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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 37 records · Page 2
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Self-calibration strategies for reducing systematic slope measurement errors of autocollimators in deflectometric profilometry

Deflectometric profilometers are used to precisely measure the form of beam shaping optics of synchrotrons and X-ray free-electron lasers. They often utilize autocollimators which measure slope by evaluating the displacement of a reticle image on a detector. Based on our privileged access to the raw image data of an autocollimator, novel strategies to reduce the systematic measurement errors by using a set of overlapping images of the reticle obtained at different positions on the detector are discussed. It is demonstrated that imaging properties such as, for example, geometrical distortions and vignetting, can be extracted from this redundant set of images without recourse to external calibration facilities. This approach is based on the fact that the properties of the reticle itself do not change – all changes in the reticle image are due to the imaging process. Firstly, by combining interpolation and correlation, it is possible to determine the shift of a reticle image relative to a reference image with minimal error propagation. Secondly, the intensity of the reticle image is analysed as a function of its position on the CCD and a vignetting correction is calculated. Thirdly, the size of the reticle image is analysed as a function of its position and an imaging distortion correction is derived. It is demonstrated that, for different measurement ranges and aperture diameters of the autocollimator, reductions in the systematic errors of up to a factor of four to five can be achieved without recourse to external measurements.

47 OTHER INSTRUMENTATION↗
NASA NTRS1998

The Radio-to-X-Ray Spectrum of GRB 970508 on 1997 May 21.0 UT

We have reconstructed the spectrum of the afterglow of GRB 970508 on 1997 May 21.0 UT (12.1 days after the gamma-ray burst burst) on the basis of observations spanning, the X-ray-to-radio range. The low-frequency power-law index of the spectrum, alpha = 0.44 +/- 0.07 (F, proportional to nu(sup alpha)) is in agreement with the expected value alpha = 1/3 for optically thin synchrotron radiation. The 1.4 emission is self-absorbed. We infer constraints on the break frequencies nu(sub c) and nu(sub m) on 1997 May 21.0 UT from a spectral transition from F, approximately nu(sup -0.6) to F, approximately nu(sup -1.1) in the optical passband around 1.4 days. A model of an adiabatically expanding blast wave emitting synchrotrons radiation, in which a significant fraction of the electrons cool rapidly, provides a successful and consistent description of the afterglow observations over nine decades in frequency, ranging in time from trigger until several months later.

Galama, T. J.↗
NASA NTRS1998

The Radio-to-X-Ray Spectrum of GRB 970508 on 1997 May 21.0 UT

We have reconstructed the spectrum of the afterglow of GRB 970508 on 1997 May 21.0 UT (12.1 days after the gamma-ray burst) on the basis of observations spanning the X-ray-to-radio range. The low-frequency power-law index of the spectrum, alpha = 0.44 +/- 0.07 (F(sub nu) proportional to nu(exp alpha)), is in agreement with the expected value alpha = 1/3 for optically thin synchrotron radiation. The 1.4 GHz emission is self-absorbed. We infer constraints on the break frequencies nu(sub c) and nu(sub m) on 1997 May 21.0 UT from a spectral transition from F(sub nu) approx. nu(exp -0.6) to F(sub nu) approx. nu(exp -1.1) in the optical passband around 1.4 days. A model of an adiabatically expanding, blast wave emitting synchrotron radiation, in which a significant fraction of the electrons cool rapidly, provides a successful and consistent description of the afterglow observations over nine decades in frequency, ranging in time from trigger until several months later.

Galama, T. J.↗
NASA NTRS1977

Structure of radio sources with remarkably flat spectra - PKS 0735+178

Three incoherent synchrotron models are used to account for the very flat radio spectrum of the BL Lac object PKS 0735+178. The first interpretation is that the spectrum results from optically-thin synchrotron emission from relativistic electrons with a particular energy distribution. The second posits a single nonuniform, self-absorbed source generated by a wind flowing from a central object. The third suggests that sources with flat spectra are caused by the presence of multiple (three or more) discrete uniform components, and that the magnetic field and relativistic electron distribution for each source is correlated with the size of the individual components. It is proposed that the last model is the most tenable explanation of the phenomenon, and multi-frequency VLBI observations are suggested for the evaluation of the detailed structure of compact radio sources.

