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NASA NTRS2011

FTIR Analysis of Aerogel Keystones from the Stardust Interstellar Dust Collector: Assessment of Terrestrial Organic Contamination and X-Ray Microprobe Beam Damage

The Stardust Interstellar Dust Collector (SIDC) was intended to capture and return contemporary interstellar dust. The approx.0.1 sq m collector was composed of aerogel tiles (85% of the collecting area) and aluminum foils and was exposed to the interstellar dust stream for a total exposure factor of 20 sq m day. The Stardust Interstellar Preliminary Examination (ISPE) is a consortium-based project to characterize the collection using nondestructive techniques. Sandford et al. recently assessed numerous potential sources of organic contaminants in the Stardust cometary collector. These contaminants could greatly complicate the analysis and interperetation of any organics associated with interstellar dust, particularly because signals from these particles are expected to be exceedingly small. Here, we present a summary of FTIR analyses of over 20 aerogel keystones, many of which contained candidates for interstellar dust.

Zolensky, M. E.↗
NASA NTRS1988

Stochastic histories of refractory interstellar dust

Histories of refractory interstellar dust particles (IDPs) are calculated. The profile of a particle population is assembled from a large number of stochastic, or Monte Carlo, histories of single particles; the probabilities for each of the events that may befall a given particle are specified, and the particle's history is unfolded by a sequence of random numbers. The assumptions that are made and the techniques of the calculation are described together with the results obtained. Several technical demonstrations are presented.

Liffman, Kurt↗
NASA NTRS1988

Properties of interstellar dust in reflection nebulae

Observations of interstellar dust in reflection nebulae are the closest analog in the interstellar medium to studies of cometary dust in our solar system. The presence of a bright star near the reflection nebula dust provides the opportunity to study both the reflection and emission characteristics of interstellar dust. At 0.1 to 1 micrometer, the reflection nebula emission is due to starlight scattered by dust. The albedo and scattering phase function of the dust is determined from observations of the scattered light. At 50 to 200 micrometers, thermal emission from the dust in equilibrium with the stellar radiation field is observed. The derived dust temperature determines the relative values of the absorption coefficient of the dust at wavelengths where the stellar energy is absorbed and at far infrared wavelengths where the absorbed energy is reradiated. These emission mechanisms directly relate to those seen in the near and mid infrared spectra of comets. In a reflection nebula the dust is observed at much larger distances from the star than in our solar system, so that the equilibrium dust temperature is 50 K rather than 300 K. Thus, in reflection nebulae, thermal emission from dust is emitted at 50 to 200 micrometer.

Sellgren, Kristin↗
NASA NTRS2003

The Nature of Interstellar Dust

The STARDUST mission is designed to collect dust the coma of comet Wild 2 and to collect interstellar dust on a second set of collectors. We have a reasonable idea of what to expect from the comet dust collection because the research community has been studying interplanetary dust particles for many years. It is less clear what we should expect from the interstellar dust. This presentation discusses what we might expect to find on the STARDUST interstellar dust collector.

Huss, G. R.↗
NASA NTRS1986

Composition, structure and chemistry of interstellar dust

The observational constraints on the composition of the interstellar dust are analyzed. The dust in the diffuse interstellar medium consists of a mixture of stardust (amorphous silicates, amorphous carbon, polycyclic aromatic hydrocarbons, and graphite) and interstellar medium dust (organic refractory material). Stardust seems to dominate in the local diffuse interstellar medium. Inside molecular clouds, however, icy grain mantles are also important. The structural differences between crystalline and amorphous materials, which lead to differences in the optical properties, are discussed. The astrophysical consequences are briefly examined. The physical principles of grain surface chemistry are discussed and applied to the formation of molecular hydrogen and icy grain mantles inside dense molecular clouds. Transformation of these icy grain mantles into the organic refractory dust component observed in the diffuse interstellar medium requires ultraviolet sources inside molecular clouds as well as radical diffusion promoted by transient heating of the mantle. The latter process also returns a considerable fraction of the molecules in the grain mantle to the gas phase.

Tielens, Alexander G. G. M.↗
NASA NTRS1990

From interstellar dust to comets - A unification of observational constraints

The interstellar dust model of comets is numerically worked out to satisfy simultaneously several basic constraints provided by observations of Comet Halley, and to derive the porosity of coma dust. The observational constraints are (1) the strengths of the 3.4 and 9.7 micron emission bands, (2) the shape of the 9.7 micron band, (3) the amount of silicates relative to organic materials, and (4) the mass distribution of the dust. The method used involves precise calculations of temperatures and the emission characteristics of porous aggregates of interstellar dust as a function of their mass, porosity, and distance to the sun and the wavelength. The results indicate that coma dust has a porosity in the range 0.93-0.975, i.e., a packing factor of 0.07 or less, consistent with independent observations of comet densities of 0.6 to 0.26 g/cu cm and meteor densities of less than 0.2 g/cu cm.

