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DOE OSTI2025

Multiscale modeling and laser diagnostics to reveal non-equilibrium reaction chemistry at a plasma-liquid interface

Low-temperature, atmospheric-pressure plasmas in contact with liquid are at the core of a wide range of applications including water treatment, medicine, materials synthesis, and chemical transformation. In general, plasma-liquid processes are scientifically compelling because reactivity can be produced without a catalyst, in relatively inert molecules, such as air or nitrogen and liquid water, in their native states at ambient conditions. However, reactions at a plasma-liquid interface are extremely complex, occurring at a multiphase, gas-liquid boundary where excited or dissociate gaseous species dissolve and react with solution-phase species, and unique reaction pathways are induced by non-equilibrium chemistry. In particular, detailed knowledge of the physical and chemical processes, including what species are produced in the gas phase and how these species are subsequently transported across and react near the interfacial region, remains largely unanswered. In this project, modeling of the non-equilibrium reaction chemistry at the interface of low-temperature, atmospheric-pressure plasmas and liquid water is developed, supported by advanced laser diagnostics.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS1973

Low gravity reorientation in a scale-model Centaur liquid-hydrogen tank

An experiment was conducted to investigate the process of liquid reorientation from one end of a scale-model Centaur liquid-hydrogen tank to the other end by means of low-level accelerations. Prior to reorientation, the liquid was stabilized at the top of the tank at a Bond number of 15. Tanks both with and without ring baffles and with tank radii of 5.5 and 7.0 centimeters were used in the study. Reorientation acceleration values were varied to obtain Bond numbers of 200 and 450. Liquid fill levels of 20 and 70 percent were used. From the data in this study, relations were developed to estimate reorientation event times in unbaffled tanks through the point of final liquid clearing from the top of the tank. The insertion of ring baffles drastically changed the reorientation flow profiles but resulted in only minor differences in the times of tank-top uncovering and liquid collection.

Salzman, J. A.↗

NASA NTRS1974

Effect of gravity on liquid phase sintering

The unique conditions offered by the earth orbital environment in material processing involving both solid and liquid phases, such as liquid phase sintering, were studied. An experimental development program involving both test and theoretical work was initiated. Experimental work using material combinations selected such that maximum information about the effect of gravity can be derived has been conducted. Wetting of the solid phase by the liquid during sintering is an important phenomenon in liquid phase sintering, and gravity has influence on both capillary phenomenon and density segregation; hence, material combinations were selected such that these two effects can be suitably studies. The experimental work is meant to form the basis for similar comparative work done under low-g conditions. The part of the model dealing with the capillary phenomenon, as related to liquid phase sintering and the effect of gravity on it, suggest that gravity will have negligible effect on the Bond number and that the cohesive force is dependent on both the amount of liquid phase and the angle of contact.

Mookherji, T.↗

NASA NTRS1974

Evaluation of a Liquid Amine System for Spacecraft Carbon Dioxide Control

The analytical and experimental studies are described which were directed toward the acquisition of basic information on utilizing a liquid amine sorbent for in use in a CO2 removal system for manned spacecraft. Liquid amine systems are successfully used on submarines for control of CO2 generated by the crew, but liquid amines were not previously considered for spacecraft applications due to lack of development of satisfactory rotary phase separators. Developments in this area now make consideration of liquid amines practical for spacecraft system CO2 removal. The following major tasks were performed to evaluate liquid amine systems for spacecraft: (1) characterization, through testing, of the basic physical and thermodynamic properties of the amine solution; (2) determination of the dynamic characteristics of a cocurrent flow absorber; and (3) evaluation, synthesis, and selection of a liquid amine system concept oriented toward low power requirements. A low weight, low power system concept was developed. Numerical and graphical data are accompanied by pertinent observations.

