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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
NASA NTRS2006

Compressive Failure of Fiber Composites under Multi-Axial Loading

This paper examines the compressive strength of a fiber reinforced lamina under multi-axial stress states. An equilibrium analysis is carried out in which a kinked band of rotated fibers, described by two angles, is sandwiched between two regions in which the fibers are nominally straight. Proportional multi-axial stress states are examined. The analysis includes the possibility of bifurcation from the current equilibrium state. The compressive strength of the lamina is contingent upon either attaining a load maximum in the equilibrium response or satisfaction of a bifurcation condition, whichever occurs first. The results show that for uniaxial loading a non-zero kink band angle beta produces the minimum limit load. For multi-axial loading, different proportional loading paths show regimes of bifurcation dominated and limit load dominated behavior. The present results are able to capture the beneficial effect of transverse compression in raising the composite compressive strength as observed in experiments.

Basu, Shiladitya↗
DOE OSTI2024

Generalized grain boundary constitutive description implemented in a strain-gradient large-strain FFT-based formulation: Application to nano-metallic laminates

Herein this paper presents a general treatment of grain boundary constitutive behavior in the context of strain-gradient (SG) plasticity, and its numerical implementation in a large-strain (LS) elasto-viscoplastic (EVP) fast Fourier transform (FFT)-based micromechanical model. Two novel grain boundary constitutive equations are proposed, allowing for more accurate description of the Burgers vector flow at the grain boundary. The capabilities of the generalized SG-LS-EVPFFT formulation are illustrated for the case of kink-band formation during layer-parallel compression of nano-metallic laminates (NMLs), requiring consideration of the interaction between dislocations and interfaces.

36 MATERIALS SCIENCE↗
NASA NTRS1992

Mechanisms of compressive failure in woven composites and stitched laminates

Stitched laminates and angle interlock woven composites have been studied in uniaxial, in-plane, monotonic compression. Failure mechanisms have been found to depend strongly on both the reinforcement architecture and the degree of constraint imposed by the loading grips. Stitched laminates show higher compressive strength, but are brittle, possessing no load bearing capacity beyond the strain for peak load. Post-mortem inspection shows a localized shear band of buckled and broken fibers, which is evidently the product of an unstably propagating kink band. Similar shear bands are found in the woven composites if the constraint of lateral displacements is weak; but, under strong constraint, damage is not localized but distributed throughout the gauge section. While the woven composites tested are weaker than the stitched laminates, they continue to bear significant loads to compressive strains of approx. 15 percent, even when most damage is confined to a shear band.

Cox, B. N.↗
NASA NTRS2024

Microstructural Evolution of the Civet Cat Norite (72255)

The ‘Civet Cat Norite’ is a ~ 2.5 cm clast within the Apollo impact melt breccia sample 72255 collected during Apollo 17 EVA 2 at Boulder 1. The norite is primarily composed of plagioclase and orthopyroxene with fine-scale exsolution lamellae of augite. The plagioclase and orthopyroxene (OPX) coexist with minor quartz and augitic clinopyroxene (CPX), and accessory apatite, baddeleyite, chromite, ilmenite, loveringite, merrillite, rutile and zircon. The major minerals range from 1 to 4 mm in size and show a cataclastic texture indicated by banding of the light and dark phases]. The chemical composition of the orthopyroxene, augitic exsolution lamellae, and exsolved oxides suggest the norite crystallized in the lower crust of the Moon (10 – 70 km depth) and was subsequently excavated by impact(s). Shock pressure estimates for the norite range from 15 – 35 GPa based on maskeleynite formation within the plagioclase, kink banding in pyroxenes, and granular recrystallization in the accessory phosphates. Previous Rb-Sr and 40 Ar/ 39 Ar analyses recalculated with modern decay constants yield relatively young ages of 4.16 ± 0.05 Ga and 3.99 ± 0.03 Ga, respectively. However, recent U-Pb analyses of some zircon grains from within the Civet Cat yield an age of 4.45 ± 0.03 Ga. While this is the oldest age for any rock recovered from the Moon, the full age spread of zircon from the Civet Cat range from ca. 4.46 to 4.02 Ga, indicating variable Pb-loss and complicating interpretation of the primary age. Recent atom probe analyses indicate minimal Pb mobilization within the oldest zircon grain from Civet Cat, supporting the interpretation that these ancient zircon ages reflect the age of the norite, rather than an apparent antiquity caused by reverse discordance. To investigate the potential antiquity and deep crustal origin of the Civet Cat norite, we have undertaken high resolution microstructural analyses of the major, minor, and accessory minerals to characterize the primary igneous textures and secondary overprinting by impact and metamorphism. The employed analytical techniques include scanning electron microscope-based electron backscatter diffraction (EBSD) analyses, electron probe microanalyzer (EPMA) chemical analyses, and transmission electron microscopy (TEM) of pyroxene, plagioclase, quartz, zircon, and phosphates.

