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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRS2009

Modern Material Analysis Instruments Add a New Dimension to Materials Characterization and Failure Analysis

Modern analytical tools can yield invaluable results during materials characterization and failure analysis. Scanning electron microscopes (SEMs) provide significant analytical capabilities, including angstrom-level resolution. These systems can be equipped with a silicon drift detector (SDD) for very fast yet precise analytical mapping of phases, as well as electron back-scattered diffraction (EBSD) units to map grain orientations, chambers that admit large samples, variable pressure for wet samples, and quantitative analysis software to examine phases. Advanced solid-state electronics have also improved surface and bulk analysis instruments: Secondary ion mass spectroscopy (SIMS) can quantitatively determine and map light elements such as hydrogen, lithium, and boron - with their isotopes. Its high sensitivity detects impurities at parts per billion (ppb) levels. X-ray photo-electron spectroscopy (XPS) can determine oxidation states of elements, as well as identifying polymers and measuring film thicknesses on coated composites. This technique is also known as electron spectroscopy for chemical analysis (ESCA). Scanning Auger electron spectroscopy (SAM) combines surface sensitivity, spatial lateral resolution (10 nm), and depth profiling capabilities to describe elemental compositions of near and below surface regions down to the chemical state of an atom.

Panda, Binayak↗
NASA NTRS1992

Lunar Resources Using Moderate Spectral Resolution Visible and Near-infrared Spectroscopy: Al/si and Soil Maturity

Modern visible and near-infrared detectors are critically important for the accurate identification and relative abundance measurement of lunar minerals; however, even a very small number of well-placed visible and near-infrared bandpass channels provide a significant amount of general information about crucial lunar resources. The Galileo Solid State Imaging system (SSI) multispectral data are an important example of this. Al/Si and soil maturity will be discussed as examples of significant general lunar resource information that can be gleaned from moderate spectral resolution visible and near-infrared data with relative ease. Because quantitative-albedo data are necessary for these kinds of analyses, data such as those obtained by Galileo SSI are critical. SSI obtained synoptic digital multispectral image data for both the nearside and farside of the Moon during the first Galileo Earth-Moon encounter in December 1990. The data consist of images through seven filters with bandpasses ranging from 0.40 microns in the ultraviolet to 0.99 microns in the near-infrared. Although these data are of moderate spectral resolution, they still provide information for the following lunar resources: (1) titanium content of mature mare soils based upon the 0.40/0.56-micron (UV/VIS) ratio; (2) mafic mineral abundance based upon the 0.76/0.99-micron ratio; and (3) the maturity or exposure age of the soils based upon the 0.56-0.76-micron continuum and the 0.76/0.99-micron ratio. Within constraints, these moderate spectral resolution visible and near-infrared reflectance data can also provide elemental information such as Al/Si for mature highland soils.

Fischer, Erich M.↗
NASA NTRS1999

Fundamental Studies of Solidification in Microgravity Using Real-Time X-Ray Microscopy

This research applies a state of the art X-ray Transmission Microscope, XTM, to image (with resolutions up to 3 micrometers) the solidification of metallic or semiconductor alloys in real-time. We have successfully imaged in real-time: interfacial morphologies, phase growth, coalescence, incorporation of phases into the growing interface, and the solute boundary layer in the liquid at the solid-liquid interface. We have also measured true local growth rates and can evaluate segregation structures in the solid; a form of in-situ metallography. During this study, the growth of secondary phase fibers and lamellae from eutectic and monotectic alloys have been imaged during solidification, in real-time, for the first time in bulk metal alloys. Current high resolution X-ray sources and high contrast X-ray detectors have advanced to allow systematic study of solidification dynamics and the resulting microstructure. We have employed a state-of-the-art sub-micron source with acceleration voltages of 10-100 kV to image solidification of metals. One useful strength of the XTM stems from the manner an image is formed. The radiographic image is a shadow formed by x-ray photons that are not absorbed as they pass through the specimen. Composition gradients within the specimen cause variations in absorption of the flux such that the final image represents a spatial integral of composition (or thickness). The ability to image these features in real-time enables more fundamental and detailed understanding of solidification dynamics than has previously been possible. Hence, application of this technique towards microgravity experiments will allow rigorous testing of critical solidification models.