Breaux, D. K.↗

NASA NTRS1975

Liquid jet pumped by rising gas bubbles

A two-phase mathematical model is proposed for calculating the induced turbulent vertical liquid flow. Bubbles provide a large buoyancy force and the associated drag on the liquid moves the liquid upward. The liquid pumped upward consists of the bubble wakes and the liquid brought into the jet region by turbulent entrainment. The expansion of the gas bubbles as they rise through the liquid is taken into account. The continuity and momentum equations are solved numerically for an axisymmetric air jet submerged in water. Water pumping rates are obtained as a function of air flow rate and depth of submergence. Comparisons are made with limited experimental information in the literature.

Hussain, N. A.↗

NASA NTRS1975

Analysis of liquid metal embrittlement from a bond energy viewpoint

Absorption induced embrittlement of solid metals by certain liquid metals is analyzed through an Engel-Brewer calculation of the solid-liquid interaction energy, and of the effect of the latter in reducing fracture surface energy. The reduction in fracture surface energy is estimated by comparison of the electronic contribution to the solid-liquid interaction energy with solid-solid bond energy for some 40 liquid-solid couples. Regular solution theory is used to estimate mutual solubility as the relative difference in parameter values. Embrittlement can be predicted by using reduction in fracture surface energy and solubility parameter difference as critical variables. The effect of solute additions to the liquid on the degree of embrittlement is interpreted via the same two variables; the principal effect of solutes is to modify solubility relationships at the solid-liquid interface.

Kelley, M. J.↗

NASA NTRS1978

Liquid propellant reorientation in a low-gravity environment

An existing empirical analysis relating to the reorientation of liquids in cylindrical tanks due to propulsive settling in a low gravity environment was extended to include the effects of geyser formation in the Weber number range from 4 to 10. Estimates of the minimum velocity increment required to be imposed on the propellant tank to achieve liquid reorientation were made. The resulting Bond numbers, based on tank radius, were found to be in the range from 3 to 5, depending upon the initial liquid fill level, with higher Bond number required for high initial fill levels. The resulting Weber numbers, based on tank radius and the velocity of the liquid leading edge, were calculated to be in the range from 6.5 to 8.5 for cylindrical tanks having a fineness ratio of 2.0, with Weber numbers of somewhat greater values for longer cylindrical tanks. It, therefore, appeared to be advantageous to allow small geysers to form and then dissipate into the surface of the collected liquid in order to achieve the minimum velocity increment. The Bond numbers which defined the separation between regions in which geyser formation did and did not occur due to propulsive settling in a spherical tank configuration ranged from 2 to 9 depending upon the liquid fill level.

Sumner, I. E.↗

NASA NTRS1979

Plagiogranites as late-stage immiscible liquids in ophiolite and mid-ocean ridge suites - An experimental study

A study of relationships between basic and acidic rocks was made by fractionating primitive basalt at low pressure anhydrous conditions at various fugacities. Fractionally crystallized basalt became increasingly enriched in iron which became silicate liquid immiscible, producing Fe-enriched basaltic and granitic liquids. The latter is similar to plagiogranites found in mid-oceanic rift (MOR) regions, showing that silicate liquid immiscibility could be the petrogenic process which produces plagiogranites in some MOR regions and ophiolites. The major problem in considering plagiogranites as products of silicate liquid immiscibility is absence of any description of the Fe-enriched conjugate liquid in the ophiolite or MOR literature, and the identification of this magma is essential for a definite case of silicate liquid immiscibility.

Dixon, S.↗

NASA NTRS1980

Transverse injection of a particle-laden liquid jet in supersonic flow: A three-phase flow

The results of a two part study of the behavior of particle laden liquid jets injected into air are presented. Water was used as the liquid carrier and either 1-37 or 13-44 microns diam. spherical glass beads with a specific gravity of 2.8-3.0 as the particles. The observations were mainly photographic. The breakup of jets injected into still air was investigated as a function of particle loading, and the results were compared to the pure liquid jet case. The jets were found to be more stable with particles present. The length to breakup was increased, and the formation of satellite droplets was suppressed. The penetration and breakup of transverse jets in a Mach 3.0 air stream was studied. The general breakup mechanism of wave formation was found to be the same as for the all liquid case. Significant separation of the phases was observed, and the penetration of the liquid phase was reduced compared to all liquid cases at the same value of the jet to free stream momentum flux ratio.

