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NASA NTRS1989

Environmental effects on high strain rate properties of graphite/epoxy composite

The effects of hygrothermal conditions on the high-strain-rate properties of a unidirectional graphite/epoxy material, AS4/3501-6, were evaluated using standard physical and mechanical tests to determine the properties of the lamina. A time-temperature-moisture equivalence principle was applied to obtain master curves for the longitudinal, transverse, and in-plane shear moduli and corresponding strengths and ultimate strains of the specimens. It was found that the longitudinal properties of the material remained unchanged at all conditions, except for the longitudinal modulus, which showed a slight increase with temperature, moisture, and strain rate. On the other hand, all transverse and intralaminar shear properties were found to decrease with increasing temperature and moisture contents at a fixed strain rate.

Yaniv, Gershon↗

NASA NTRS1999

Effect of a Nonplanar Melt-Solid Interface On Lateral Compositional Distribution During Unidirectional Solidification of a Binary Alloy with a Constant Growth Velocity V: Theory - Pt. 1

Infrared detected materials, such as Hg(1-x)Cd(x)Te, Hg(1-x)Zn(x)Te have energy gaps almost linearly proportional to their composition. Due to the wide separation of liquidus and solidus curves of their phase diagram, there are compositional segregation in both of the axial and radial directions of these crystals grown in the Bridgman system unidirectionally with constant growth rate. It is important to understand the mechanisms, which affect lateral segregation such that large radially uniform composition crystal can be produced. Following Coriel, etc's treatment, we have developed a theory to study the effect of a curved melt-solid interface shape on lateral composition distribution. The model is considered to be a cylindrical system with azimuthal symmetry and a curved melt-solid interface shape which can be expressed as a linear combination of a series of Bessell's functions. The results show that melt-solid interface shape has a dominant effect on the lateral composition distribution of these systems. For small values of beta, the solute concentration at the melt-solid interface scales linearly with interface shape with a proportional constant of the produce of beta and (1 -k), where beta = VR/D, with V as growth velocity, R as the sample radius, D as the diffusion constant and k as the distribution constant. A detailed theory will be presented. A computer code has been developed and simulations have been performed and compared with experimental results. These will be published in another paper.

Wang, Jai-Ching↗

NASA NTRS1999

Effect of a Nonplanar Melt-Solid Interface on Lateral Compositional Distribution during Unidirectional Solidification of a Binary Alloy with a Constant Growth Velocity V: Theory - Part 1

Infrared detector materials, such as Hg(1-x)Cd(x)Te, Hg(1-x)Zn(x)Te have energy gaps almost linearly proportional to its composition. Due to the wide separation of liquidus and solidus curves of their phase diagram, there are compositional segregations in both of axial and radial directions of these crystals grown in the Bridgman system unidirectionally with constant growth rate. It is important to understand the mechanisms which affect lateral segregation such that large uniform radial composition crystal is possible. Following Coriell, etc's treatment, we have developed a theory to study the effect of a curved melt-solid interface shape on the lateral composition distribution. The system is considered to be cylindrical system with azimuthal symmetric with a curved melt-solid interface shape which can be expressed as a linear combination of a series of Bessell's functions. The results show that melt-solid interface shape has a dominate effect on lateral composition distribution of these systems. For small values of b, the solute concentration at the melt-solid interface scales linearly with interface shape with a proportional constant of the product of b and (1 - k), where b = VR/D, with V as growth velocity, R as sample radius, D as diffusion constant and k as distribution constant. A detailed theory will be presented. A computer code has been developed and simulations have been performed and compared with experimental results. These will be published in another paper.

Wang, Jai-Ching↗

NASA NTRS2020

An Improved Plastically Dilatant Unified Viscoplastic Constitutive Formulation for Multiscale Analysis of Polymer Matrix Composites Under High Strain Rate Loading

Polymer matrix composites are commonly used to fabricate energy-absorbing structures expected to experience impact loading. As such, a detailed understanding of the dynamic response of the constituent materials is necessary. Since the rate, temperature, and pressure dependence of carbon fiber reinforced polymer matrix composites are primarily manifestations of the rate, temperature, and pressure dependence of the polymer matrix, it is crucial that the constitutive behavior of the matrix be accurately characterized. In this work, an existing unified viscoplastic constitutive formulation is extended to ensure thermodynamic consistency and to more accurately account for the tension-compression asymmetry observed in the response of polymeric materials. A new plastic potential function is proposed, and elementary loading conditions are utilized to determine relations between model constants to ensure nonnegative plastic dissipation, a necessary thermodynamic requirement. Expressions for plastic Poisson’s ratios are derived and are bounded by enforcing nonnegative plastic dissipation. The model is calibrated against available experimental data from tests conducted over a range of strain rates, temperatures, and loading cases on a representative thermoset epoxy; good correlation between simulations and experimental data is obtained. Temperature rises due to the conversion of plastic work to heat are computed via the adiabatic heat energy equation. The viscoplastic polymer model is then used as a constitutive model in the generalized method of cells micromechanics theory to investigate the effects of matrix adiabatic heating on the high strain rate response of a unidirectional composite. The thermodynamic consistency of the model ensures plastic dissipation can only cause an increase in temperature. Simulation results indicate that significant thermal softening due to the conversion of plastic work to heat is observed in the composite for matrix dominated deformation modes.

