Experiments to measure material and mechanism damping at cryogenic temperatures
Explore the source record for details and available documents.
damping materials cryogenic↗
SEARCH · Search NASA
Results for “measurement of materials”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Material Properties Measurements for Selected Materials
Hugoniot equation of state measurements were made on Coconino sandstone, Vacaville basalt, Kaibab limestone, Mono Crater, pumice and Zelux (a polycarbonate resin) for pressures to 2 Mb. A single data point was obtained for fused quartz at 1.6 Mb. In addition to the hugoniot studies, the uniaxial compressive stress behavior of Vacaville basalt and Zelux was investigated at strain rates from about 10(exp -5)/sec to 10(exp 3)/second. The data presented include the stress - strain relations as a function of strain rate for these two materials.
Green, S. J.↗
A technique for measurement of material damping in metals
The paper outlines the theory, design, and application of an apparatus based on the single beam resonant dwell technique to determine the damping capacity of metallic materials by measuring the response of a structural element to excitation at a modal frequency. In this apparatus, a cantilever beam specimen of a test material is clamped to a bar which is connected at one end to an electromagnetic shaker and at the other to a heavy base. The thickness of the bar at the base end is reduced by two saw cuts to provide a pivot around which the remainder of the bar can rotate when excited by the shaker which is connected to the bar by a rod passing through a hole in the base. The response of the supporting system to shaker excitation is measured with an accelerometer mounted on the bar at the root of the specimen. Specimen response is measured optically with a low-power microscope with a reticle. Specimen loss factor is determined in terms of acceleration at the beam root, beam tip displacement, and the beam natural frequency.
Heine, J. C.↗
The measurement of total normal emittance of three nuclear reactor materials
Measurement of total normal emittance of nuclear reactor materials - carbon steel, boron steel, & borated graphite
EMISSION↗
Measuring the thermal conductivity of irradiated foam-type insulation materials.
Measurement of thermal conductivity of irradiated foam-type insulation materials
NUCLEAR RADIATION↗
Experimental measurements of material damping in free fall with tuneable excitation
An experimental method of measuring material damping of a specimen in free fall has been developed. An initially simply-supported test specimen was simultaneously excited and lofted into free fall with a spring-mass launcher. The launcher could be tuned to produce varying initial stress amplitude levels in the specimens. Damping information was obtained from the transient response of the specimens while in free fall in a vacuum. A dynamic model of the launch process was developed which indicates the range of frequency and initial specimen stress amplitude over which tests can be performed. To verify the facility, material damping was measured in 2024-T3 aluminum, and (+ or - 45)2s AS1/3501-6 graphite/epoxy. Free-free frequencies ranged from 20-357 Hz in aluminum, and from 18-171 Hz in the (+ or - 45)2s specimens. Damping values in aluminum were found to be close to theoretical values and independent of stress levels below 130 MPa (18.7 Ksi). Damping ratios in the (+ or - 45)2s graphite/epoxy specimens were found to be largely independent of stress levels below 43.8 MPa (6.35 Ksi) and only slightly dependent on frequency. A small dependence of the frequency of free vibration on specimen stress amplitude was also noted.
Crawley, E. F.↗
Testing of nonmagnetic materials
Measuring magnetic properties of nonmagnetic materials in low magnetic fields
MATERIALS SCIENCE↗
Measurement of material recession and shock standoff in plasma windtunnel using neural nets
Arcjets are plasma wind tunnels used to test the performance of heatshield materials for spacecraft atmospheric entry. These facilities present an extremely harsh flow environment with heat fluxes up to 10^9 W/m^2 for up to 30 minutes. The plasma is low-temperature (~1 eV) but high pressure (> 10 kPa) creating high-enthalpy supersonic flows similar to atmospheric entry conditions. Typically, material samples are measured before and after a test to characterize the total recession. However, this does not capture time-dependent effects such as material expansion and non-linear recession. This work will present new analysis of arcjet test videos which measure both the time-dependent 2D recession of the material samples and the shock standoff distance. New results showing non-linear material erosion rates will be highlighted. The material and shock edges are extracted from the videos by training and applying a convolutional neural network. Due to the consistent camera settings, the machine learning model achieves high accuracy (~99%) on new data with only a small number of training frames (~80). The new results will be discussed in the context of temperature dependent plasma-surface interaction.
