyn E.↗
NASA NTRS1983

Plasma wave experiment for the ISEE-3 mission

Sensitive, high resolution plasma probes for analysis of the distribution functions and plasma wave instruments for measurements of electromagnetic and electrostatic wave modes are commonly flown together to provide information on plasma instabilities and wave particle interactions. Analysis of the data for the ISEE 3 mission is provided.

Scarf, F. L.↗
NASA NTRS1995

Non-gyrotropic proton and alpha-particle velocity distributions in the solar wind: TAUS observations and stability analysis

Ion velocity distribution functions have been measured with high time resolution by the TAUS plasma instrument on the PHOBOS mission to Mars in 1989. The unambiguous separation of protons and alpha-particles by TAUS enabled us to study the nonthermal features of their distributions separately and to analyze the stability of the distributions against excitation of waves in the cyclotron-frequency domain. Typical nonthermal features include temperature anisotropies, with T(sub perpendicular) larger than T(sub parallel), and ion beam populations drifting along the local magnetic field direction. Also, distinctly non-gyrotropic alpha-particle velocity distributions were sometimes found. Non-gyrotropy strongly changes the wave dispersion and gives rise to new growing modes, related to the coupling of the standard wave modes existing in gyrotropic plasma. It is found that for the measured non-gyrotropic ion distributions the right-hand polarized wave can also be excited by a temperature anistropy instead of the usual beam drift.

Astudillo, H. F.↗
NASA NTRS2017

Dual Ion Spectrometers and Their Calibration for the Fast Plasma Investigation on NASA's Magnetospheric Multiscale Mission

The scientific target of NASA's Magnetospheric Multiscale (MMS) mission is to study the fundamentally important phenomenon of magnetic reconnection. Theoretical models of this process predict a small size, on the order of hundred kilometers, for the ion diffusion region where ions are demagnetized at the dayside magnetopause. This region may typically sweep over the spacecraft at relatively high speeds of 50 km/s, requiring the fast plasma investigation (FPI) instrument suite to have an extremely high time resolution for measurements of the 3D particle distribution functions. As part of the FPI on MMS, the 16 dual ion spectrometers (DIS) will provide fast (150 ms) 3D ion velocity distributions, from 10 to 30,000 eV/q, by combining the measurements from four dual spectrometers on each of four MMS spacecraft. For any multispacecraft mission, the response uniformity among the spectrometer set assumes an enhanced importance. Due to these demanding instrument requirements and the effort of calibrating more than 32 sensors (16 × 2) within a tight schedule, a highly systematic and precise calibration was required for measurement repeatability. To illustrate how this challenge was met, a brief overview of the FPI DIS was presented with a detailed discussion of the calibration method of approach and implementation. Finally, a discussion of DIS performance results, their unit-to-unit variation, and the lessons learned from this calibration effort are presented.

Coffey, V. N.↗
DOE OSTI2026

New Directions in Focused Ion Beam Induced Deposition for the Nanoprinting of Functional 3D Heterostructures

The focused ion beam (FIB) microscope is well established as a high-resolution machining instrument capable of site-selectively removing material down to the nanoscale. Beyond subtractive processing, however, the FIB can also add material via a technique known as focused ion beam induced deposition (FIBID). Using FIBID, the FIB can thus be employed for the direct-write of complex nanostructures. This work explores new directions in three-dimensional FIBID nanoprinting, harnessing unique features of helium and neon FIBs. In particular, the superior spatial resolution of these novel FIBs is leveraged to fabricate precise multimaterial architectures, an isotope effect is used to create satellite deposits, and dose-controlled implantation of the gaseous ions is used to engineer internal voids. In the context of voids, the fabrication of hollow nanopillars by helium-FIBID due to concurrent milling (as shown previously by others) is revisited. Insight into the chemical and structural composition of the nanostructures is obtained using advanced electron microscopy, accurately revealing buried interfaces, crystallite distributions, chemical compositions, and material transformations. Next-generation devices and technologies that could be enabled by the novel heterostructures demonstrated here are discussed, setting the stage for the potential evolution of FIBID into a versatile platform for functional nanomaterials design and fabrication.

FIBID↗
NASA NTRS1978

Thorium concentrations in the lunar surface. II - Deconvolution modeling and its application to the regions of Aristarchus and Mare Smythii

The broad angular response which characterized the Apollo gamma ray spectrometer resulted in a loss of spatial resolution and some of the contrast in determining surface concentrations within lunar regions small compared to the field of view. A deconvolution technique has been developed which removes much of this instrumental effect, thereby improving both spatial resolution and accuracy at the cost of a loss in precision. Geometric models of regional thorium distribution are convoluted through the response function of the instrument to yield a predicted distribution which is compared with the observed data field for quality of fit. Application to areas which include Aristarchus and Mare Smythii confirm some geological relationships and fail to support others.

Haines, E. L.↗