Impact loading↗

NASA NTRS1991

Characterization of elastic-viscoplastic properties of an AS4/PEEK thermoplastic composite

The elastic-viscoplastic properties of an AS4/PEEK (APC-2) thermoplastic composite were characterized at 24 C (75 F) and 121 C (250 F) by using a one-parameter viscoplasticity model. To determine the strain-rate effects, uniaxial tension tests were performed on unidirectional off-axis coupon specimens with different monotonic strain rates. A modified Bodner and Partom's model was also used to describe the viscoplasticity of the thermoplastic composite. The experimental results showed that viscoplastic behavior can be characterized quite well using the one-parameter overstress viscoplasticity model.

Yoon, K. J.↗

NASA NTRS1976

Strain rate effects on mechanical properties of fiber composites, part 3

An experimental investigation was conducted to determine the strain rate effects in fiber composites. Unidirectional composite specimens of boron/epoxy, graphite/epoxy, S-glass/epoxy and Kevlar/epoxy were tested to determine longitudinal, transverse and intralaminar (in-plane) shear properties. In the Longitudinal direction the Kevlar/epoxy shows a definite increase in both modulus and strength with strain rate. In the transverse direction, a general trend toward higher strength with strain rate is noticed. The intralaminar shear moduli and strengths of boron/epoxy and graphite/epoxy show a definite rise with strain rate.

Daniel, I. M.↗

DOE OSTI2020

Exploring an ‘ideal hill': how lithology and transport mechanisms affect the possibility of a steady state during weathering and erosion

We introduce a model of chemical reaction within hills to explore how evolving porosity (and by inference, permeability) affects flow pathways and weathering. The model consists of hydrologic and reactive-transport equations that describe alteration of ferrous minerals and feldspar. These reactions were chosen because previous work emphasized that oxygen- and acid-driven weathering affects porosity differently in felsic and mafic rocks. A parameter controlling the order of the fronts is presented. In the absence of erosion, the two reaction fronts move at different velocities and the relative depths depend on geochemical conditions and starting composition. In turn, the fronts and associated changes in porosity drastically affect both the vertical and lateral velocities of water flow. For these instances, estimates of weathering advance rates based on simple models that posit unidirectional constant-velocity advection do not apply. In the model hills, weathering advance rates diminish with time as the Darcy velocities decrease with depth. The system can thus attain a dynamical steady state at any erosion rate where the regolith thickness is constant in time and velocities of both fronts become equal to one another and to the erosion rate. The slower the advection velocities in a system, the faster it attains a steady state. For example, a massive rock with relatively fast-dissolving minerals such as diabase -- where solute transport across the reaction front mainly occurs by diffusion -- can reach a steady state more quickly than granitoid rocks in which advection contributes to solute transport. The attainment of a steady state is controlled by coupling between weathering and hydrologic processes that force water to flow horizontally above reaction fronts where permeability changes rapidly with depth and acts as a partial barrier to fluid flow.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS1985

Delamination micromechanics analysis

A three-dimensional finite element analysis was developed which includes elastoplastic, orthotropic material response, and fracture initiation and propagation. Energy absorption due to physical failure processes characteristic of the heterogeneous and anisotropic nature of composite materials is modeled. A local energy release rate in the presence of plasticity was defined and used as a criterion to predict the onset and growth of cracks in both micromechanics and macromechanics analyses. This crack growth simulation technique is based upon a virtual crack extension method. A three-dimensional finite element micromechanics model is used to study the effects of broken fibers, cracked matrix and fiber-matrix debond on the fracture toughness of the unidirectional composite. The energy release rates at the onset of unstable crack growth in the micromechanics analyses are used as critical energy release rates in the macromechanics analysis. This integrated micromechanical and macromechanical fracture criterion is shown to be very effective in predicting the onset and growth of cracks in general multilayered composite laminates by applying the criterion to a single-edge notched graphite/epoxy laminate subjected to implane tension normal to the notch.