Curreri, Peter A.↗
NASA NTRS1998

Design and Performance of a Miniature Lidar Wind Profiler (MLWP)

The directional velocity of the wind is one of the most critical components for understanding meteorological and other dynamic atmospheric processes. Altitude-resolved wind velocity measurements, also known as wind profiles or soundings, are especially necessary for providing data for meteorological forecasting and overall global circulation models (GCM's). Wind profiler data are also critical in identifying possible dangerous weather conditions for aviation. Furthermore, a system has yet to be developed for wind profiling from the surface of Mars which could also meet the stringent requirements on size, weight, and power of such a mission. Obviously, a novel wind profiling approach based on small and efficient technology is required to meet these needs. A lidar system based on small and highly efficient semiconductor lasers is now feasible due to recent developments in the laser and detector technologies. The recent development of high detection efficiency (50%), silicon-based photon-counting detectors when combined with high laser pulse repetition rates and long receiver integration times has allowed these transmitter energies to be reduced to the order of microjoules per pulse. Aerosol lidar systems using this technique have been demonstrated for both Q-switched, diode-pumped solid-state laser transmitters (lambda = 523 nm) and semiconductor diode lasers (lambda = 830 nm); however, a wind profiling lidar based on this technique has yet to be developed. We will present an investigation of a semiconductor-laser-based lidar system which uses the "edge-filter" direct detection technique to infer Doppler frequency shifts of signals backscattered from aerosols in the planetary boundary layer (PBL). Our investigation will incorporate a novel semiconductor laser design which mitigates the deleterious effects of frequency chirp in pulsed diode lasers, a problem which has limited their use in such systems in the past. Our miniature lidar could be used on a future Mars lander and perhaps find its own niche in terrestrial applications due to its potential low cost an small size.

Cornwell, Donald M., Jr.↗
NASA NTRS1992

Theoretical simulation of a 2 micron airborne solid state laser anemometer

In the near future, military aircraft will need to know precisely their true airspeed in order to optimize flight conditions. In comparison with classical anemometer probes, an airborne Doppler lidar allows measurement of the air velocity without influence from aircraft aerodynamic disturbance. While several demonstration systems of heterodyne detection using a CO2 laser have been reported, improvements in the technology of solid state lasers have recently opened up the possibility that these devices can be used as an alternative to CO2 laser systems. In particular, a diode pumped Tm:Ho:YAG laser allows a reliable compact airborne system with an eye safe wavelength (lambda = 2.09 microns) to be achieved. The theoretical study of performances of a coherent lidar using a solid state diode pumped Tm:Ho:YAG laser, caled SALSA, for measuring aircraft airspeed relative to atmospheric aerosols is described. A computer simulation was developed in order to modelize the Doppler anemometer in the function of atmospheric propagation and optical design. A clever analysis of the power budget on the detector area allows optical characteristic parameters of the system to be calculated, and then it can be used to predict performances of the Doppler system. Estimating signal to noise ratios (SNR) and heterodyne efficiency provides the available energy of speed measurement as well as a useful measurement of the alignment of the backscattered and reference fields on the detector.

Imbert, Beatrice↗
NASA NTRS2013

Laboratory Instruments Available to Support Space Station Researchers at Marshall Space Flight Center

A number of research instruments are available at NASA's Marshall Space Flight Center (MSFC) to support ISS researchers and their investigations. These modern analytical tools yield valuable and sometimes new informative resulting from sample characterization. Instruments include modern scanning electron microscopes equipped with field emission guns providing analytical capabilities that include angstron-level image resolution of dry, wet and biological samples. These microscopes are also equipped with silicon drift X-ray detectors (SDD) for fast yet precise analytical mapping of phases, as well as electron back-scattered diffraction (EBSD) units to map grain orientations in crystalline alloys. Sample chambers admit large samples, provide variable pressures for wet samples, and quantitative analysis software to determine phase relations. Advances in solid-state electronics have also facilitated improvements for surface chemical analysis that are successfully employed to analyze metallic materials and alloys, ceramics, slags, and organic polymers. Another analytical capability at MSFC is a mganetic sector Secondary Ion Mass Spectroscopy (SIMS) that quantitatively determines and maps light elements such as hydrogen, lithium, and boron along with their isotopes, identifies and quantifies very low level impurities even at parts per billion (ppb) levels. Still other methods available at MSFC include X-ray photo-electron spectroscopy (XPS) that can determine oxidation states of elements as well as identify polymers and measure film thicknesses on coated materials, Scanning Auger electron spectroscopy (SAM) which combines surface sensitivity, spatial lateral resolution (approximately 20 nm), and depth profiling capabilities to describe elemental compositions in near surface regions and even the chemical state of analyzed atoms. Conventional Transmission Electron Microscope (TEM) for observing internal microstructures at very high magnifications and the Electron Probe Micro-analyzer (EPMA) for very precise microanalysis are available as needed by the researcher. Space Station researchers are invited to work with MSFC in analyzing their samples using these techniques.

