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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 361 records · Page 20
All sourcesNASA NTRSDOE OSTI
NASA NTRS1990

Low cost attitude sensors for spacecraft

A review is presented of two-low cost attitude sensors developed with existing technology, but with emphasis directed to reducing the unit costs without compromising reliability or quality. The solar aspect sensor was developed to determine the angle of the sun with respect to the optical axis of the Shuttle Solar Backscatter Ultraviolet (SSBUV) Experiment Package. Using sensor readings updated every five milliseconds, signal processing electronics determine the location of the center of the sun's image on the array. An earth horizon sensor was developed to measure the nadir angle with respect to the optical axis of the SSBUV Experiment Package to an accuracy of + or - 0.5 deg. Operation of each of the sensors is described along with flight results obtained when flown onboard Atlantis as part of the SSBUV Experiment Package.

Auer, S.↗
NASA NTRS1993

Enhancement of photoluminescence intensity of GaAs with cubic GaS chemical vapor deposited using a structurally designed single-source precursor

A two order-of-magnitude enhancement of photoluminescence intensity relative to untreated GaAs has been observed for GaAs surfaces coated with chemical vapor-deposited GaS. The increase in photoluminescence intensity can be viewed as an effective reduction in surface recombination velocity and/or band bending. The gallium cluster /(t-Bu)GaS/4 was used as a single-source precursor for the deposition of GaS thin films. The cubane core of the structurally characterized precursor is retained in the deposited film producing a cubic phase. Furthermore, a near-epitaxial growth is observed for the GaS passivating layer. Films were characterized by transmission electron microscopy, X-ray powder diffraction, and X-ray photoelectron and Rutherford backscattering spectroscopies.

Macinnes, Andrew N.↗
NASA NTRS1993

Photoluminescence intensity enhancement of GaAs by vapor-deposited GaS - A rational approach to surface passivation

A two order-of-magnitude enhancement of photoluminescence intensity relative to untreated GaAs has been observed for GaAs surfaces coated with chemical vapor-deposited GaS. The increase in photoluminescence intensity can be viewed as an effective reduction in surface recombination velocity and/or band bending. The gallium cluster (/t-Bu/GaS)4 was used as a single-source precursor for the deposition of GaS thin films. The cubane core of the structurally-characterized precursor is retained in the deposited film producing a cubic phase. Furthermore, a near-epitaxial growth is observed for the GaS passivating layer. Films were characterized by transmission electron microscopy, X-ray powder diffraction, and X-ray photoelectron and Rutherford backscattering spectroscopies.

Jenkins, Phillip P.↗
NASA NTRS1994

Reaction of Ta thin film with single crystalline (001) beta-SiC

The reaction between a sputtered-deposited Ta film (320 nm thick) and a single crystalline (001) beta-SiC substrate induced by vacuum annealing at temperatures of 600-1200 C for 1 h (30 min at 1100 C) is investigated by 3 MeV He(+2) backscattering spectrometry, x-ray diffraction, secondary ion mass spectrometry, and transmission and scanning electron microscopies. No significant reaction is observed at 800 C or at lower tempertures. At 900 C, the main product phases are Ta2C and carbon-stabilized Ta5Si3. A minor amount of unreacted Ta is also present. After annealing at 1000 C, all the tantalum has reacted; the reaction zone possesses a multilayered structure of beta-SiC/TaC/carbon-stabilized Ta5Si3/alpha-Ta5Si3/Ta2C. The diffusion path at 1000 C is plotted on the isothermal section of the Ta-Si-C phase diagram. At 1100 C, the reacted layer has an interface with the SiC substrate that is still quite flat but has a rough surface due to the formation of macroscopic voids within the reacted layer. The equilibrium products predicted by the phase diagram are TaC and TaSi2. This final state is reached by annealing at 1200 C for 1 h. At that point, the reacted layer has a latterally very uneven structure and morphology.