T M Erickson↗
DOE OSTI2023

Unraveling kinking: A plasticity enhancing failure mode in high strength nano metallic laminates

Kinking is an important and plasticity-enhancing deformation/failure mode in numerous mechanically anisotropic materials including high-strength nano metallic laminates (NMLs). However, our current limited understanding of the mechanics of kinking and its dependence on microstructural attributes is insufficient for thoroughly comprehending and eventually being able to control failure behaviors of materials. In this study, we investigate kinking dependencies on microstructural attributes in NMLs via in situ micropillar compression, multiscale microstructure characterization, dislocation dynamic simulations, and crystal plasticity modeling. Additionally, by examining several NML systems (Cu/Fe, Ag/Fe, Al-4Mg/Fe), we demonstrate that the development of internal stresses during loading activates local layer-parallel glide triggering kinking in NMLs. Furthermore, this work reveals the effect of key microstructural features including layer thickness, layer waviness, interface barrier strength, and work hardening capacity on kink band formation in NMLs. More broadly, our efforts represent a generically applicable approach for probing large-strain deformation behavior of complex materials via synergetic modeling and experimental efforts.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Effect of tension during sulfonation stabilization for UHMWPE-derived carbon fibers

Polyethylene is a promising low-cost alternative precursor material for carbon fiber production, but it has yet to show mechanical properties near or surpassing polyacrylonitrile-derived carbon fibers. The high molecular weight and order of ultra-high molecular weight polyethylene (UHMWPE) may offer a pathway to realizing this promise by enabling long-range graphitic structure formation and superior mechanical properties. The tension applied during the precursor stabilization process is crucial to maintaining the shape of the fibers during the conversion process, but no published study has yet probed the relationship between sulfonation tension and carbon fiber microstructure and mechanical properties. In this work, a logarithmic sweep of tensile stress was applied to UHMWPE fibers during the stabilization process followed by carbonization. Increasing tension significantly reduced fiber shrinkage, resulted in straighter fibers with less severe kink bands, and greatly improved the mechanical properties of the fibers. Raman spectroscopy and X-ray diffraction revealed that in all cases the carbon fibers were largely amorphous, but increasing tension resulted in increased size and alignment of the turbostratic crystallites with the fiber axis. Large voids were present in the sample fibers, so the Griffith-Irwin relation was employed to predict the potential ultimate tensile strength of the fibers with voids reduced to sizes comparable to commercially produced fibers. Furthermore, this work demonstrates the importance of tension applied during the stabilization of polyethylene fibers for carbon fiber production and establishes a framework for achieving high mechanical properties from these precursors.

36 MATERIALS SCIENCE↗
NASA NTRS1973

Fatigue hardening in niobium single crystals.

