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NASA NTRS2011

Separation of Single-Walled Carbon Nanotubes with DEP-FFF

A process using a modified dielectrophoresis device separates single-walled carbon nanotubes (SWNTs) according to their polarizability in electric fields. This depends on the size and dielectric constant of individual nanotubes and easily separates metallic from semiconducting nanotubes. Separation by length has also been demonstrated. Partial separation (enrichment) according to bandgap (which is linked to polarizability) has also been shown and can be improved to full separation of individual types of semiconducting SWNTs with better control over operational parameters and the length of SWNT starting material. This process and device can be scaled affordably to generate useful amounts of semiconducting SWNTs for electronic device development and production. In this study, a flow injection dielectrophoresis technique was used with a modified dielectrophoresis device. The length, width, and height of the modified chamber were 28, 2.5, and 0.025 cm, respectively. On the bottom of the chamber, there are two arrays of 50-m-wide, 2-m-thick gold electrodes, which are connected to an AC voltage generator and are alternately arranged so that every electrode is adjacent to two electrodes of the opposite polar. There is an additional plate electrode on the top of the chamber that is negatively biased. During the experiment, a syringe pump constantly pumps in the mobile phase, 1-percent sodium dodecylbenzene sulfonate (SDBS) solution, into the chamber. The frequency and voltage are set to 1 MHz and 10 V peak-to-peak, respectively. About 150 micro-L of SWNTs in 1- percent SDBS decanted solution are injected to the mobile phase through a septum near the entrance of the chamber. The flow rate of the mobile phase is set to 0.02 cu cm/min. The injected SWNTs sample flows through the chamber before it is lead into a fluorescence flow-through cell and collected for further analysis. The flow-through cell has three windows, thus allowing the fluorometer to collect fluorescence spectrum and visible absorption spectrums simultaneously. Dielectrophoresis field-flow fractionation (DEP-FFF) generally depends on interaction of a sedimentation force and DEP force for particle separation, and SWNTs are neutrally buoyant in water. In this innovation, the third electrode was added to create a sedimentation force based on DC electrophoresis. This makes this particular device applicable to separations on any neutrally buoyant particles in solution and a more general process for a broad range of nanomaterials sorting and separations.

Schmidt, Howard K.↗

NASA NTRS1982

Computations and turbulent flow modeling in support of helicopter rotor technology

Efforts continue to investigate the applicability of the Deiwert's time dependent numerical airfoil calculation code to the simulation of two dimensional airfoil flows with large amounts of separation present. A modified logarithmic region mixing length term produced substantial differences in the calculated flow fields for the large separation of the M=0.4, high angle of attack cases. Reasons are given for interest in applying that model to previously investigated cases of the 64A010 airfoil section at Mach number 0.8 for angles of attack of 4 deg and 6.2 deg. The effects of these turbulence models at alterations and the time dependent behavior from impulsively started conditions are discussed.

Rose, W. C.↗

NASA NTRS1961

Vanguard Satellite Separation Mechanisms

Early in the Vanguard program it became apparent that a thoroughly reliable means of separating the satellite packages from the third-stage rocket would be required. A completely self -contained standard mechanism was developed with redundant firing circuits for use on both test vehicles and satellite-launching vehicles. A change in the experimental objectives of the test-vehicle payload units necessitated modification of some of the standard separation mechanisms. A strap, pull-pin, girth-ring separation device was developed which employed the basic actuation of the standard mechanisms. Evidence of residual burning of the third stage made it necessary to delay separation longer than the time designed into the long-delay separation device. The standard separation mechanism was modified and integrated with the satellite command receiver system so that a ground command after third-stage burnout would cause separation. Flight performance of the various separation mechanisms proved their reliability; they performed without failure in all Vanguard launchings.

Baumann, Robert C.↗

NASA NTRS1985

Flow and atomization in flashing injectors

Flashing injection involves expanding a fluid through an injector until a supersaturated state is reached, causing a portion of the fluid to flash to a vapor. This investigation considered the flow, atomization and spreading properties of flashing injectors with flowing liquids containing dissolved gases (Jet A/air) as well as superheated liquids (Freon-11). The use of a two-stage expansion process, separated by an expansion chamber, was found to be beneficial for good atomization properties of flashing injection - particularly for dissolved gas systems. Both locally homogeneous and separated flow models provided good predictions of injector flow properties. Conventional correlations for drop sizes from pressure and airblast injectors were successfully modified, using the separated flow model to prescribe injector exit conditions, and to correlate drop size measurements. Additional experimental results are provided for spray angles of sprays from flashing injectors.

