Trace activation analysis of element groups with computer reduction of Ge
Stony meteorite trace elements groups neutron activation analysis with computer reduction of Ge/Li spectra
Case, D. R.↗
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Analysis of trace halocarbon contaminants in ultra high purity helium
This study describes the analysis of ultra high purity helium. Purification studies were conducted and containment removal was effected by the utilization of solid adsorbent purge-trap systems at cryogenic temperatures. Volatile organic compounds in ultra high purity helium were adsorbed on a solid adsorbent-cryogenic trap, and thermally desorbed trace halocarbon and other contaminants were analyzed by combined gas chromatography-mass spectrometry.
Fewell, Larry L.↗
Analysis of memory use for improved design and compile-time allocation of local memory
Trace analysis techniques are used to study memory referencing behavior for the purpose of designing local memories and determining how to allocate them for data and instructions. In an attempt to assess the inherent behavior of the source code, the trace analysis system described here reduced the effects of the compiler and host architecture on the trace by using a technical called flattening. The variables in the trace, their associated single-assignment values, and references are histogrammed on the basis of various parameters describing memory referencing behavior. Bounds are developed specifying the amount of memory space required to store all live values in a particular histogram class. The reduction achieved in main memory traffic by allocating local memory is specified for each class.
Mcniven, Geoffrey D.↗
Ray tracing optical analysis of offset solar collector for space station solar dynamic system
OFFSET, a detailed ray tracing computer code, was developed at NASA Lewis Research Center to model the offset solar collector for the Space Station solar dynamic electric power system. This model traces rays from 50 points on the face of the Sun to 10 points on each of the 456 collector facets. The triangular facets are modeled with spherical, parabolic, or toroidal reflective surface contour and surface slope errors. The rays are then traced through the receiver aperture to the walls of the receiver. Images of the collector and of the Sun within the receiver produced by this code provide insight into the collector receiver interface. Flux distribution on the receiver walls, plotted by this code, is improved by a combination of changes to aperture location and receiver tilt angle. Power loss by spillage at the receiver aperture is computed and is considerably reduced by using toroidal facets.
Jefferies, Kent S.↗
Ray tracing optical analysis of offset solar collector for Space Station solar dynamic system
OFFSET, a detailed ray tracing computer code, was developed at NASA Lewis Research Center to model the offset solar collector for the Space Station solar dynamic electric power system. This model traces rays from 50 points on the face of the sun to 10 points on each of the 456 collector facets. The triangular facets are modeled with spherical, parabolic, or toroidal reflective surface contour and surface slope errors. The rays are then traced through the receiver aperture to the walls of the receiver. Images of the collector and of the sun within the receiver produced by this code provide insight into the collector receiver interface. Flux distribution on the receiver walls, plotted by this code, is improved by a combination of changes to aperture location and receiver tilt angle. Power loss by spillage at the receiver aperture is computed and is considerably reduced by using toroidal facets.
Jefferies, Kent S.↗
In Situ Trace Element Analysis of an Allende Type B1 CAI: EK-459-5-1
Variations in refractory major and trace element composition of calcium, aluminum-rich inclusions (CAIs) provide constraints on physical and chemical conditions and processes in the earliest stages of the Solar System. Previous work indicates that CAIs have experienced complex histories involving, in many cases, multiple episodes of condensation, evaporation, and partial melting. We have analyzed major and trace element abundances in two core to rim transects of the melilite mantle as well as interior major phases of a Type B1 CAI (EK-459-5-1) from Allende by electron probe micro-analyzer (EPMA) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) to investigate the behavior of key trace elements with a primary focus on the REEs Tm and Yb.
Jeffcoat, C. R.↗
Apollo 12 lunar samples - Trace element analysis of a core and the uniformity of the regolith
Apollo 12 lunar core and soil samples indicating meteoritic trace elements abundance
Anders, E.↗
Design and analysis of optical systems for the Stanford/MSFC Multi-Spectral Solar Telescope Array
This paper reports on the design and the theoretical ray trace analysis of the optical systems which will comprise the primary imaging components for the Stanford/MSFC Multi-Spectral Solar Telescope Array (MSSTA). This instrument is being developed for ultra-high resolution investigations of the sun from a sounding rocket. Doubly reflecting systems of sphere-sphere, ellipsoid-sphere (Dall-Kirkham), paraboloid-hyperboloid (Cassegrain), and hyperboloid-hyperboloid (Ritchey-Chretien) configurations were analyzed. For these mirror systems, ray trace analysis was performed and through-focus spot diagrams, point spread function plots, and geometrical and diffraction MTFs were generated. The results of these studies are presented along with the parameters of the Ritchey-Chretien optical system selected for the MSSTA flight. The payload, which incorporates seven of these Ritchey-Chretien systems, is now being prepared for launch in late September 1989.
Hadaway, James B.↗
A trace-driven analysis of name and attribute caching in a distributed system
This paper presents the results of simulating file name and attribute caching on client machines in a distributed file system. The simulation used trace data gathered on a network of about 40 workstations. Caching was found to be advantageous: a cache on each client containing just 10 directories had a 91 percent hit rate on name look ups. Entry-based name caches (holding individual directory entries) had poorer performance for several reasons, resulting in a maximum hit rate of about 83 percent. File attribute caching obtained a 90 percent hit rate with a cache on each machine of the attributes for 30 files. The simulations show that maintaining cache consistency between machines is not a significant problem; only 1 in 400 name component look ups required invalidation of a remotely cached entry. Process migration to remote machines had little effect on caching. Caching was less successful in heavily shared and modified directories such as /tmp, but there weren't enough references to /tmp overall to affect the results significantly. We estimate that adding name and attribute caching to the Sprite operating system could reduce server load by 36 percent and the number of network packets by 30 percent.