Chen, J. S.↗
NASA NTRS2007

RadSTAR L-Band Imaging Scatterometer: Performance Assessment

RadSTAR is an instrument development program aimed at combining a radiometer and a scatterometer system into a highly compact configuration that uses a single, electronically scanned antenna to provide co-located and simultaneous measurements of emission and backscatter for airborne and spaceborne applications [I]. The program was designed to map soil moisture and ocean salinity, both important components of the water cycle, and to map sea ice density and thickness, an important factor in ocean-atmosphere heat exchange in Polar Regions. The accuracy in estimation of these and a number of other Earth science parameters can be greatly enhanced by providing the co-aligned radar/radiometer microwave measurements. For instance, radiometer estimates of soil moisture from soil emission are affected by emission from vegetation, and from the roughness of the surface. Complementary measurements using the scatterometer can be used to evaluate the vegetation and surface roughness effects. Hence, the combined observations can provide an improved estimate. As with soil moisture, the ocean salinity is a function of the microwave emission from the sea surface temperature (SST) and sea roughness. There, the addition of radar backscatter measurements of sea roughness enables the correction of the emissivity and provide more accurate estimates of ocean salinity. Similar arguments can be made for other important Earth science parameters. This paper discusses the RadSTAR program, the radar system design, calibration, and digital beamforming techniques, and presents preliminary analysis of the data collected during the test flights. The data sets obtained during the flights and during the radar calibration in the anechoic chamber are also employed to asses the performance of the radar. The paper also discusses the Digital Beamforming Synthetic Aperture Radar (DBSAR) processor, a real-time processor recently developed for the LIS instrument which enables beam synthesis, fine resolutions, and large swaths.

Rincon, Rafael↗
NASA NTRS1972

A new method for in situ electron temperature determinations from plasma wave phenomena

A discrepancy has been reported between the values of the electron temperature t sub e deduced from satellite electrostatic probe measurements and ground based radar backscatter measurements. This discrepancy (radar backscatter temperature less than the probe temperature) is not present when the probe experiment is flown on a rocket to lower altitudes but reappears when the rocket probe attains higher altitudes. There is a need for an independent radio wave method for making in-situ t sub e measurements in order to help resolve this problem. A new method of determining t sub e from the satellite resonant phenomena is presented. It is based on the splitting (observed at high latitudes) of the diffuse resonance which occurs at the frequency f sub d1 between f sub h and 2 f sub h. The advantage of this method over the other methods involving ionospheric resonances is the simplicity of the required calculations. There is, however, the limitation of plasma conditions where the f sub d1 resonance can be observed and the limitation to mid-to-high latitudes where the splitting is observed.

Oya, H.↗
NASA NTRS1985

Comparative in situ studies of the unstable day-time equatorial E-region

Three in situ rocket observations of electrostatic fluctuations which characterize the strong, mild, and weak day-time unstable E-region are compared. The fluctuations are analyzed in relation to the ambient electron density gradients, the measured or inferred drift velocities and, where possible, to simultaneous VHF backscatter radar measurements. Based on these parameters, the linear dispersion relation is solved to find the range of altitudes and wavenumbers for which the growth rate indicates that instability will occur. These computations are compared with actual observations of the irregularities. How well the linear growth rate predicts the altitude range of the unstable layer, and to what extent the regime of the unstable wavenumbers is reflected in the spectra of the irregularities, is shown. Overall, the agreement is good.