Solomon, A. S. P.↗

NASA NTRS1982

Investigation of spray characteristics for flashing injection of fuels containing dissolved air and superheated fuels

The flow, atomization and spreading of flashing injector flowing liquids containing dissolved gases (jet/air) as well as superheated liquids (Freon II) were considered. The use of a two stage expansion process separated by an expansion chamber, ws found to be beneficial for flashing injection particularly for dissolved gas systems. Both locally homogeneous and separated flow models provided good predictions of injector flow properties. Conventional correlations for drop sizes from pressure atomized and airblast injectors were successfully modified, using the separated flow model to prescribe injector exit conditions, to correlate drop size measurements. Additional experimental results are provided for spray angle and combustion properties of sprays from flashing injectors.

Solomon, A. S. P.↗

NASA NTRS1982

Atomization and combustion properties of flashing injectors

Flashing injection involves expanding a fluid through an injector until a supersaturated state is reached, causing a portion of the fluid to flash to a vapor. This investigation considered the flow, atomization and spreading properties of flashing injectors flowing liquids containing dissolved gases (Jet A/air) as well as superheated liquids (Freon 11). The use of a two stage expansion process, separated by an expansion chamber, was found to be beneficial for good atomization properties of flashing injection - particularly for dissolved gas systems. Both locally homogeneous and separated flow models provided good predictions of injector flow properties. Conventional correlations for drop sizes from pressure atomized and airblast injectors were successfully modified, using the separated flow model to prescribe injector exit conditions, to correlate drop size measurements. Additional experimental results are provided for spray angle and combustion properties of sprays from flashing injectors.

Solomon, A. S. P.↗

NASA NTRS1984

Analysis of airfoil transitional separation bubbles

A previously developed local inviscid-viscous interaction technique for the analysis of airfoil transitional separation bubbles, ALESEP (Airfoil Leading Edge Separation) has been modified to utilize a more accurate windward finite difference procedure in the reversed flow region, and a natural transition/turbulence model has been incorporated for the prediction of transition within the separation bubble. Numerous calculations and experimental comparisons are presented to demonstrate the effects of the windward differencing scheme and the natural transition/turbulence model. Grid sensitivity and convergence capabilities of this inviscid-viscous interaction technique are briefly addressed. A major contribution of this report is that with the use of windward differencing, a second, counter-rotating eddy has been found to exist in the wall layer of the primary separation bubble.

Davis, R. L.↗

NASA NTRS1984

Analysis of airfoil transitional separation bubbles

A previously developed local inviscid-viscous interaction technique for the analysis of airfoil transitional separation bubbles, ALESEP (Airfoil Leading Edge Separation), has been modified to utilize a more accurate windward finite difference procedure in the reversed flow region, and a natural transition turbulence model has been incorporated for the prediction of transition within the separation bubble. Numerous calculations and experimental comparisons are presented to demonstrate the effects of the windward differencing scheme and the natural transition turbulence model. Grid sensitivity and convergence capabilities of this inviscid-viscous interaction technique are briefly addressed. A major conclusion of this paper is that a second, counter-rotating eddy has been found to exist in the wall layer of the primary separation bubble with the use of windward differencing.