Shirriff, Ken W.↗
Light Isotopes and Trace Organics Analysis of Mars Samples with Mass Spectrometry
Precision measurement of light isotopes in Mars surface minerals and comparison of this isotopic composition with atmospheric gas and other, well-mixed reservoirs such as surface dust are necessary to understand the history of atmospheric evolution from a possibly warmer and wetter Martian surface to the present state. Atmospheric sources and sinks that set these ratios are volcanism, solar wind sputtering, photochemical processes, and weathering. Measurement of a range of trace organic species with a particular focus on species such as amino acids that are the building blocks of terrestrial life are likewise important to address the questions of prebiotic and present or past biological activity on Mars. The workshop topics "isotopic mineralogy" and "biology and pre-biotic chemistry" will be addressed from the point of view of the capabilities and limitations of insitu mass spectrometry (MS) techniques such as thermally evolved gas analysis (TEGA) and gas chromatography (GC) surface experiments using MS, in both cases, as a final chemical and isotopic composition detector. Insitu experiments using straightforward adaptations of existing space proven hardware can provide a substantial improvement in the precision and accuracy of our present knowledge of isotopic composition both in molecular and atomic species in the atmosphere and those chemically bound in rocks and soils. Likewise, detection of trace organic species with greatly improved sensitivity from the Viking GCMS experiment is possible using gas enrichment techniques. The limits to precision and accuracy of presently feasible insitu techniques compared to laboratory analysis of returned samples will be explored. The insitu techniques are sufficiently powerful that they can provide a high fidelity method of screening samples obtained from a diverse set of surface locations such as the subsurface or the interior of rocks for selection of those that are the most interesting for return to Earth.
Mahaffy, P.↗
Interplanetary dust - Trace element analysis of individual particles by neutron activation
Although micrometeorites of cometary origin are thought to be the dominant component of interplanetary dust, it has never been possible to positively identify such micrometer-sized particles. Two such particles have been identified as definitely micrometeorites since their abundances of volatile and nonvolatile trace elements closely match those of primitive solar system material.
Ganapathy, R.↗
Ordinary chondrites - Multivariate statistical analysis of trace element contents
The contents of mobile trace elements (Co, Au, Sb, Ga, Se, Rb, Cs, Te, Bi, Ag, In, Tl, Zn, and Cd) in Antarctic and non-Antarctic populations of H4-6 and L4-6 chondrites, were compared using standard multivariate discriminant functions borrowed from linear discriminant analysis and logistic regression. A nonstandard randomization-simulation method was developed, making it possible to carry out probability assignments on a distribution-free basis. Compositional differences were found both between the Antarctic and non-Antarctic H4-6 chondrite populations and between two L4-6 chondrite populations. It is shown that, for various types of meteorites (in particular, for the H4-6 chondrites), the Antarctic/non-Antarctic compositional difference is due to preterrestrial differences in the genesis of their parent materials.
Lipschutz, Michael E.↗
Trace element analysis of coal by neutron activation
The irradiation, counting, and data reduction scheme is described for an analysis capability of 1000 samples per year. Up to 56 elements are reported on each sample. The precision and accuracy of the method are shown for 25 elements designated as hazardous by the Environmental Protection Agency (EPA). The interference corrections for selenium and ytterbium on mercury and ytterbium on selenium are described. The effect of bromine and antimony on the determination of arsenic is also mentioned. The use of factorial design techniques to evaluate interferences in the determination of mercury, selenium, and arsenic is shown. Some typical trace element results for coal, fly ash, and bottom ash are given.
Sheibley, D. W.↗
Trace element analysis of coal by neutron activation.
The irradiation, counting, and data reduction scheme is described for an analysis capability of 1000 samples per year. Up to 56 elements are reported on each sample. The precision and accuracy of the method are shown for 25 elements designated as hazardous by the Environmental Protection Agency (EPA). The interference corrections for selenium and ytterbium on mercury and ytterbium on selenium are described. The effect of bromine and antimony on the determination of arsenic is also mentioned. The use of factorial design techniques to evaluate interferences in the determination of mercury, selenium, and arsenic is shown. Some typical trace element results for coal, fly ash, and bottom ash are given.
Sheibley, D. W.↗
Chromatographic detection and analysis of traces of hydrocarbons
Special analytical column having in series two separate absorption sections charged with beads of porous polymer and a sample of gas detects traces of hydrocarbons. New method requires only 15 minutes for execution.
Fickey, E. W.↗
Analysis of trace contaminants
Composition and daily fluctuations of trace contaminants during 90-day space station simulator test
Honorof, E. P.↗
Trace-element analysis of 1000 environmental samples per year using instrumental neutron activation analysis
The technology and methods developed at the Plum Brook Reactor to analyze 1000 samples per year and report data on as many as 56 elements are described. The manpower for the complete analysis of 20 to 24 samples per week required only 3 to 3.5 hours per sample. The solutions to problems encountered in sample preparation, irradiation, and counting are discussed. The automation of data reduction is described. Typical data on various sample matrices are presented.
Sheibley, D. W.↗
Dynamic delta method for trace gas analysis
Method has been developed in which measurements are made only over viscous flow range, eliminating fractionation before the molecular leak and problems due to surface elution.
Wood, G. M.↗