Pfaff, R. F.↗
NASA NTRS1992

Spacecraft thermal control coatings

The Experiment AO 138-6 was located on the trailing edge of the Long Duration Exposure Facility as part of the French Cooperative Payload (FRECOPA) Experiment. It was purely passive in nature: material specimens 2 x 2 cm, independently mounted in sample-holders, with their surface in the same reference plane, were exposed to space. Thirty samples were set in a vacuum-tight canister which was opened in space a few days after LDEF deployment and closed while still in orbit ten months later; twenty-four samples were directly exposed to space for the total flight duration (preflight handling, shuttle bay environment, separation from shuttle, shuttle environment, LEO environment, docking, descent, transfer to KSC). Materials included paints (conductive or nonconductive), SSM's, polymeric films, surface coatings, composite materials, and metals. After sample retrieving, inspection and measurements were carried out in atmospheric laboratory conditions on each sample: observation with binocular lenses and scanning electron microscopy, spectral relectance and transmittance using an integrating sphere in the wavelength range 280-2300 nm, emissivity by the means of a Gier & Dunkle portable reflectometer, electron spectroscopy for chemical analysis-x-ray photoelectron spectroscopy (ESCA-XPS), and Rutherford backscattering spectroscopy (RBS) measurements on some selected samples. The results obtained from flight were compared to laboratory data obtained in UV-irradiation tests when these data were available. As a general statement a good spectral concordance is observed for all samples not in the canister so long as air recoveries are taken into account. For one material, the degradation is more important for the sample in the canister than for those of the same material mounted at the surface of the tray; for most samples in the canister the degradation is slightly higher than the one which can be predicted from laboratory standard irradiations. Contamination problems having been ruled out, the higher temperature experience by the samples on the inside of canister probably explains these phenomena.

Guillaumon, Jean-Claude↗
NASA NTRS1997

A Novel Microcharacterization Technique in the Measurement of Strain and Orientation Gradient in Advanced Materials

Representation of morphology and evolution of the microstructure during processing and their relation to properties requires proper experimental techniques. Residual strains, lattice distortion, and texture (micro-texture) at the interface and the matrix of a layered structure or a functionally gradient material and their variation are among parameters important in materials characterization but hard to measure with present experimental techniques. Current techniques available to measure changes in interred material parameters (residual stress, micro-texture, microplasticity) produce results which are either qualitative or unreliable. This problem becomes even more complicated in the case of a temperature variation. These parameters affect many of the mechanical properties of advanced materials including stress-strain relation, ductility, creep, and fatigue. A review of some novel experimental techniques using recent advances in electron microscopy is presented here to measure internal stress, (micro)texture, interracial strength and (sub)grain formation and realignment. Two of these techniques are combined in the chamber of an Environmental Scanning Electron Microscope to measure strain and orientation gradients in advanced materials. These techniques which include Backscattered Kikuchi Diffractometry (BKD) and Microscopic Strain Field Analysis are used to characterize metallic and intermetallic matrix composites and superplastic materials. These techniques are compared with the more conventional x-ray diffraction and indentation techniques.

Garmestai, H.↗
NASA NTRS1983

Backscattering cascade of beam modes off ambient density fluctuations

The effects of a given nonthermal low-frequency density-fluctuation spectrum on the amplification of Langmuir waves by a 'bump-on-tail' beam of electrons are studied. The density-fluctuation spectrum is assumed to contain a uniform distribution of wavelengths ranging from much shorter than the beam mode wavelength to of the same order. This permits multiple large-angle (back) scattering to occur. One-dimensional numerical solutions of the kinetic equations are found which yield criteria for linear saturation of the beam instability of a cascade of backscattering to high wavenumber. The relevant time scales and spectral shapes are also determined in both the stable and unstable regions. Linear damping and Cerenkov emission by a possible nonthermal tail of electrons is taken into account. An application is made to the beam modes observed simultaneously with density fluctuations off the Jovian bow shock. It is shown that the observed level of density fluctuations is sufficient to saturate the unstable Langmuir waves, although nonthermal Landau damping may prevent a cascade to very high wavenumbers.

Russell, D. A.↗
NASA NTRS1978

The localized origin of equatorial F region irregularity patches

An intensive study of nighttime irregularities of electron density in the equatorial ionosphere was performed in October 1976 by making 50-MHz radar backscatter measurements at Jicamarca, Peru, and scintillation measurements of 249-MHz transmissions from Les 9 at two ground stations (Ancon and Huancayo, both in Peru) as well as by aircraft flying in the vicinity of the stations. The 137-MHz scintillations from the orbiting Wideband satellite were also recorded at Huancayo. The results of such measurements made on October 16-17, 1976, are discussed in this report. We find that on this particular night a large-scale irregularity patch evolved first in the west, as was detected by the radar at Jicamarca, and drifted eastward to cause successive onsets of scintillation activity on propagation paths from Ancon and Huancayo. The observations indicate the east-west dimension of the large-scale structure to be 400 km drifting eastward at a speed of approximately 100 m/s, having a lifetime of several hours, and containing a hierarchy of irregularity scale sizes in the range of kilometers to meters causing both scintillations at 249 MHz and radar backscatter at 50 MHz.