Marscher, A. P.↗
NASA NTRS1998

The Parsec-Scale Magnetic Field Properties of Low-Optical Polarization Blazars

Past variability studies of flat-spectrum, compact extra-galactic radio sources have suggested that low- and high-optically polarized quasars (LPQ/HPQ) are the same type of object, differing only in the angle their relativistic jets make to the line of sight. This view has been challenged, however, by recent millimeter-wave polarization observations which indicate intrinsic differences in the inner magnetic field properties of the two classes. The inner jets of LPQs tend to have lower fractional polarizations than HPQs, and inferred magnetic field directions that are mostly parallel to the jet. The magnetic fields of HPQs, on the other hand, lie mainly in a transverse direction. The latter configuration is a prediction of the standard shock-in-jet model, in which a portion of a jet undergoes a strong transverse compression, thereby enhancing the perpendicular components of an originally tangled magnetic field. The main goal of this study is to establish a connection between the optical polarization and magnetic field properties of the inner jets of blazars. The magnetic field orientations of several HPQs have been shown to be stable over many years, which may be due to standing shock(s) located close to the base of the jet. Since these shocks are able to produce large amounts of optically polarized synchrotron radiation, their presence may very well determine whether an object is classified as an HPQ or LPQ. We have imaged the parsec-scale jet regions and magnetic fields of 11 LPQs with the Very Long Baseline Array (VLBA) at 43 and 22 GHz, and have obtained near- simultaneous optical polarization data for the sample. We discuss correlations between the optical and radio polarization data, and compare the LPQ properties to those of a sample of HPQs presently being monitored with the VLBA and JCMT at mm and sub-mm wavelengths, respectively. This research was performed in part at the Jet Propulsion Laboratory, California Institute of Technology, under contract to NASA.

Lister, Matthew L.↗
DOE OSTI2026

Sagittal collimating diaboloid: a new grazing-incidence mirror surface for higher-throughput resonant inelastic X-ray scattering spectrometers

A major challenge in soft X-ray spectroscopy is the efficient collection of the emitted X-rays by grazing-incidence mirrors. In this energy range, grazing-incidence mirrors are widely used as optics for the collection of light. The small angle of incidence necessarily limits the collection solid angle of soft X-ray spectrometers. We present a new mirror surface, a sagittal collimating diaboloid, that can both collect and focus light from a point source in an aberration-free manner. The usefulness of this optic in increasing throughput is demonstrated with a realistic example design of a moderate-sized (3 m) medium-resolution resonant inelastic X-ray scattering spectrometer.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Assembly of Building Blocks by Double-End-Anchored Polymers in the Dilute Regime Mediated by Hydrophobic Interactions at Controlled Distances