Adams, D. F.↗

NASA NTRS1991

High strain rate properties of off-axis composite laminates, part 2

Unidirectional off-axis graphite/epoxy and graphite/S-glass/epoxy laminates were characterized in uniaxial tension at strain rates ranging from quasi-static to over 500 s(sup -1). Laminate ring specimens were loaded by internal pressure with the tensile stress at 22.5, 30, and 45 degrees relative to the fiber direction. Results were presented in the form of stress-strain curves to failure. Properties determined included moduli, Poisson's ratios, strength, and ultimate strain. In all three laminates of both materials the modulus and strength increase sharply with strain rate, reaching values roughly 100, 150, and 200 percent higher than corresponding static values for the 22.5(sub 8), 30(sub 8), and 45(sub 8) degree laminates, respectively. In the case of ultimate strain no definite trends could be established, but the maximum deviation from the average of any value for any strain rate was less than 18 percent.

Daniel, I. M.↗

NASA NTRS1988

Gravitational macrosegregation in unidirectionally solidified lead-tin alloy

Nine small samples of binary lead-tin alloys were solidifed unidirectionally upward, with both cooling rate and thermal gradient being closely controlled. Results presented include thermal measurements, chemical composition measurements, and microstructural characterization. In the six Pb-15 wt pct Sn ingots, normal macrosegregation was observed, with Sn content being highest at the top of the ingot. No significant macrosegretation was noted in the three ingots of nominal composition Sn-15 wt pct Sn.

Wang, L.↗

DOE OSTI2026

Characteristics of Fluid‐Solid Interaction Constitutive Models Within Poroelastodynamics at Higher Strain‐Rates and Large Deformations Implemented in 1D

The large deformation, mixed formulation, finite element (FE) modeling approach presented in Irwin et al. 2024 is extended herein to include improved constitutive models for representing dynamic solid-fluid interactions at higher strain rates (𝒪⁢(1⁢0 2 −1⁢0 3 )⁢s −1 ) and larger overpressure magnitudes (𝒪⁡(1⁢0 2 )⁢kPa) within a biphasic soft porous material using Theory of Porous Media (TPM) at finite strain. Specifically, these constitutive modeling improvements are the following: (i) a more physically robust constitutive model for pore fluid seepage velocity via inclusion of pore fluid viscous stress, and (ii) a modified deformation-dependent-permeability model and updated hyperelastic constitutive model better suited for handling larger volumetric compressions and extensions. The novelty of the present work is mainly the contribution (i): inclusion of pore fluid viscous stress at higher strain-rate and large deformations, which requires 𝐶 1 continuity in the weak formulation, accomplished by employing Hermite cubic interpolation functions within a mixed nonlinear poromechanical finite element formulation. In (ii), the model is updated to weakly enforce solid phase incompressibility, such that this assumption is not violated numerically, which provides improved numerical stability for achieving larger overpressure magnitudes on 𝒪⁡(1⁢0 2 ) kPa, which were not achievable with the previous Kozeny–Carman model in Irwin et al. 2024. Also in (ii), the volumetric part of the solid skeleton free energy function is modified to ensure proper bounds on the solid skeleton Jacobian of deformation 𝐽 s related to incompressibility of the solid phase. Uniaxial strain, unidirectional flow examples at higher strain rates (𝒪⁢(1⁢0 2 −1⁢0 3 )⁢s −1 ) and larger deformations (up to 0.2 (or 20%) nominal axial strain) demonstrate the improved physical representation—and numerical stability—of these constitutive model improvements.

42 ENGINEERING↗

NASA NTRS1975

Acoustic emission from composite-reinforced metals

Acoustic-emission (AE) count rates are presented for tensile loading of unidirectional boron-epoxy and for aluminum sheets reinforced with unidirectional boron-epoxy. It is shown that different prepreg materials have different characteristic AE patterns. Results from composite-reinforced metal specimens show that early failures are accompanied by a sharp increase in AE count rate at the knee of the bilinear stress-strain diagram. It is further shown that the count rates are a function of specimen fabrication and that higher total counts do not necessarily correspond to early failures.

Henneke, E. G., II↗

NASA NTRS1988

Hygrothermal and strain-rate effects on properties of graphite/epoxy composites

The combined effects of moisture (M), temperature (T), and strain rate (SR) on the properties of the unidirectional graphite/epoxy composite AS4/3501-6 are investigated experimentally. Longitudinal tensile, in-plane shear, and transverse tensile specimens with moisture content 0 or 1 percent were characterized using standard mechanical tests and the techniques described by Yaniv et al. (1987) at temperatures 23-128 C and strain rates from 5 x 10 to the -6th/sec to 5/sec. The results are presented in graphs and discussed in detail. The longitudinal properties of the composite were found to be generally unaffected by changes in the parameters, whereas transverse and interlaminar properties decreased with increasing T and M at constant SR and the transverse and in-plane shear moduli increased with SR. A time-T-M equivalence principle is used to derive master curves for all the matrix-dominated properties, expressed in terms of a two-variable shift function.