Aarons, J.↗
NASA NTRS1979

Pulsed-electron-beam annealing of ion-implantation damage

Short-duration high-intensity pulsed electron beams have been used to anneal ion-implantation damage in silicon and to electrically activate the dopant species. Lattice regrowth and dopant activation were determined using He(+)-4 backscattering, SEM, TEM, and device performance characteristics as diagnostic techniques. The annealing mechanism is believed to be liquid-phase epitaxial regrowth initiating from the substrate. The high-temperature transient pulse produced by the electron beam causes the dopant to diffuse rapidly in the region where the liquid state is achieved.

Greenwald, A. C.↗
DOE OSTI2026

Expanding the Zinc Precursor Toolbox: A Comparative Study of Precursors for Thermal ALD of ZnO Thin Films

Atomic layer deposition (ALD) of zinc oxide (ZnO) has been widely researched using diethyl zinc (DEZ)-based methods. The significant importance of thin films of ZnO as transparent conductive oxides (TCO) in optoelectronic devices and photovoltaics warrants examining alternative Zn precursors for ZnO ALD as potential replacements for the pyrophoric DEZ. In this study, we investigated three alternative Zn precursors: Zn(EEKI)2, Zn(DMP)2, ZnEt(HMDS), in the process development for high-quality ZnO thin films and compared them to DEZ. The ALD processes were studied using in situ spectroscopic ellipsometry. The properties of the ALD ZnO films were characterized using ex situ X-ray photoelectron spectroscopy (XPS), Rutherford backscattering spectrometry and nuclear reaction analysis (RBS/NRA), X-ray diffraction (XRD), atomic force microscopy (AFM), transmission electron microscopy (TEM), and ultraviolet-visible (UV/Vis) spectrophotometry. These measurements confirmed the formation of pure, stoichiometric, and polycrystalline ZnO films using all four Zn precursors. Although the selected precursors are chemically diverse Zn compounds, they all yielded saturating ALD processes and high-quality ZnO thin films at 200 °C. This study highlights the potential benefits of alternative zinc precursors in designing ALD processes for ZnO thin films.

Obenlüneschloß, Jorit↗
NASA NTRS1990

Narrow bandgap semiconducting silicides: Intrinsic infrared detectors on a silicon chip

Work done during the final report period is presented. The main technical objective was to achieve epitaxial growth on silicon of two semiconducting silicides, ReSi2 and CrSi2. ReSi2 thin films were grown on (001) silicon wafers by vacuum evaporation of rhenium onto hot substrates in ultrahigh vacuum. The preferred epitaxial relationship was found to be ReSi2(100)/Si(001) with ReSi2(010) parallel to Si(110). The lattice matching consists of a common unit mesh of 120 A(sup 2) area, and a mismatch of 1.8 percent. Transmission electron microscopy revealed the existence of rotation twins corresponding to two distinct but equivalent azimuthal orientations of the common unit mesh. MeV He(+) backscattering spectrometry revealed a minimum channeling yield of 2 percent for an approximately 1,500 A thick film grown at 650 C. Although the lateral dimension of the twins is on the order of 100 A, there is a very high degree of alignment between the ReSi2(100) and the Si(001) planes. Highly oriented films of CrSi2 were grown on (111) silicon substrates, with the matching crystallographic faces being CrSi2(001)/Si(111). The reflection high-energy electron diffraction (RHEED) patterns of the films consist of sharp streaks, symmetrically arranged. The predominant azimuthal orientation of the films was determined to be CrSi2(210) parallel to Si(110). This highly desirable heteroepitaxial relationship has been obtained previously by others; it may be described with a common unit mesh of 51 A(sup 2) and mismatch of 0.3 percent. RHEED also revealed the presence of limited film regions of a competing azimuthal orientation, CrSi2(110) parallel to Si(110). A channeling effect for MeV He(+) ions was not found for this material. Potential commercial applications of this research may be found in silicon-integrated infrared detector arrays. Optical characterizations showed that semiconducting ReSi2 is a strong absorber of infrared radiation, with the adsorption constant increasing above 2 x 10(exp 4) cm(sup -1) for photon energies above 0.2 eV. CrSi2 is of potential utility for detection at photon energies above approximately 0.3 eV.