Hierarchical assembly of building blocks via competing, orthogonal interactions is a hallmark of many of nature’s composite materials that do not require highly specific ligand-receptor interactions. To mimic this assembly mechanism requires the development of building blocks capable of tunable interactions. In the present work, we explored the interplay between repulsive (steric and electrostatic) and attractive hydrophobic forces. The designed building blocks allow hydrophobic forces to effectively act at controlled, large distances, to create and tune the assembly of membrane-based building blocks under dilute conditions and affect their interactions with cellular membranes via physical cross-bridges. Specifically, we employed double-end-anchored poly(ethylene glycol)s (DEA-PEGs)—hydrophilic PEG tethers with hydrophobic tails on both ends. Using differential-interference-contrast optical microscopy, synchrotron small angle X-ray scattering (SAXS), and cryogenic electron microscopy, we investigated the ability of DEA-PEGs to mediate assembly in the dilute regime on multiple length scales and on practical time scales. The PEG length, anchor hydrophobicity, and molar fraction of DEA-PEG molecules within a membrane strongly affect the assembly properties. Additional tuning of the intermembrane interactions can be achieved by adding repulsive interactions via PEG-lipids (steric) or cationic lipids to the DEA-PEG-mediated attractions. Further, while the optical and electron microscope imaging methods provided qualitative evidence of the ability of DEA-PEGs to assemble liposomes, the SAXS measurements and quantitative line-shape analysis in dilute preparations demonstrated that the ensemble average of loosely organized liposomal assemblies maintains DEA-PEG concentration-dependent tethering on defined nanometer length scales. For cationic liposome–DNA nanoparticles (CL–DNA NPs), aggregation induced by DEA-PEGs decreased internalization of NPs by cells, but tuning the DEA-PEG-induced attractions by adding repulsive steric interactions via PEG-lipids limited aggregation and increased NP uptake. However, confocal microscopy imaging together with colocalization studies with Rab11 and LysoTracker as markers of intracellular pathways showed that modifying CL–DNA NPs with DEA-PEGs alters their interactions with the plasma and endosomal membranes.

- x-ray scattering↗
NASA NTRS1998

A Viewing Angle-Kinetic Luminosity Scheme for BL Lacertae Objects

We propose a unified classification for BL Lacertae objects (BLs), focusing on the synchrotron peak frequency of the spectral energy distribution. The unification scheme is based on the angle theta that describes the orientation of the relativistic jet and on the electron kinetic luminosity Lamba(sub kin) of the jet. We assume that Lamba(sub kin) scales with the size of the jet (r) in a self-similar fashion (Lamba(sub kin) is proportional to r(exp 2)), as supported by observational data. The jets are self-similar in geometry and have the same pressure and median magnetic field at the inlet, independent of size. The self-similarity is broken for the highest energy electrons, which radiate mainly at high frequencies, since for large sources they suffer more severe radiative energy losses over a given fraction of the jet length. We calculate the optically thin synchrotron spectrum using an accelerating inner jet model based on simple relativistic gas dynamics and show that it can fit the observed infrared-to-X-ray spectrum of PKS 2155-304. We couple the accelerating jet model to the unification scheme and compare the results to complete samples of BLs. The negative apparent evolution of X-ray-selected BLs is explained as a result of positive evolution of the jet electron kinetic luminosity Lamba(sub kin). We review observational arguments in favor of the existence of scaled-down accretion disks and broad emission-line regions in BLs. The proposed unification scheme can explain the lack of observed broad emission lines in X-ray-selected BLs as well as the existence of those lines preferentially in luminous radio-selected BLs. Finally, we review observational arguments that suggest the extension of this unification scheme to all blazars.

Georganopoulos, Markos↗
DOE OSTI2020

Seeing is believing: visualization of antiferromagnetic domains

Abstract Understanding and utilizing novel antiferromagnetic (AFM) materials has been recently one of the central issues in condensed matter physics, as well as in materials science and engineering. The relevant contemporary topics include multiferroicity, topological magnetism and AFM spintronics. The ability to image magnetic domains in AFM materials is of key importance for the success of these exciting fields. While imaging techniques of magnetic domains on the surfaces of ferro-(ferri)magnetic materials with, for example, magneto-optical Kerr microscopy and magnetic force microscopy have been available for a number of decades, AFM domain imaging is a relatively new development. We review various experimental techniques utilizing scanning, optical, and synchrotron X-ray probes to visualize AFM domains and domain walls, and to unveil their physical properties. We also discuss the existing challenges and opportunities in these techniques, especially with further increase of spatial and temporal resolution.