Schetz, J. A.↗

NASA NTRS1980

A mechanism for the compressive ignition of liquid monopropellants

Possible mechanisms for compressive ignition of liquid monopropellants are discussed. These mechanisms all involve the collapse of a gas filled bubble imbedded in the liquid. A model of the collapse of a gas bubble in an incompressible liquid and the combustion of the surrounding liquid after ignition occurs is presented. The effect of gas covolume, liquid density, the adiabatic exponent, rate of pressurization and prepressurization are investigated. Calculations for finite and infinite liquid volumes are also presented. Gas generation in the bubble is shown to have a significant effect on its evolution and the introduction of a surface enhancement factor leads to a runaway reaction. For the conditions considered, the reacting bubble oscillates at a frequency of about 35 kHz over the first 0.5 milliseconds. This frequency decreases as the surface enhancement factor is increased. The implication is that a one dimensional model of this process may be tractable from the standpoint of computer time.

Morrison, W. F.↗

NASA NTRS1952

The Calculated and Measured Performance Characteristics of a Heated-Wire Liquid-Water-Content Meter for Measuring Icing Severity

Ground tests have been made of an instrument which, when assembled in a more compact form for flight installation, could be used to obtain statistical flight data on the liquid-water content of icing clouds and to provide an indication of icing severity. The sensing element of the instrument consists of an electrically heated wire which is mounted in the air stream. The degree of cooling of the wire resulting from evaporation of the impinging water droplets is a measure. of the liquid-water content of the cloud. Determination of the value of the liquid-water content from the wire temperature at any instant requires a knowledge of the airspeed, altitude, and air temperature. An analysis was made of the temperature response of a heated wire exposed to an air stream containing water drops. Comparisons were made of the liquid-water content as measured with several heated wires and absorbent cylinders in an artificially produced cloud. For one of the wires, comparative tests were made with a rotating-disk icing-rate meter in an icing wind tunnel. From the test results, it was shown that an instrument for measuring the concentration of liquid water in an air stream can be built using an electrically heated wire of known temperatureresistance characteristics, and that the performance of such a device can be predicted using appropriate theory. Although an instrument in a form suitable for gathering statistical data in flight was not built, the practicability of constructing such an instrument was illustrated. The ground-test results indicated that a flight heated-wire instrument would be simple and durable, would respond rapidly to variations in liquid-water content, and could be used for the measurement of water content in clouds which are above freezing temperature, as well as in icing clouds.

Neel, Carr B.↗

NASA NTRS1982

Behavior of liquid hydrogen inside an ICF target

The configuration of liquid hydrogen inside spherical glass shell ICF target was studied both theoretically and experimentally. Because of the zero contact angle between the .D2 liquid and glass substrate and the limited wetting surface that is continuous, the liquid hydrogen completely covers the interior of the glass shell, resulting in the formation of a void at the center. For this reason, the present problem distinguishes itself from that for a sessile drop sitting on a flat surface. A theory was formulated to calculate the liquid hydrogen configuration by including the London-dispersion force between the liquid and the substrate molecules. The net result is an augmented Bashforth-Adams equation appropriate to a spherical substrate, which is considered to be the major contribution of the present work. Preliminary calculations indicate that this equation accurately models the liquid hydrogen behavior inside a spherical microshell.

Kim, K.↗

NASA NTRS1981

Calculations of the surface tensions of liquid metals

The understanding of the surface tension of liquid metals and alloys from as close to first principles as possible is discussed. The two ingredients which are combined in these calculations are: the electron theory of metals, and the classical theory of liquids, as worked out within the framework of statistical mechanics. The results are a new theory of surface tensions and surface density profiles from knowledge purely of the bulk properties of the coexisting liquid and vapor phases. It is found that the method works well for the pure liquid metals on which it was tested; work is extended to mixtures of liquid metals, interfaces between immiscible liquid metals, and to the temperature derivative of the surface tension.