Greenberg, J. Mayo↗
NASA NTRS1989

Stochastic evolution of refractory interstellar dust during the chemical evolution of a two-phase interstellar medium

The evolution course of refractoary interstellar dust during the chemical evolution of a two-phase interstellar medium (ISM) is studied using a simple model of the chemical evolution of ISM. It is assumed that, in this medium, the stars are born in molecular clouds, but new nucleosynthesis products and stellar return are entered into a complementary diffuse medium; the well-mixed matter of each interstellar phase is repeatedly cycled stochastically through the complementary phase and back. The dust is studied on a particle-by-particle bases as it is sputtered by shock waves in the diffuse medium, accretes an amorphous mantle of gaseous refractory atoms while its local medium joins the molecular cloud medium, and encounters the possibility of astration within molecular clouds. Results are presented relevant to the size spectrum of accreted mantles, its age spectrum and the distinction among its several lifetimes, depletion factors of refractory atoms in the diffuse gas, and isotopic anomalies.

Liffman, Kurt↗
NASA NTRS1984

Interstellar dust, comets, comet dust and carbonaceous meteorites

Evidence is adduced to show that comets, and carbonaceous meteorites have a common origin via aggregation of interstellar dust. The dust to gas ratio for comets and the trend in its variation with solar distance is derived from the sequential evaporation of the various comet dust constituents. The 'missing carbon' in comets is explained as residing predominantly in the approximately 20 percent fraction of the comets consisting of the complex organic component of interstellar dust. The C-12/C-13 isotopic ratios in interstellar dust, comets and carbonaceous meteorites are linked by dividing the carbon into its 'pure' and molecular parts. The silicate signature in circumstellar, interstellar, comet and interplanetary dust is compared.

Greenberg, J. M.↗
NASA NTRS1992

Interstellar dust from the Milky Way to the Magellanic Clouds

Interstellar dust in the Magellanic Clouds, with a weak or nearly absent 2175 A extinction feature, may be of interest in studies of galaxies in early stages of chemical evolution. To this inquiry, we extend the graphite-silicate grain model, introduced by Mathis, Rumpl, and Nordsieck and developed by Draine and Lee (1984) from the Milky Way to the Magellanic Clouds. We find that the empirical extinction curves in the Large and Small Magellanic Clouds can be reproduced by adjusting only the relative abundances of graphite and silicate grains, while leaving all other model properties fixed to those appropriate for the Galactic extinction curve. Using the graphite-silicate models, we calculate the absorption and scattering optical depths, the mass-density ratio of interstellar dust to neutral hydrogen, and the Kramers-Kronig relation for all three galaxies. We also present a fitting function for the three extinction curves, valid not only over the observed range of wavelengths but also over the full range as predicted by the models. All the quantities we derived here are independent of the dust-to-gas ratios in the Milky Way and the Magellanic Clouds, and can be applied to other galaxies if they contain Galactic or Magellanic-type dust.

Pei, Yichuan C.↗
NASA NTRS2014

Final Reports of the Stardust ISPE: Seven Probable Interstellar Dust Particles

The Stardust spacecraft carried the first spaceborne collector specifically designed to capture and return a sample of contemporary interstellar dust to terrestrial laboratories for analysis [1]. The collector was exposed to the interstellar dust stream in two periods in 2000 and 2002 with a total exposure of approximately 1.8 10(exp 6) square meters sec. Approximately 85% of the collector consisted of aerogel, and the remainder consisted of Al foils. The Stardust Interstellar Preliminary Examination (ISPE) was a consortiumbased effort to characterize the collection in sufficient detail to enable future investigators to make informed sample requests. Among the questions to be answered were these: How many impacts are consistent in their characteristics with interstellar dust, with interplanetary dust, and with secondary ejecta from impacts on the spacecraft? Are the materials amorphous or crystalline? Are organics detectable? An additional goal of the ISPE was to develop or refine the techniques for preparation, analysis, and curation of these tiny samples, expected to be approximately 1 picogram or smaller, roughly three orders of magnitude smaller in mass than the samples in other small particle collections in NASA's collections - the cometary samples returned by Stardust, and the collection of Interplanetary Dust Particles collected in the stratosphere.

Allen, Carlton↗
NASA NTRS1988

Interstellar dust and the IUE

Understanding of the physical nature of interstellar dust, as modified by observations of extinction obtained with IUE, is considered. Properties of extinction laws along various lines of sight, with emphasis on the bump, are reviewed. Correlations of the UV and optical/near infrared extinction are discussed. Other diagnostics of interstellar dust, such as the near infrared emission bands, polarization, far infrared thermal emission, and depletions are mentioned, and theories are summarized.

Mathis, John S.↗
NASA NTRS1988

Monte-Carlo histories of refractory interstellar dust

Monte-carlo histories of 6 x 10 to the 6th individual dust particles injected uniformly from stars into the interstellar medium during a 6 x 10 to the 9th year history are calculated. The particles are given a two-phase internal structure of successive thermal condensates, and are distributed in initial radius as 1/a-cubed over the value of a between 0.01 and 0.1 micron. The evolution of this system illustrates the distinction between several different lifetimes for interstellar dust. Most are destroyed, but some grow in size. Several important consequences for interstellar dust are described.