36 MATERIALS SCIENCE↗
DOE OSTI2021

High-energy emission from a magnetar giant flare in the Sculptor galaxy

Magnetars are the most highly magnetized neutron stars in the cosmos (with magnetic field 10 13 –10 15 G). Giant flares from magnetars are rare, short-duration (about 0.1 s) bursts of hard X-rays and soft γ rays. Owing to the limited sensitivity and energy coverage of previous telescopes, no magnetar giant flare has been detected at gigaelectronvolt (GeV) energies. Here, we report the discovery of GeV emission from a magnetar giant flare on 15 April 2020 (refs. 3,4 and A. J. Castro-Tirado et al., manuscript in preparation). The Large Area Telescope (LAT) on board the Fermi Gamma-ray Space Telescope detected GeV γ rays from 19 s until 284 s after the initial detection of a signal in the megaelectronvolt (MeV) band. Our analysis shows that these γ rays are spatially associated with the nearby (3.5 megaparsecs) Sculptor galaxy and are unlikely to originate from a cosmological γ-ray burst. Thus, we infer that the γ rays originated with the magnetar giant flare in Sculptor. Furthermore, we suggest that the GeV signal is generated by an ultra-relativistic outflow that first radiates the prompt MeV-band photons, and then deposits its energy far from the stellar magnetosphere. After a propagation delay, the outflow interacts with environmental gas and produces shock waves that accelerate electrons to very high energies; these electrons then emit GeV γ rays as optically thin synchrotron radiation. This observation implies that a relativistic outflow is associated with the magnetar giant flare, and suggests the possibility that magnetars can power some short γ-ray bursts.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

The development and use of metal-based probes for X-ray fluorescence microscopy

Abstract X-ray fluorescence microscopy (XFM) has become a widely used technique for imaging the concentration and distribution of metal ions in cells and tissues. Recent advances in synchrotron sources, optics, and detectors have improved the spatial resolution of the technique to <10 nm with attogram detection sensitivity. However, to make XFM most beneficial for bioimaging—especially at the nanoscale—the metal ion distribution must be visualized within the subcellular context of the cell. Over the years, a number of approaches have been taken to develop X-ray-sensitive tags that permit the visualization of specific organelles or proteins using XFM. In this review, we examine the types of X-ray fluorophore used, including nanomaterials and metal ions, and the approaches used to incorporate the metal into their target binding site via antibodies, genetically encoded metal-binding peptides, affinity labeling, or cell-specific peptides. We evaluate their advantages and disadvantages, review the scientific findings, and discuss the needs for future development.

36 MATERIALS SCIENCE↗
DOE OSTI2025

AutoFocus: AI/ML-driven real-time wavefront diagnostics to autonomously align and optimize X-ray optics

We present an integrated system that combines advanced wavefront diagnostics with artificial intelligence (AI) to automate and optimize X-ray optics at synchrotron beamlines. This system couples real-time wavefront sensing with AI-driven control algorithms to achieve precise beam alignment, stabilization, and performance optimization. A key feature is the use of multi-fidelity transfer learning, which enables knowledge gained from both real-world beamline optimizations and ultra-realistic digital twin simulations to be effectively applied to in situ optimization. By leveraging multi-objective bayesian optimization, the system continuously refines its performance, reducing optimization time and minimizing the need for manual adjustments. Designed for seamless deployment, it operates with existing beamline hardware and provides an intuitive graphical interface. Initial deployments at the advanced photon source beamlines have demonstrated its ability to enhance beam stability, improve reproducibility, and significantly streamline alignment procedures. This AI-enhanced control framework represents a significant step toward fully autonomous beamline operation in next-generation synchrotron facilities.

Rebuffi, Luca [Argonne National Laboratory (ANL), ↗
NASA NTRS1977

Cygnus A at 99 GHz: Observations of the three principal components and interpretation of the central source

The three principal emission components of Cygnus A were observed at 99 GHz, the highest frequency at which radio measurements of this source have been accomplished. The observations show no definite indication of a high-frequency cutoff in the spectrum of the compact central component, which perhaps may be attributed to an optically thin synchrotron source that peaks at a frequency of several hundred GHz.