Stroud, D. G.↗

NASA NTRS1983

Drop motion in a rotating immiscible liquid body

The interaction of liquids is an important part of many processes and is often used for such purposes as causing a separation of solution components by mass transfer between phases, allowing a chemical reaction between liquids or their components, providing direct contact heating or cooling, or creating emulsions. Containerless space processing may well involve the interaction of liquids in the form of drops. For example it may be desirable to form an alloy in space by merger of two or more drops. Encapsulation of a volatile liquid by a second less volatile and immiscible liquid might be a means for avoiding volatilization. Rotation of such systems would enhance mixing where desirable and/or provide means for drop management. In this study, single drop behavior in rotating liquid bodies is studied experimentally.

Annamalai, P.↗

NASA NTRS1982

Finite element analysis of the effect of a non-planar solid-liquid interface on the lateral solute segregation during unidirectional solidification

The effect of solid-liquid interface shape on lateral solute segregation during steady-state unidirectional solidification of a binary mixture is calculated under the assumption of no convection in the liquid. A finite element technique is employed to compute the concentration field in the liquid and the lateral segregation in the solid with a curved boundary between the liquid and solid phases. The computational model is constructed assuming knowledge of the solid-liquid interface shape; no attempt is made to relate this shape to the thermal field. The influence of interface curvature on the lateral compositional variation is investigated over a range of system parameters including diffusivity, growth speed, distribution coefficient, and geometric factors of the system. In the limiting case of a slightly nonplanar interface, numerical results from the finite element technique are in good agreement with the analytical solutions of Coriell and Sekerka obtained by using linear theory. For the general case of highly non-planar interface shapes, the linear theory fails and the concentration field in the liquid as well as the lateral solute segregation in the solid can be calculated by using the finite element method.

Carlson, F. M.↗

NASA NTRS1983

A helium-3 refrigerator employing capillary confinement of liquid cryogen

A condensation refrigerator suitable for operation in a zero gravity space environment was constructed. The condensed liquid refrigerant is confined by surface tension inside a porous metal matrix. Helium-4 and helium-3 gases were condensed and held in a copper matrix. Evaporative cooling of confined liquid helium-4 resulted in a temperature of 1.4K. Using a zeolite adsorption pump external to the cryostat, a temperature of 0.6 K was achieved through evaporative cooling of liquid helium-3. The amount of time required for complete evaporation of a controlled mass of liquid helium-4 contained in the copper matrix was measured as a function of the applied background power. For heating powers below 18 mW the measured times are consistent with the normal boiling of the confined volume of liquid refrigerant. At background powers above 18 mW the rapid rise in the temperature of the copper matrix the signature of the absence of confined liquid occurs in a time a factor of two shorter than that expected on the basis of an extrapolation of the low power data.

Ennis, D. J.↗

NASA NTRS1985

Research on solar pumped liquid lasers

A solar pumped liquid laser that can be scaled up to high power (10 mW CW) for space applications was developed. Liquid lasers have the advantage over gases in that they provide much higher lasant densities and thus high-power densities. Liquids also have advantages over solids in that they have much higher damage thresholds and are much cheaper to produce for large scale applications. Among the liquid laser media that are potential candidates for solar pumping, the POC13: Nd sup 3+:ZrC14 liquid was chosen for its high intrinsic efficiency and its relatively good stability against decomposition due to protic contamination. The development of a manufacturing procedure and performance testing of the laser, liquid and the development of an inexpensive large solar concentrator to pump the laser are examined.

Cox, J. D.↗

NASA NTRS1990

Liquid-Flow Controller With Trickle Preflow

Liquid-flow controller allows pressure in liquid to increase steeply with flow as flow starts, then provides more-gradual nearly linear rise of pressure with flow as flow and pressure increase beyond preset breakpoint. Controller alternative version of mechanism described in "Liquid-Flow Controller Responds To Pressure" (MFS-28329) and "Liquid-Flow Controller With Preset Break Pressure" (MFS-28330). Material cut out of cone at tip of pintle. Liquid always passes from shell, albeit at low rate. When pressure in shell great enough to force orifice away from pintle, liquid flows at greater rate.

Cox, George B., Jr.↗