Magnus A Haw↗
Measurement of Material Recession and Shock Standoff in Plasma Windtunnel using Neural Nets
Arcjets are plasma wind tunnels used to test the performance of heatshield materials for spacecraft atmospheric entry. These facilities present an extremely harsh flow environment with heat fluxes up to 109 W/m2 for up to 30 minutes. The plasma is low-temperature (∼1 eV) but high pressure (> 10 kPa) creating high-enthalpy supersonic flows similar to atmospheric entry conditions. Typically, material samples are measured before and after a test to characterize the total recession. However, this does not capture time-dependent effects such as material expansion and non-linear recession. This work will present new analysis of arcjet test videos which measure both the time-dependent 2D recession of the material samples and the shock standoff distance. The results show non-linear time-dependent effects are present for some conditions. The material and shock edges are extracted from the videos by training and applying a convolutional neural network. Due to the consistent camera settings, the machine learning model achieves high accuracy (± 2 px) relative to manually segmented images with only a small number of training frames (80).
Neural network↗
MEASURED EFFECTS OF THE VARIOUS COMBINATIONS OF NUCLEAR RADIATION, VACUUM, AND CRYOTEMPERATURES ON ENGINEERING MATERIALS
Measured effects of various combinations of nuclear radiation, vacuum, and cryotemperatures on component parts of nuclear-powered spacecraft
NUCLEAR RADIATION↗
Measurements of material properties for solar cells
Measurements on two candidate materials for space flight are reported. The observed optical transmittance of aluminum films vapor deposited on fused quartz showed anomalously high transmittance thru 400 A and 600 A and showed an effective skin depth of 110 A in the latter part of the 1000 A thickness. KAPTON films are shown by their optical transmission spectra to have an energy gap for electron excitation of approximately 2.5 eV, which value depends on the thickness as manufactured. The resistance of KAPTON film to ionizing radiation is described by their optical spectra and their electron spin resonance spectra.
Castle, J. G., Jr.↗
Spectroscopic Behavior of Composite, Black Thermal Paint, Solar Cell, and Multi-layered Insulation Materials in a GEO Simulated Environment
Materials currently populating Earth orbital regimes can be distinguished by comparing remote observational data to that of optical material measurements obtained in the laboratory. Experimentation for this research primarily involved the acquisition of spectroscopic measurements on materials of interest to the telescopic observational community for enhanced space situational awareness. Common spacecraft materials worthy of preeminent analysis for this investigation include a carbon-carbon (c-c) matrix composite, various black thermal paints, a GPS solar cell and three different cover glass components. These materials were subjected to a simulated geosynchronous Earth orbit (GEO) space environment with the intent of observing material optical property behavior over quantitative exposure time. The aforementioned materials have been measured in their pristine and GEO simulated exposed conditions. A reflectance spectrometer and a bi-directional reflectance distribution function (BRDF) optical system have been operated to perform material characterization, optical property analysis, and to further compare such data to telescopic observational data acquired on equal materials.
Reyes, Jacqueline A.↗
A study of acoustic impedance measurements of materials with air flow Final report
Acoustic impedance measurements of materials with air flow for reducing compressor noise of jet engines - graphs
Source record↗
Spectral and Total Normal Emittance of Reusable Surface Insulation Materials
Measurements of spectral and total normal emittance have been made on three types of reusable external insulation materials proposed for space shuttles. Emittances were measured in the spectral range 1 to 15 micrometer at temperatures of 800 K and 1100 K using a radiometric measurement technique. Results indicated that the total normal emittance of these materials was less than 0.8 between 800 K and 1300 K. The total normal emittance decreased with increasing temperature. The three ceramic coating candidate materials exhibited a similar spectral emittance distribution.
Kantsios, A. G.↗
Experimental measurement of material damping for space structures
A procedure for the measurement of material damping is described. The free decay of free-free beams, when lofted into free fall in vacuum, was recorded. Tests were performed on aluminum, graphite/epoxy, and graphite/magnesium metal matrix materials. Specimens with a fundamental free-free frequency below the elaxation frequency showed a higher level of damping and of stress dependence than predicted. For 0 sub 8 laminates, a material damping ratio of 0.00055 was found for fequencies varying from 45 Hz to 237 Hz. The damping was neither stress nor frequency dependent. For 90 sub 8 laminates, the damping ratio ranged from 0.0055 to 0.0066 as frequency ranged from 42 Hz to 143 Hz. Damping ratios for 90 sub 8 specimens were independent of stress. Experimentally measured damping ratios for metal matrix specimens with unidirectional graphite fibers, magnesium matrix, and either titanium or magnesium foil, ranged from .00039 to .00099, depending upon the matrix material, frequency, and possibly the stress range involved.