Daniel, I. M.↗

NASA NTRS2014

A Novel Method for Characterizing Fatigue Delamination Growth Under Mode I Using the Double Cantilever Beam Specimen

A novel method is proposed to obtain Mode I delamination growth rate from a Double Cantilever Beam (DCB) specimen. In the proposed method, Unidirectional (UD) DCB specimens are tested in fatigue at different initial maximum energy release rates levels. The growth rate data obtained in the first increments of crack growth at each maximum energy release rate level are used to generate a Paris Law equation, which characterizes delamination growth rate without fiber-bridging, and can also be used to determine a delamination onset curve. The remaining delamination growth rate data from each test are used to determine a modified Paris law, which characterizes the delamination growth rate in a DCB specimen, explicitly accounting for fiber-bridging. The proposed expression captures well the scatter in experimental data obtained using the DCB specimens, suggesting its adequacy. The Paris Law characterizing delamination growth rate without fiber-bridging predicts higher delamination growth rates for the same maximum energy release rate applied, leading to a conservative estimate for delamination growth. This is particularly relevant, since in generic ply interfaces, fiber-bridging is less predominant than in UD DCB specimens. Failing to account for fiber-bridging in UD DCB specimens may underestimate the delamination growth rate, yielding non-conservative predictions.

Carvalho, Nelson↗

NASA NTRS1979

Wave propagation in transversely impacted composite laminates

An experimental study was conducted to determine the wave-propagation characteristics, transient strains and residual properties of unidirectional and angle-ply boron/epoxy and graphite/epoxy laminates impacted with silicon-rubber projectiles at velocities up to 250 m/sec. Results include the following: (1) the predominant wave is the flexural wave propagating at different velocities in different directions; (2) peak strains and strain rates in the transverse to the (outer) fiber direction are much higher than those in the direction of the fibers; (3) strain rates up to 640/sec were measured; and (4) unidirectional laminates under impact showed appreciable modulus and strength degradation in the direction transverse to fibers.

Daniel, I. M.↗

NASA NTRS1981

Strain rate, temperature, and humidity on strength and moduli of a graphite/epoxy composite

Results of an experimental study of the influence of strain rate, temperature and humidity on the mechanical behavior of a graphite/epoxy fiber composite are presented. Three principal strengths (longitudinal, transverse and shear) and four basic moduli (E1, E2, G12 and U12) of a unidirectional graphite/epoxy composite were followed as a function of strain rate, temperature and humidity. Each test was performed at a constant tensile strain rate in an environmental chamber providing simultaneous temperature and humidity control. Prior to testing, specimens were given a moisture preconditioning treatment at 60 C. Values for the matrix dominated moduli and strength were significantly influenced by both environmental and rate parameters, whereas the fiber dominated moduli were not. However, the longitudinal strength was significantly influenced by temperature and moisture content. A qualitative explanation for these observations is presented.

Lifshitz, J. M.↗

DOE OSTI2022

Deep learning-based noise filtering toward millisecond order imaging by using scanning transmission electron microscopy

Application of scanning transmission electron microscopy (STEM) to in situ observation will be essential in the current and emerging data-driven materials science by taking STEM’s high affinity with various analytical options into account. As is well known, STEM’s image acquisition time needs to be further shortened to capture a targeted phenomenon in real-time as STEM’s current temporal resolution is far below the conventional TEM’s. However, rapid image acquisition in the millisecond per frame or faster generally causes image distortion, poor electron signals, and unidirectional blurring, which are obstacles for realizing video-rate STEM observation. Here we show an image correction framework integrating deep learning (DL)-based denoising and image distortion correction schemes optimized for STEM rapid image acquisition. By comparing a series of distortion corrected rapid scan images with corresponding regular scan speed images, the trained DL network is shown to remove not only the statistical noise but also the unidirectional blurring. This result demonstrates that rapid as well as high-quality image acquisition by STEM without hardware modification can be established by the DL. The DL-based noise filter could be applied to in-situ observation, such as dislocation activities under external stimuli, with high spatio-temporal resolution.

47 OTHER INSTRUMENTATION↗

NASA NTRS1984

Hot stage and sample cell design for the solidification of transparent materials with and without forced convection

A temperature gradient stage design for optical microscopy is described. Exceptional thermal stability is the major feature. The stage is used to study crystal growth phenomena occurring at the solid-liquid interface. The apparatus is designed to use transparent organic solutions as models for the study of metal-like solidification. The stage provides a controlled thermal environment for unidirectional solidification of low melting temperature materials. Freezing rate is regulated by mechanically sliding in the stage a thin glass cell containing the materials being studied. Two cell assemblies are described. One type is used for convection-free and the other for controlled forced convection studies of the solidification interface.

Kaukler, W. F.↗