Nb single crystals of various orientations were cyclically deformed in tension-compression under strain control. At low strain amplitudes all crystals oriented for single slip and some oriented for multiple slip showed a two stage hardening. When present, the first stage was characterized with almost no cyclic work hardening. The rate of hardening in the second stage increased with strain amplitude and the amount of secondary slip. In crystals oriented for single slip kink bands developed on their side faces during rapid hardening stage which resulted in considerable amount of asterism in Laue spots. A cyclic stress-strain curve independent of prior history was found to exist which was also independent of crystal orientation. Furthermore, this curve differed only slightly from that of polycrystalline Nb obtained from data in literature.

Doner, M.↗
NASA NTRS1984

Compression failure mechanisms in unidirectional composites

Compression failure mechanisms in unidirectional composites were examined. Possible failure modes of constituent materials are summarized and analytical models for fiber microbuckling are reviewed from a unified viewpoint. Due to deficiencies in available models, a failure model based on nonlinear properties and initial fiber curvature is proposed. The effect of constituent properties on composite compression behavior was experimentally investigated using two different graphite fibers and four different epoxy resins. The predominant microscopic scale failure mode was found to be shear crippling. In a soft resin, shear crippling was in the form of buckling of fibers on a microscopic scale. However, stiff resins failure was characterized by the formation of a kink band. For unidirectional laminates, compressive strength, and compressive modulus to a less extent, were found to increase with increasing magnitude of resin modulus. The change in compressive strength with resin modulus was predicted using the proposed nonlinear model.

Hahn, H. T.↗
NASA NTRS1986

Compression failure mechanisms in unidirectional composites

Compression failure mechanisms in unidirectional composites were examined. Possible failure modes of constituent materials are summarized and analytical models for fiber microbuckling are reviewed from a unified viewpoint. Due to deficiencies in available models, a failure model based on nonlinear properties and initial fiber curvature is proposed. The effect of constituent properties on composite compression behavior was experimentally investigated using two different graphite fibers and four different epoxy resins. The predominant microscopic scale failure mode was found to be shear crippling. In a soft resin, shear crippling was in the form of buckling of fibers on a microscopic scale. However, stiff resins failure was characterized by the formation of a kink band. For unidirectional laminates, compressive strength, and compressive modulus to a less extent, were found to increase with increasing magnitude of resin modulus. The change in compressive strength with resin modulus was predicted using the proposed nonlinear model.

Hahn, H. T.↗
NASA NTRS1991

Studies of fiber-matrix adhesion on compression strength

A study was initiated on the effect of the matrix polymer and the fiber matrix bond strength of carbon fiber polymer matrix composites. The work includes tests with micro-composites, single ply composites, laminates, and multi-axial loaded cylinders. The results obtained thus far indicate that weak fiber-matrix adhesion dramatically reduces 0 degree compression strength. Evidence is also presented that the flaws in the carbon fiber that govern compression strength differ from those that determine fiber tensile strength. Examination of post-failure damage in the single ply tests indicates kink banding at the crack tip.

Bascom, Willard D.↗
NASA NTRS1992

Mechanisms of compressive failure in 3D composites

The present study of angle-interlock woven polymer matrix composite behavior under uniaxial monotonic compression notes these materials to be macroscopically ductile, with compressive strains in failure that can exceed 15 percent. Some of the tests conducted on stitched laminates indicated brittle behavior. Woven composite failure mechanisms have been studied by a combination of optical microscopy, moire interferometry, stereoscopy, and digital image comparisons; the critical failure event was in all cases a kink band formation in the primary load-bearing axial rows.

Cox, B. N.↗
NASA NTRS1994

Effects of fiber, matrix, and interphase on carbon fiber composite compression strength

The major goal of this project was to obtain basic information on compression failure properties of carbon fiber composites. To do this, we investigated fiber effects, matrix effects, and fiber/matrix interface effects. Using each of nine fiber types, we prepared embedded single-fiber specimens, single-ply specimens, and full laminates. From the single-fiber specimens, in addition to the standard fragmentation test analysis, we were able to use the low crack density data to provide information about the distribution of fiber flaws. The single-ply specimens provided evidence of a correlation between the size of kink band zones and the quality of the interface. Results of the laminate compression experiments mostly agreed with the results from single-ply experiments, although the ultimate compression strengths of laminates were higher. Generally, these experiments showed a strong effect of interfacial properties. Matrix effects were examined using laminates subjected to precracking under mixed-mode loading conditions. A large effect of precracking conditions on the mode 1 toughness of the laminates was found. In order to control the properties of the fiber/matrix interface, we prepared composites of carbon fiber and polycarbonate and subjected these to annealing. The changes in interfacial properties directly correlated with changes in compression strength.