Mahan, John E.↗
NASA NTRS2007

Comparisons of NDT Methods to Inspect Cork and Cork filled Epoxy Bands

Sheet cork and cork filled epoxy provide external insulation for the Reusable Solid Rocket Motor (RSRM) on the Nation's Space Transportation System (STS). Interest in the reliability of the external insulation bonds has increased since the Columbia incident. A non-destructive test (NDT) method that will provide the best inspection for these bonds has been under evaluation. Electronic Shearography has been selected as the primary NDT method for inspection of these bond lines in the RSRM production flow. ATK Launch Systems Group has purchased an electronic shearography system that includes a vacuum chamber that is used for evaluation of test parts and custom vacuum windows for inspection of full-scale motors. Although the electronic shearography technology has been selected as the primary method for inspection of the external bonds, other technologies that exist continue to be investigated. The NASA/Marshall Space Flight Center (MSFC) NDT department has inspected several samples for comparison with electronic shearography with various inspections systems in their laboratory. The systems that were evaluated are X-ray backscatter, terahertz imaging, and microwave imaging. The samples tested have some programmed flaws as well as some flaws that occurred naturally during the sample making process. These samples provide sufficient flaw variation for the evaluation of the different inspection systems. This paper will describe and compare the basic functionality, test method and test results including dissection for each inspection technology.

Lingbloom, Mike↗
NASA NTRS1994

Electron density measurements during the NLC-91 campaign

A Super Arcas rocket, MISTI B, containing DC and RF probes, was launched as a part of the PMSE (Polar Mesosphere Summer Echoes) Salvo during the NLC-91 (Noctilucent Cloud) campaign to measure electron density irregularities with high spatial resolution. Measurements of large and small scale structures in the electron density were made on rocket ascent and descent at the altitudes of 86.5 and 88.5 +/- 0.5 km corresponding to the two altitudes of strongest backscatter recorded by the nearby CUPRI (Cornell University Portable Radar Interferometer) radar. Power spectra of the fluctuations shows two different structuring and scattering mechanisms exist at altitudes only 1 km apart. Since the rocket apogee was 89 km, the rocket was in the height range 88.5 +/- 0.5 km for 30 seconds giving an unusual measurement of horizontal structure over a distance of 5.5 km. Using the simultaneous DC and RF probe measurements of electron depletions and sharp gradient in the lower layer, the role of aerosols in creating these depletions and gradients is speculated upon.

Ulwick, J. C.↗
NASA NTRS1973

Parametric instability of a relativistically strong electromagnetic wave.

The stability of a circularly polarized electromagnetic wave that is strong enough to make plasma electrons, but not ions, relativistic is studied. Small perturbations are considered which propagate parallel to the large-amplitude driver. A relativistically strong wave can be unstable on time scales as short as twice its own oscillation period, and decays into a forward-going plasma oscillation and either one or two electromagnetic waves. Ion motion introduces an additional instability which can be important at short perturbation wavelengths, where the driver would otherwise be stable. The unstable ion and electron modes both have potential for producing anomalously large acceleration of relativistic particles, as well as significant amounts of backscattered light. These effects may be important in two applications: (1) the use of intense lasers to heat or compress plasma, and (2) the plasma surrounding a pulsar, if the pulsar is losing energy by radiation of electromagnetic waves at its rotation frequency. Instability persists in the nonrelativistic regime, reducing to stimulated Raman scattering as a special case.

Max, C. E.↗