Davis, R. L.↗

NASA NTRS2004

Masked Proportional Routing

Masked proportional routing is an improved procedure for choosing links between adjacent nodes of a network for the purpose of transporting an entity from a source node ("A") to a destination node ("B"). The entity could be, for example, a physical object to be shipped, in which case the nodes would represent waypoints and the links would represent roads or other paths between waypoints. For another example, the entity could be a message or packet of data to be transmitted from A to B, in which case the nodes could be computer-controlled switching stations and the links could be communication channels between the stations. In yet another example, an entity could represent a workpiece while links and nodes could represent, respectively, manufacturing processes and stages in the progress of the workpiece towards a finished product. More generally, the nodes could represent states of an entity and the links could represent allowed transitions of the entity. The purpose of masked proportional routing and of related prior routing procedures is to schedule transitions of entities from their initial states ("A") to their final states ("B") in such a manner as to minimize a cost or to attain some other measure of optimality or efficiency. Masked proportional routing follows a distributed (in the sense of decentralized) approach to probabilistically or deterministically choosing the links. It was developed to satisfy a need for a routing procedure that 1. Does not always choose the same link(s), even for two instances characterized by identical estimated values of associated cost functions; 2. Enables a graceful transition from one set of links to another set of links as the circumstances of operation of the network change over time; 3. Is preferably amenable to separate optimization of different portions of the network; 4. Is preferably usable in a network in which some of the routing decisions are made by one or more other procedure(s); 5. Preferably does not cause an entity to visit the same node twice; and 6. Preferably can be modified so that separate entities moving from A to B do not arrive out of order.

Wolpert, David↗

NASA NTRS2004

Unsteady Aerodynamic Response of a Linear Cascade of Airfoils in Separated Flow

The overall objective of this research program was to investigate methods to modify the leading edge separation region, which could lead to an improvement in aeroelastic stability of advanced airfoil designs. The airfoil section used is representative of current low aspect ratio fan blade tip sections. The experimental potion of this study investigated separated zone boundary layer from removal through suction slots. Suction applied to a cavity in the vicinity of the separation onset point was found to be the most effective location. The computational study looked into the influence of front camber on flutter stability. To assess the influence of the change in airfoil shape on stability the work-per-cycle was evaluated for torsion mode oscillations. It was shown that the front camberline shape can be an important factor for stabilizing the predicted work-per-cycle and reducing the predicted extent of the separation zone. In addition, data analysis procedures are discussed for reducing data acquired in experiments that involve periodic unsteady data. This work was conducted in support of experiments being conducted in the NASA Glenn Research Center Transonic Flutter Cascade. The spectral block averaging method is presented. This method is shown to be able to account for variations in airfoil oscillation frequency that can occur in experiments that force oscillate the airfoils to simulate flutter.

Capece, Vincent R.↗

NASA NTRS1972

An economical net solar flux radiometer.

The theory and design of an economical solar flux radiometer readily adaptable to the conventional radiosonde system are presented in response to the need cited by the Atmospheric Radiation Working Group (1971) for the development of an inexpensive light-weight short-wave radiometer sonde. Prototype instrument tests and current modifications are discussed. It is shown that the basic instrument can be easily modified to measure separately the upward and downward directed flux components, in addition to the net flux.

Darkow, G. L.↗

NASA NTRS1978

Upgraded viscous flow analysis of multielement airfoils

A description of an improved version of the NASA/Lockheed multielement airfoil analysis computer program is presented. The improvements include several major modifications of the aerodynamic model as well as substantial changes of the computer code. The modifications of the aerodynamic model comprise the representation of the boundary layer and wake displacement effects with an equivalent source distribution, the prediction of wake parameters with Green's lag-entrainment method, the calculation of turbulent boundary layer separation with the method of Nash and Hicks, the estimation of the onset of confluent boundary layer separation with a modified form of Goradia's method, and the prediction of profile drag with the formula of Squire and Young. The paper further describes the modifications of the computer program for which the structured approach to computer software development was employed. Important aspects of the structured program development such as the functional decomposition of the aerodynamic theory and its numerical implementation, the analysis of the data flow within the code, and the application of a pseudo code are discussed.

Brune, G. W.↗

NASA NTRS1979

Upgraded viscous flow analysis of multi-element airfoils

A description of an improved version of the NASA/Lockheed multi-element airfoil analysis computer program is presented. The improvements include several major modifications of the aerodynamic model as well as substantial changes of the computer code. The modifications of the aerodynamic model comprise the representation of the boundary layer and wake displacement effects with an equivalent source distribution, the prediction of wake parameters with Green's lag-entrainment method, the calculation of turbulent boundary layer separation with the method of Nash and Hicks, the estimation of the onset of confluent boundary layer separation with a modified form of Goradia's method, and the prediction of profile drag with the formula of Squire and Young. The modifications of the computer program for which the structured approach to computer software development was employed are also described. Important aspects of the structured program development such as the functional decomposition of the aerodynamic theory and its numerical implementation, the analysis of the data flow within the code, and the application of a pseudo code are discussed.