Clayton, D. D.↗
NASA NTRS1991

Cometary and interstellar dust grains - Analysis by ion microprobe mass spectrometry and other techniques

A survey of microanalytical measurements on interplanetary dust particles (IDPs) and interstellar dust grains from primitive meteorites is presented. Ion-microprobe mass spectrometry with its capability to determine isotopic compositions of many elements on a micron spatial scale has played a special role. Examples are measurements of H, N, and O isotopes and refractory trace elements in IDPs; C, N, Mg, and Si isotopes in interstellar SiC grains; and C and N isotopes and H, N, Al, and Si concentrations in interstellar graphite grains.

Zinner, Ernst↗
NASA NTRS1999

Deflection of the local interstellar dust flow by solar radiation pressure

Interstellar dust grains intercepted by the dust detectors on the Ulysses and Galileo spacecrafts at heliocentric distances from 2 to 4 astronomical units show a deficit of grains with masses from 1 x 10(-17) to 3 x 10(-16) kilograms relative to grains intercepted outside 4 astronomical units. To divert grains out of the 2- to 4-astronomical unit region, the solar radiation pressure must be 1.4 to 1.8 times the force of solar gravity. These figures are consistent with the optical properties of spherical or elongated grains that consist of astronomical silicates or organic refractory material. Pure graphite grains with diameters of 0.2 to 0.4 micrometer experience a solar radiation pressure force as much as twice the force of solar gravity.

Cosmic Dust↗
NASA NTRS2013

Stardust Interstellar Preliminary Examination II: Curating the Interstellar Dust Collector, Picokeystones, and Sources of Impact Tracks

We discuss the inherent difficulties that arise during "ground truth" characterization of the Stardust interstellar dust collector. The challenge of identifying contemporary interstellar dust impact tracks in aerogel is described within the context of background spacecraft secondaries and possible interplanetary dust particles and beta-meteoroids. In addition, the extraction of microscopic dust embedded in aerogel is technically challenging. Specifically, we provide a detailed description of the sample preparation techniques developed to address the unique goals and restrictions of the Interstellar Preliminary Exam. These sample preparation requirements and the scarcity of candidate interstellar impact tracks exacerbate the difficulties. We also illustrate the role of initial optical imaging with critically important examples, and summarize the overall processing of the collection to date.

Dust↗
NASA NTRS2006

The Origin and Evolution of Interstellar Dust

In this lecture I will discuss the many different manifestation of interstellar dust, and current dust models that satisfy interstellar extinction, diffuse infrared emission, and interstellar abundances constraints. Dust is made predominantly in AGB stars and Type I1 supernovae, and I will present observational evidence for the presence of dust in these sources. I will then present chemical evolution models that follow the abundance of dust which is determined by the combined processes of formation, destruction by interstellar shock waves, and accretion in molecular clouds. The model will be applied to the evolution of PAHs and the evolution of dust in the high-redshift galaxy (z=6.42) JD11.

Dwek, Eli↗
NASA NTRS2014

Stardust Interstellar Preliminary Examination V: XRF Analyses of Interstellar Dust Candidates at ESRF ID13

Here, we report analyses by synchrotron X-ray fluorescence microscopy of the elemental composition of eight candidate impact features extracted from the Stardust Interstellar Dust Collector (SIDC). Six of the features were unambiguous tracks, and two were crater-like features. Five of the tracks are so-called midnight tracks that is, they had trajectories consistent with an origin either in the interstellar dust stream or as secondaries from impacts on the Sample Return Capsule (SRC). In a companion paper reporting synchrotron X-ray diffraction analyses of ISPE candidates, we show that two of these particles contain natural crystalline materials: the terminal particle of track 30contains olivine and spinel, and the terminal particle of track 34 contains olivine. Here, we show that the terminal particle of track 30, Orion, shows elemental abundances, normalized to Fe, that are close to CI values, and a complex, fine-grained structure. The terminal particle of track 34, Hylabrook, shows abundances that deviate strongly from CI, but shows little fine structure and is nearly homogenous. The terminal particles of other midnight tracks, 29 and 37, had heavy element abundances below detection threshold. A third, track28, showed a composition inconsistent with an extraterrestrial origin, but also inconsistent with known spacecraft materials. A sixth track, with a trajectory consistent with secondary ejecta from an impact on one of the spacecraft solar panels, contains abundant Ce and Zn. This is consistent with the known composition of the glass covering the solar panel. Neither crater-like feature is likely to be associated with extraterrestrial materials. We also analyzed blank aerogel samples to characterize background and variability between aerogel tiles. We found significant differences in contamination levels and compositions, emphasizing the need for local background subtraction for accurate quantification.

Stardust↗