Hobbs, R. W.↗
NASA NTRS1978

Cygnus A at 99 GHz - Observations of the three principal components and interpretation of the central source

The three principal emission components of Cygnus A have been observed at 99 GHz, the highest frequency at which radio measurements of this source have been accomplished. The observations show no definite indication of a high-frequency cutoff in the spectrum of the compact central component, which perhaps may be attributed to an optically thin synchrotron source that peaks at a frequency of several hundred GHz.

Hobbs, R. W.↗
NASA NTRS1983

Extragalactic 1 millimeter sources - Simultaneous observations at centimeter, millimeter, and visual wavelengths

Observations simultaneously made at visual (B, V, and R) wavelengths, at 1, 1.4, and 3.4 mm and at 1.3, 2, 6, and 20 cm of 9 QSOs and BL Lac objects are reported. The range of the millimeter-visual spectral index alpha sub mv was only 0.65-0.82, typical of optically thin synchrotron emission. This may indicate that the electrons radiating synchrotron emission in this portion of the spectrum are not subjected to large radiation losses, and therefore relativistic bulk motion with Doppler factors of about 10 are required. The visual spectral index is much more broadly distributed and typically larger than alpha sub mv. The spectral energy distributions have not changed much in the last two to five years except for 2251+15 and perhaps 0235+164. Only 1749+09 shows a sharp spectral break shortward of 1 mm. Sixteen other sources were observed at 1 mm, of which seven were detected.

Landau, R.↗
NASA NTRS1983

Millimeter and submillimeter observations of 3C 273

The first detection of 3C 273 (1226 + 023) at wavelengths of 107, 240, and 400 microns together with contemporary measurements at 800 microns, 1.1, 1.9, 3.3, and 8.9 mm, is reported. These observations show that the continuum spectrum of 3C 273 can be extrapolated smoothly from the submillimeter to the infrared with a constant spectral index. There is no evidence of thermal emission from dust. It is shown that the spectrum is consistent with optically thin synchrotron emission from a relativistic beam at a small angle to the line of sight.

Glaccum, W.↗
NASA NTRS1984

X-ray spectra and time variability of active galactic nuclei

X ray measurements taken with the HEAO-1 and -2 satellites are examined for clues to the source of emissions from active galactic nuclei (AGN). The data covered the energy range 2-100 keV and 0.5-4.5 keV and encompassed quasars, BL Lac objects, Seyfert I galaxies and broadline radio galaxies. The broadline spectra were best fit with a power law with a slope of about 0.68. The continua displayed roughly equivalent energy at all wavelengths except for radio bands. Spectral variability was detected in the BL Lac objects, which may emit optical, UV and soft X ray radiation from optically thin synchrotron emission with a hard X ray tail from inverse Compton scattering. No strong variability was evidenced with other AGN, suggesting that the emitting regions are below the Eddington luminosity and thus exhibit stable flow characteristics.

Mushotzky, R. F.↗
NASA NTRS1991

Steep radio spectra in high-redshift radio galaxies

The generic spectrum of an optically thin synchrotron source steepens by 0.5 in spectral index from low frequencies to high whenever the source lifetime is greater than the energy-loss timescale for at least some of the radiating electrons. Three effects tend to decrease the frequency nu(b) of this spectral bend as the source redshift increases: (1) for fixed bend frequency nu* in the rest frame, nu(b) = nu*/(1 + z); (2) losses due to inverse Compton scattering the microwave background rise with redshift as (1 + z) exp 4, so that, for fixed residence time in the radiating region, the energy of the lowest energy electron that can cool falls rapidly with increasing redshift; and (3) if the magnetic field is proportional to the equipartition field and the emitting volume is fixed or slowly varying, flux-limited samples induce a selection effect favoring low nu* at high z because higher redshift sources require higher emissivity to be included in the sample, and hence have stronger implied fields and more rapid synchrotron losses. A combination of these effects may explain the trend observed in the 3CR sample for higher redshift radio galaxies to have steeper spectra, and the successful use of ultrasteep spectrum surveys to locate high-redshift galaxies.

Krolik, Julian H.↗