Brune, G. W.↗

NASA NTRS1979

Length and bursting of separation bubbles: A physical interpretation

A physical interpretation of the observed form of the pressure distribution beneath a two-dimensional separation bubble which modified the external inviscid pressure distribution only locally is given in terms of boundary layer concepts. A simple method for estimating along a mean streamline entrained into the underside of a growing shear layer through the transition region is discussed, and predictions of bubble bursting conditions and a lower bound on the bubble length are compared with experiment.

Russell, J. M.↗

NASA NTRS1988

Algebraic turbulence models for the computation of two-dimensional high speed flows using unstructured grids

The incorporation of algebraic turbulence models in a solver for the 2-D compressible Navier-Stokes equations using triangular grids is described. A practical way to use the Cebeci Smith model, and to modify it in separated regions is proposed. The ability of the model to predict high speed, perfect gas boundary layers is investigated from a numerical point of view.

Rostand, Philippe↗

NASA NTRS1989

Algebraic turbulence models for the computation of two-dimensional high-speed flows using unstructured grids

The incorporation of algebraic turbulence models in a solver for the 2-D compressible Navier-Stokes equations using triangular grids is described. A practial way to use the Cebeci Smith model, and to modify it in separated regions is proposed. The ability of the model to predict high speed, perfect gas boundary layers is investigated from a numerical point of view.

Rostand, Philippe↗

NASA NTRS2002

Report on Project to Characterize Multi-Junction Solar Cells in the Stratosphere using Low-Cost Balloon and Communication Technologies

Balloon, control and communication technologies are under development in our laboratory for testing multi-junction solar cells in the stratosphere to achieve near AM0 conditions. One flight, Suntracker I, has been carried out reported earlier. We report on our efforts in preparation for a second flight, Suntracker II, that was aborted due to hardware problems. The package for Suntracker I system has been modified to include separate electronics and battery packs for the 70 centimeter and 2 meter systems. The collimator control system and motor gearboxes have been redesigned to address problems with the virtual stops and backlash. Surface mount technology on a printed circuit board was used in place of the through-hole prototype circuit in efforts to reduce weight and size, and improve reliability. A mobile base station has been constructed that includes a 35' tower with a two axis rotator and multi-element yagi antennas. Modifications in Suntracker I and the factors that lead to aborting Suntracker II are discussed.

Mirza, Ali↗

NASA NTRS2004

Preparation of Proton Exchange Membranes and Lithium Batteries from Melamine-containing Ormosils

Our laboratory has recently reported a series of rodcoil polymers for lithium batteries that display dimensionally stable films with good ionic conductivity. The rod segments consist of rigid linear and branched polyimides and the coil segments are polyethylene oxides (PEO). It has been proposed that good mechanical and transport properties are due to phase separation between the rod and coil segments. It was also observed that increased branching and molecular weight lead to increased conductivity. The following study was undertaken to assess the effects of phase separation in polyalkylene oxides connected by melamine linkages. Melamine was chosen as the linking unit because it provides a branching site, cation binding sites to help ionic transport between polymer chains, and the opportunity for self assembly through hydrogen bonding. Polymers were made by the reaction of cyanuric chloride with a series of amine-terminated alkylene oxides. A linear polymer was first made, followed by reaction of the third site on cyanuric chloride with varying ratios of monofunctional Jeffamine and (3-aminopropyl)triethoxysilane. The lithium trifluoromethane sulfonamide-doped polymers are then crosslinked through a sol-gel process to form free-standing films. Initial results have shown mechanically strong films with lithium conductivities on the order of 2 x 10(exp -5) S/cm at ambient temperature. In a separate study, organically modified silanes (Ormosils) that contain sulfonic acid derivatized melamines have been incorporated into proton exchange membranes. The membranes are made by reaction of the primary amine groups of various ratios of melamine derivative and difunctional Jeffamine (MW = 2000) with the epoxide group of (3-Glycidyloxypropyl)trimethoxysilane. The films were then cross-linked through a sol-gel process. Resulting sulfuric acid doped films are strong, flexible, and have proton conductivities on the order of 2 x l0(exp -2) S/cm (120 C, 25% relative humidity). Our best results have been observed when films contain 60% PEO and 40% sulfonated melamine.

Tigelaar, Dean M.↗