Panda, Binayak↗
NASA NTRS1985

Lightning mapper and the future

A trade-off analysis was completed that reveals how the lightning mapper detection efficiency will change as a function of interference filter bandwidth, pixel field of view, and telescope aperture. It is shown that the critical parameter on which we have minimum flexibility is filter band-width. The problem is that too narrow a filter bandwidth is incompatible with wide areal coverage. The trade-off analysis demonstrates that an 80 percent lightning detection efficiency will technically be relatively straight-forward, while a 90 percent detection efficiency will apparently be difficult to achieve. Three focal plane designs are currently under consideration. One would use a single large, solid state silicon integrating array with multiple output channels and off-the-focal-plane analog, time domain, background removing fibers. A second design would use the same technology, but the sensor would consist of up to four virtually independent focal plane arrays. This design reduces the areal coverage of each detector. Thus narrower interference filters could be utilized. Superior performance would be realized at a probable increase in cost. The final design would use a three-dimensional focal plane in order to perform background removal at the focal plane. Superior performance would be achieved along with reduced weight and power requirements. Unfortunately, this focal plane technology is still under development.

Christian, H. J.↗
NASA NTRS1988

Imaging spectroscopy II; Proceedings of the Meeting, San Diego, CA, Aug. 20, 21, 1987

The conference presents papers on airborne imaging spectrometers, imaging spectrometry analysis, and spaceborne imaging spectrometers. Consideration is given to an imaging spectrometer for ocean and land remote sensing, an advanced solid-state array spectroradiometer, airborne visible/infrared imaging spectrometer design and performance, and a signal chain for the airborne visible/infrared imaging spectrometer. Other topics include imaging spectrometry as a tool for botanical mapping, the estimation of forest canopy characteristics and nitrogen cycling using lasing spectrometry, and a continuous readout photon counting imaging detector.

Vane, Gregg↗
NASA NTRS1988

Focal plane array technologies for NASA space systems

A development status evaluation is presented for solid-state self-scanned imaging arrays applicable to NASA space science missions, giving attention to the visible and IR spectral range (0.5-1000 microns). Shortward of 1.1 micron, Si CCDs will continue to be used. Beyond 10 microns, the challenge for NASA researchers lies in the development of a class of detectors that can dispense with the conventional cooling to below 10 K. Above 25 microns, extrinsic Ge detectors will be used, and beyond 200 microns, a novel extrinsic material such as GaAs will have to be developed for this application.

Cutts, James A.↗
NASA NTRS1998

No Moving Parts

Under a NASA SBIR (Small Business Innovative Research), Research International developed the solid state micromachined pump used for cooling electronics in space, circulation of heat transfer fluids on spacecraft, and monitoring fire and gas hazards aboard naval warships. Incorporating Lewis Research Center's pumping technology, commercial applications for this product include both detection of toxins and pollutants in coal mines, and early warning smoke detectors for industrial applications.

Source record↗
NASA NTRS1978

The application of smart sensor techniques to a solid-state array multispectral sensor

The solid-state array spectroradiometer (SAS) developed at JSC for remote sensing applications is a multispectral sensor which has no moving parts, is virtually maintenance-free, and has the ability to provide data which requires a minimum of processing. The instrument is based on the 42 x 342 element charge injection device (CID) detector. This system allows the combination of spectral scanning and across-track spatial scanning along with its associated digitization electronics into a single detector.

Mcfadin, L. W.↗
NASA NTRS1982

An automated mapping satellite system

Topographic maps are compiled by manually operated stereoplotters that recreate the geometry of two wide-angle overlapping stereo frame photographs. Continuous imaging systems such as strip cameras, electro-optical scanners, or linear arrays of detectors (push brooms) can also create stereo coverage from which topography can be compiled; however, the instability of an aircraft in the atmosphere makes this approach impractical. The benign environment of space permits a satellite to orbit the Earth with very high stability as long as no local perturbing forces are involved. Solid-state linear-array sensors have no moving parts and create no perturbing force on the satellite. Digital data from highly stabilized stereo linear arrays are amenable to simplified processing to produce both planimetric imagery and elevation data. A proposed satellite, called MAPSAT, could accomplish automated mapping in near real time. Image maps as large as 1:50,000 scale with contours as close as 20-m interval may be produced from MAPSAT data.

Colvocoreses, A. P.↗
NASA NTRS1972

Experimental determination of cosmic ray charged particle intensity profiles in the atmosphere

Absolute cosmic-ray free air ionization and charged particle fluxes and dose rates throughout the atmosphere were measured on a series of balloon flights that commenced in 1968. Argon-filled ionization chambers equipped with solid-state electrometers, with different gas pressures and steel wall thicknesses, and a pair of aluminum-wall Gm counters have provided the basic data. These data are supplemented by measurements with air-filled and tissue equivalent ionization chambers and a scintillation spectrometer. Laboratory experiments together with analyses of the theoretical aspects of the detector responses to cosmic radiation indicate that these profiles can be determined to an overall accuracy of + or - 5 percent.

