Temperature controller for LEED experiments.
Temperature controller for establishing sample temperature as time function or other variable for use in low energy electron diffraction /LEED/ experiments
SEARCH · Search NASA
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Temperature controller for establishing sample temperature as time function or other variable for use in low energy electron diffraction /LEED/ experiments
Low energy electron diffraction study of adhesion of various materials to nickel surface
Adhesion of gold on copper planes studied with low energy electron diffraction
Thermal faceting of tungsten single crystal surfaces in oxygen, using vibrating-capacitor work function probe with low energy electron diffraction
Low energy electron diffraction oxygen adsorption kinetics on planes of tungsten at coverages below monolayer and work function measurements
Cu, W and oxidized W adhesion to Ni surface, examining before and after adhesion contact with low energy electron diffraction
Low energy electron diffraction structures due to Re crystal surface interaction with CO and molecular oxygen at high temperatures
Fcc metals surface changes following adhesion using low energy electron diffraction /LEED/, relating intersurface metal transfer to applied adhesive force
Low energy electron diffraction pattern from surface steps and facets resulting from recrystallization of Re single crystal
Hydrogen adsorption and coadsorption with oxygen on W single crystal surface measured by mass spectroscopy and low energy electron diffraction method
Auger emission spectroscopy, low energy electron diffraction, sputtering studies, and adhesion and friction experiments on single crystals of Cu-Sn, Cu-Al, and Fe-Al alloys
Free surface equilibrium segregation in solid solutions of Cu-Al alloys single crystals by Auger electron spectroscopy and low energy electron diffraction
Surface segregation, adhesion and friction of monocrystalline Cu-Al, Cu-Sn and Fe-Al alloys from Auger emission spectroscopy and low energy electron diffraction experiments
The field of surface science has undergone intense revitalization with the introduction of low-energy electron diffraction, Auger electron spectroscopy, ellipsometry, and other surface analytical techniques which have been sophisticated within the last decade. These developments have permitted submono- and monolayer structure analysis as well as chemical identification and quantitative analysis. The application of a number of these techniques to the solution of problems in the fields of friction, lubrication, and wear are examined in detail for the particular case of iron; and in general to illustrate how the accumulation of pure data will contribute toward the establishment of physiochemical concepts which are required to understand the mechanisms that are operational in friction systems. In the case of iron, LEED, Auger and microcontact studies have established that hydrogen and light-saturated organic vapors do not establish interfaces which prevent iron from welding, whereas oxygen and some oxygen and sulfur compounds do reduce welding as well as the coefficient of friction. Interpretation of these data suggests a mechanism of sulfur interaction in lubricating systems.
The studies reported were conducted to gain a fundamental understanding of adhesion and dynamic friction on an atomic or microscopic level. Fundamental aspects of low energy electron diffraction (LEED), Auger emission spectroscopy (AES), and field ion microscopy (FIM) are discussed. Typical results of studies conducted are considered, giving attention to LEED-AES experiments, pin and disk experiments, and field ion microscope investigations.
The experimental apparatus used in the investigation consisted of an ultrahigh-vacuum chamber, a triple-grid, a microwave-excited resonance lamp, and an electron energy analyzer. The chemical nature of the chemisorbed species was studied, taking into account the energy distribution of photoemitted electrons, work function determinations, and low-energy electron diffraction patterns.
The adsorption and condensation of Cu up to several monolayers in thickness on tungsten 110 and 100 single-crystal surfaces are studied by combining low-energy electron diffraction, Auger electron spectroscopy, thermal desorption spectroscopy, work-function measurements, and quartz microbalance thickness measurements in one experimental system. The results show drastic differences in the evolution of the structure, work function, and desorption behavior between 110 and 100 surfaces. These differences are understandable in terms of the atomic roughness of the surfaces.
Exoelectron emission was observed from a clean, annealed Mg (0001) surface during oxygen and chlorine adsorption at pressures of 6.5x10 0.00001- N/sq m and lower. the studies were performed in an ultrahigh vacuum system. The crystals were cleaned by argon ion bombardment and annealed at 300 C. Auger electron spectroscopy was used to verify surface cleanliness, and low energy electron diffraction was used to verify that the surface was annealed. The emission was found to be oxygen arrival rate dependent. Two peaks were observed in the electron emission with exposure. Evidence is presented that the formation of the second peak corresponds to oxidation of the Mg surface. No emission was observed from clean aluminum during adsorption. Results verify that electron emission occurs from a strain free surface simply upon adsorption of oxygen. A qualitative explanation for the mechanisms of emission in terms of chemical effects is presented.