Nairn, John A.↗
NASA NTRS2005

Influence of Compression and Shear on the Strength of Composite Laminates with Z-Pinned Reinforcement

The influence of compression and shear loads on the strength of composite laminates with z-pins is evaluated parametrically using a 2D Finite Element Code (FLASH). Meshes were generated for three unique combinations of z-pin diameter and density. A laminated plate theory analysis was performed on several layups to determine the bi-axial stresses in the zero degree plies. These stresses, in turn, were used to determine the magnitude of the relative load steps prescribed in the FLASH analyses. Results indicated that increasing pin density was more detrimental to in-plane compression strength than increasing pin diameter. FLASH results for lamina with z-pins were consistent with the closed form results, and FLASH results without z-pins, if the initial fiber waviness due to z-pin insertion was added to the fiber waviness in the material to yield a total misalignment. Addition of 10% shear to the compression loading significantly reduced the lamina strength compared to pure compression loading. Addition of 50% shear to the compression indicated shear yielding rather than kink band formation as the likely failure mode. Two different stiffener reinforced skin configurations with z-pins, one quasi-isotropic and one orthotropic, were also analyzed. Six unique loading cases ranging from pure compression to compression plus 50% shear were analyzed assuming material fiber waviness misalignment angles of 0, 1, and 2 degrees. Compression strength decreased with increased shear loading for both configurations, with the quasi-isotropic configuration yielding lower strengths than the orthotropic configuration.

O'Brien, T. Kevin↗
NASA NTRS2005

Influence of Compression and Shear on the Strength of Composite Laminates With Z-Pinned Reinforcement

The influence of compression and shear loads on the strength of composite laminates with z-pins is evaluated parametrically using a 2D Finite Element Code (FLASH) based on Cosserat couple stress theory. Meshes were generated for three unique combinations of z-pin diameter and density. A laminated plate theory analysis was performed on several layups to determine the bi-axial stresses in the zero degree plies. These stresses, in turn, were used to determine the magnitude of the relative load steps prescribed in the FLASH analyses. Results indicated that increasing pin density was more detrimental to in-plane compression strength than increasing pin diameter. Compression strengths of lamina without z-pins agreed well with a closed form expression derived by Budiansky and Fleck. FLASH results for lamina with z-pins were consistent with the closed form results, and FLASH results without z-pins, if the initial fiber waviness due to z-pin insertion was added to the fiber waviness in the material to yield a total misalignment. Addition of 10% shear to the compression loading significantly reduced the lamina strength compared to pure compression loading. Addition of 50% shear to the compression indicated shear yielding rather than kink band formation as the likely failure mode. Two different stiffener reinforced skin configurations with z-pins, one quasi-isotropic and one orthotropic, were also analyzed. Six unique loading cases ranging from pure compression to compression plus 50% shear were analyzed assuming material fiber waviness misalignment angles of 0, 1, and 2 degrees. Compression strength decreased with increased shear loading for both configurations, with the quasi-isotropic configuration yielding lower strengths than the orthotropic configuration.