Lowder, W. M.↗
NASA NTRS1980

X-ray spectroscopy of supernova remnants

The information which can be obtained from X-ray spectroscopy of supernova remnants is considerd. The fitting of X-ray detector counts to models of the incident spectrum is discussed, and the types of thermal emission models generally employed are presented, including the power law, black body, and thermal bremsstrahlung models of the continua and models of the emission of a hot, optically thin plasma in collisional equilibrium. Observations of 12 supernova remnants made with the Solid State Spectrometer on board the Einstein Observatory are reported, and metal abundances inferred from the lines of the eight remnants showing thermal spectra are summarized. Questions raised by the failure to observe the overabundance of Fe predicted by stellar evolution and hydrodynamic modeling are discussed, and the need to develop more detailed models of the conditions in a supernova remnant in order to interpret the X-ray spectra is noted.

Szymkowiak, A. E.↗
NASA NTRS1999

Temperature Control of Avalanche Photodiode Using Thermoelectric Cooler

Avalanche photodiodes (APDS) are quantum optical detectors that are used for visible and near infrared optical detection applications. Although APDs are compact, rugged, and have an internal gain mechanism that is suitable for low light intensity; their responsivity, and therefore their output, is strongly dependent on the device temperature. Thermoelectric coolers (TEC) offers a suitable solution to this problem. A TEC is a solid state cooling device, which can be controlled by changing its current. TECs are compact and rugged, and they can precisely control the temperature to within 0.1 C with more than a 150 C temperature gradient between its surfaces. In this Memorandum, a proportional integral (PI) temperature controller for APDs using a TEC is discussed. The controller is compact and can successfully cool the APD to almost 0 C in an ambient temperature environment of up to 27 C.

Refaat, Tamer F.↗
NASA NTRS2001

Continuous Magnetic Refrigerators for Cooling in the 0.05 to 10 K Range

Low temperature refrigeration is an increasingly vital technology for NASA's Space Science program since most detectors being developed for x-ray, IR and sub-millimeter missions must be cooled to below 100 mK in order to meet the requirements for energy and spatial resolution. For space applications, magnetic refrigeration has an inherent advantage over alternative techniques because it does not depend on gravity. Adiabatic demagnetization refrigerators, or ADRs, are relatively simple, solid state devices. The basic elements are a magnetocaloric refrigerant (usually an encapsulated paramagnetic salt) located in the bore of a superconducting magnet, and a heat switch linking the salt to a heat sink. The alignment of magnetic spins with the magnetic field causes the refrigerant to warm as the magnetic field increases and cool as the field decreases. Thus the simple process of magnetizing the refrigerant to high field with the heat switch closed, then demagnetizing it with the heat switch open allows one to obtain temperatures well below 100 mK using a heat sink as warm as 4.2 K. The refrigerant can maintain a low temperature for a length of time depending on the applied and parasitic heat loads, its mass, and the initial magnetic field strength. Typically ADRs are designed for 12-24 hours of hold time, after which they must be warmed up and recycled.

Shirron, Peter↗
NASA NTRS2003

Continuous Magnetic Refrigerators for Cooling in the 0.05 to 10 K Range: Progress and Future Development

Low temperature refrigeration is an increasingly vital technology for NASA s Space Science program since most detectors being developed for x-ray, IR and sub-millimeter missions must be cooled to below 100 mK in order to meet the requirements for energy and spatial resolution. For space applications, magnetic refrigeration has an inherent advantage over alternative techniques because it does not depend on gravity. Adiabatic demagnetization refrigerators, or ADRs, are relatively simple, solid state devices. The basic elements are a magnetocaloric refrigerant (usually an encapsulated paramagnetic salt) located in the bore of a superconducting magne$, and a heat switch linking the salt to a heat sink. The alignment of magnetic spins with the magnetic field causes the refrigerant to warm as the magnetic field increases and cool as the field decreases. Thus the simple process of magnetizing the refrigerant to high field with the heat switch closed, then demagnetizing it with the heat switch open allows one to obtain temperatures well below 100 mK using a heat sink as warm as 4.2 K. The refrigerant can maintain a low temperature for a length of time depending on the applied and parasitic heat loads, its mass, and the initial magnetic field strength. Typically ADRs are designed for 12-24 hours of hold time, after which they must be warmed up and recycled. The drawback to single-shot ADRs is that the cooling power per unit mass is relatively low. Refrigerants that are suitable for low temperature operation necessarily have low magnetic ion density, and therefore low entropy density. Since ADRs store entropy, systems with even modest cooling powers (a few microwatts) at temperatures below 100 mK tend to be massive, averaging 10-15 kg.

Shirron, Peter↗