Crawley, E. F.↗
Goniometric and Polarized Imaging Spectroscopic Lab Measurements ofSpacecraft Materials
To better characterize the spectral response of common spacecraft materials, the following laboratory measurements are presented to support the Space Situational Awareness community in the analysis of remotely sensed observational data. Of interest is classifying material reflective properties using spectral bidirectional reflectance distribution function (BRDF) data and spatially resolved polarized imaging spectroscopy, allowing laboratory data to be applicable to ground-based optical telescope observations. The team acquired a typical CubeSat solar panel and a sample of multi-layer insulation commonly used on spacecraft for initial measurements. The data were collected at the Goniometer of the Rochester Institute of Technology (GRIT) laboratory with a field and laboratory goniometer housing two Analytical Spectral Device (ASD) spectrometers and a Headwall micro-Hyperspec E-Series imaging spectrometer with an adjustable linear polarizer. The goniometer provides spectral reflectance over a broad spectral range from 350-2500 nm at 1 nm spacing with 3 nm spectral resolution in the visible and near infrared and 8 nm in the shortwave infrared. The Headwall imager covers a spectral range from 400-1000 nm with 1.6 nm spectral resolution. We present the results from these initial measurements that show highly reflective regions at various locations in the angular domain for both materials. In addition, the solar cell spectra exhibited strong interference effects typically observed with thin films. Our team is pursuing a variety of typical solar cells to assess variations in product type. The spatially resolved polarization ratio maps show variability across the materials due to surface structure and varying material composition. Based on these results, we outline a plan for simulating spectral radiance light curves of the materials in various orbital configurations as they would be measured from ground- based telescopes for a clear observing sky during twilight. The paper will also present a plan for expanding ours of interest to determine if the results presented are unique to these samples and to categorize the spectral response for different material classes.
Chris H. Lee↗
Thermophysical Property Measurement and Materials Research in the NASA/MSFC Electrostatic Levitator
Containerless processing is an important tool for thermophysical property measurements and materials research. The freedom from a crucible allows processing of liquid materials in a metastable undercooled state, as well as allowing processing of high temperature and highly reactive melts. Electrostatic levitation (ESL) is a containerless method which provides a number of unique advantages, including the decoupling of positioning force from sample heating, the ability to operate in ultra-high vacuum or at moderate gas pressure (approximately 3 atm), and the ability to process non-conducting materials. ESL also has the potential to reduce internal flow velocities below those possible with electromagnetic, acoustic, or aero-acoustic techniques. The ESL facility at NASA's Marshall Space Flight Center (MSFC) is in use for thermophysical property measurements and materials research by a number of different internal and external investigators. The methods for obtaining access to the facility, as well as a summary of current capabilities and some future directions will be discussed. In electrostatic levitation, the acceleration of gravity (or residual acceleration in reduced gravity) is opposed by the action of an applied electric field on a charged sample. This positioning method is applicable to any material which can be electrically charged, whether solid or liquid, conducting, or insulating. Because the position of the sample is unstable, a 3-dimensional active control loop rapidly adjusts the applied field to maintain levitation and minimize motion of the sample. Heating lasers melt the sample, and may be adjusted to maintain specified thermal profiles. Microgravity allows electrostatic levitation to work even more effectively. With the need to cancel less than 1 milli-g, the applied field required is reduced from approximately 10 MV/m to approximately 10 kV/m. Alternatively, a microgravity ESL can position larger samples than is possible on the ground, or it can position samples which maintain their charge poorly. Microgravity also reduces the effects of buoyant convection and sedimentation. In the MSFC ESL, many different classes of experiments and measurements have been demonstrated in collaboration with many investigators. These capabilities include heat capacity measurement, phase diagram determination, and nucleation and growth experiments including nucleation rate, TTT curves, and phase selection. We have demonstrated the capability of triggering recalescence of an undercooled liquid sample without loss of levitation. Currently under development are techniques for measuring the surface tension, viscosity, and density of levitated samples, as well as other thermophysical properties. Expanded levitation capabilities including various gas environments for sample processing, sample rotation control and management of thermal gradients are under development for the MSFC ESL. Containerless processing allows research on materials which may not be processed any other way. Electrostatic levitation extends the range of containerless processing to include many materials and classes of materials which cannot be processed by conventional electromagnetic, acoustic, or aerodynamic levitation techniques.
Rogers, Jan↗
Thermophysical Property Measurement and Materials Research in the NASA/MSFC Electrostatic Levitator
Containerless processing is an important tool for thermophysical property measurements and materials research. The freedom from a crucible allows processing of liquid materials in a metastable undercooled state, as well as allowing processing of high temperature and highly reactive melts. Electrostatic levitation (ESL) is a containerless method which provides a number of unique advantages, including the decoupling of positioning force from sample heating, the ability to operate in ultra-high vacuum or at moderate gas pressure (approximately 3 atm), and the ability to process non-conducting materials. ESL also has the potential to reduce internal flow velocities below those possible with electromagnetic, acoustic, or aero-acoustic techniques. The ESL facility at NASA's Marshall Space Flight Center (MSFC) is in use for thermophysical property measurements and materials research by a number of different internal and external investigators. The methods for obtaining access to the facility, as well as a summary of current capabilities and some future directions will be discussed.
Rogers, J. R.↗