OBrien, T. Kevin↗
NASA NTRS2005

Influence of Compression and Shear on the Strength of Composite Laminates with Z-Pinned Reinforcement

The influence of compression and shear loads on the strength of composite laminates with z-pins is evaluated parametrically using a 2D Finite Element Code (FLASH) based on Cosserat couple stress theory. Meshes were generated for three unique combinations of z-pin diameter and density. A laminated plate theory analysis was performed on several layups to determine the bi-axial stresses in the zero degree plies. These stresses, in turn, were used to determine the magnitude of the relative load steps prescribed in the FLASH analyses. Results indicated that increasing pin density was more detrimental to in-plane compression strength than increasing pin diameter. Compression strengths of lamina without z-pins agreed well with a closed form expression derived by Budiansky and Fleck. FLASH results for lamina with z-pins were consistent with the closed form results, and FLASH results without z-pins, if the initial fiber waviness due to z-pin insertion was added to the fiber waviness in the material to yield a total misalignment. Addition of 10% shear to the compression loading significantly reduced the lamina strength compared to pure compression loading. Addition of 50% shear to the compression indicated shear yielding rather than kink band formation as the likely failure mode. Two different stiffener reinforced skin configurations with z-pins, one quaiisotropic and one orthotropic, were also analyzed. Six unique loading cases ranging from pure compression to compression plus 50% shear were analyzed assuming material fiber waviness misalignment angles of 0, 1, and 2 degrees. Compression strength decreased with increased shear loading for both configurations, with the quasi-isotropic configuration yielding lower strengths than the orthotropic configuration.

O'Brien, T. Kevin↗
NASA NTRS2018

Validation of a Mesoscale Fiber Kinking Model Through Test and Analysis of Double Edge Notch Compression Specimens

Tests and analyses were conducted on a series of geometrically-scaled double edge notch compression specimens to validate the capability of the fiber-kinking model in the NASA continuum damage mechanics code for progressive damage analysis, CompDam. The tests and analyses focused on the fiber-kinking damage mechanism, which is of critical importance for predicting accurately longitudinal compression failure in carbon fiber reinforced polymer laminates. The fiber-kinking model in CompDam was augmented with a new capability to represent a hardening response once a kink band has fully formed, enabling prediction of band broadening. Correlation of the test and analysis results showed agreement in stiffness and strength with less than 10% error. The analysis predicts the same sequence of events leading to ultimate failure that was found in the test. The overall excellent correlation in terms of stiffness, strength, and failure process validates the capability of the model for predicting longitudinal compression failure in notched laminates with cross-ply layups.

Bergan, Andrew C.↗
NASA NTRSDate not supplied

TPSAS-NF1676L-32167-DND

Fiber Kinking Theory (FKT): Budiansky proposed that kink bands are a result of an initial (infinitely wide) band of misaligned fibers, nonlinear material behavior under shear loading, and accounting for large rotations of the fibers. CompDam is a NASA Langley CDM code that uses the deformation gradient, particular attention paid to kinematics of cracking.

Andrew Bergan↗
DOE OSTI2025

Diverse Manifestations of Electron-Phonon Coupling in a Kagome Superconductor

Recent angle-resolved photoemission spectroscopy (ARPES) experiments on the kagome metal CsV_{3}Sb_{5} revealed distinct multimodal dispersion kinks and nodeless superconducting gaps across multiple electron bands. The prominent photoemission kinks suggest a definitive coupling between electrons and certain collective modes, yet the precise nature of this interaction and its connection to superconductivity remain to be established. Here, employing the state-of-the-art ab initio many-body perturbation theory computation, we present direct evidence that electron-phonon (e-ph) coupling induces the multimodal photoemission kinks in CsV_{3}Sb_{5}, and profoundly, drives the nodeless s-wave superconductivity, showcasing the diverse manifestations of the e-ph coupling. Our calculations well capture the experimentally measured kinks and their fine structures, and reveal that vibrations from different atomic species dictate the multimodal behavior. Results from anisotropic GW-Eliashberg equations predict a phonon-mediated superconductivity with nodeless s-wave gaps, in excellent agreement with various ARPES and scanning tunneling spectroscopy measurements. Despite the universal origin of the e-ph coupling, the contributions of several characteristic phonon vibrations vary in different phenomena, highlighting a versatile role of e-ph coupling in shaping the low-energy excitations of kagome metals.

Electron-phonon coupling↗