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DOE OSTI2022

Temperature distribution in a laser-heated diamond anvil cell as described by finite element analysis

Finite element analysis (FEA) is a powerful tool for numerically solving partial differential equations over complex geometries and is thus useful for analyzing heat transport in laser-heated diamond anvil cell (LHDAC) experiments. Our models expand on previously published simulations by calculating the volume-averaged temperatures of both the sample and insulation/pressure media under steady-state heating to determine the thermal pressure of the hot sample. Our goal is to produce an accurate relationship between the measured surface temperature of the absorbing sample and the temperature of the transparent insulating media, which is used to determine thermal pressure but susceptible to steep temperature gradients. We find that in doing so, our FEA models of temperature within the pressure/insulation media can differ from simplified estimates of temperature gradients by more than a factor of 2. We also explore temperature-dependent and temperature-independent thermal conductivity models and find that the volume-averaged temperatures differ by up to a factor of 1.3, forcing the predicted thermal pressures determined to also differ by up to a factor of 1.5 at a temperature of 2000 K at 50 GPa for neon. Higher temperatures exacerbate this difference. We also find that unintentional asymmetric sample insertion and sample heating, which are common in LHDAC experiments, do not have a first-order effect on volume-averaged temperatures. The FEA models, available in both Python and FlexPDE, are versatile across different sample geometries, materials, and heat source laser shapes.

Farah, Frederick↗

DOE OSTI2024

Dependence of Uranium Oxide Polymorphism on Plasma Synthesis Conditions

Here, we synthesized uranium oxide nanoparticles using a plasma flow reactor (PFR) and studied the effects of three different experimental parameters on the resulting morphologies and speciation of the particles: (1) collection duration, (2) collection substrate temperature, and (3) radial collection position due to radial temperature gradients in the PFR. We also induced three distinct temperature histories along the axis of the plasma flow reactor by varying the gas flow rates downstream of the plasma torch. Transmission electron microscopy (TEM) analyses of collected particles showed two phases of uranium oxides (fcc-UO 2 and α-UO 3 ). The chemical compositions of the resulting uranium oxide particles were not altered by the three parameters investigated in this work but varied based on the temperature history induced. Preheating of the collection substrate led to deposition of fewer particles, which is attributed to a reduction in thermophoretic force caused by the reduced temperature gradient for preheated substrates. The relative amounts of UO 2 to UO 3 and particle size varied depending on the cooling history employed during synthesis.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

NASA NTRS1982

Tube-Furnace Production of Silicon

Packed-bed reactor produces silicon by decomposing ultrapure silane gas in temperature gradient. Based on previous experiments with relatively low decomposition temperatures and with temperature gradients, heterogeneous decomposition will produce few fines. Fines produced are screened out and reinserted into furnace.

Farrier, E. G.↗

NASA NTRS1986

Cellular solidification of transparent monotectics

Understanding how liquid phase particles are engulfed or pushed during freezing of a monotectic is addressed. The additional complication is that the solid-liquid interface is nonplanar due to constitutional undercooling. Some evidence of particle pushing where the particles are the liquid phase of the montectic was already observed. Cellular freezing of the succinonitrile-glycerol system also occurred. Only a few compositions were tested at that time. The starting materials were not especially pure so that cellular interface observed was likely due to the presence of unkown impurities, the major portion of which was water. Topics addressed include: the effort of modeling the particle pushing process using the computer, establishing an apparatus for the determination of phase diagrams, and the measurement of the temperature gradients with a specimen which will solidify on the temperature gradient microscope stage.

Kaulker, W. F.↗

DOE OSTI2022

[Presentation Slides] Code-to-Code Benchmark Study for Thermal Stress Modeling and Preliminary Analysis of the High-temperature Single Heat-Pipe Experiment

In the heat-pipe-cooled microreactor, heat pipes remove heat from the reactor core as a passive heat-transfer device, so the fluid circulation is not required for cooling, which can substantially simplify the overall reactor design. However, given the extremely high temperatures in the core region and potentially large temperature gradients across the structure materials, thermal stresses need to be well-analyzed to ensure structural integrity during normal operations and accident scenarios. This presentation slides discuss finite element method-based thermal-stress analysis for the high-temperature single heat-pipe test article in the Single Primary Heat Extraction and Removal Emulator (SPHERE) facility at Idaho National Laboratory (INL), using two commercial software packages, Abaqus and Star-CCM+. A code-to-code benchmark study was performed to crosscheck the model setup and capability of each code and to gain preliminary insights into the potential thermal stress concerns from the current experimental setup. It is observed the significant thermal stresses happen at the inner surface of the heat pipe hole surrounded by electric heaters where the largest temperature gradients appear. The temperature fields have good agreements between Abaqus and Star-CCM+, while the induced thermal stresses show modest deviations probably due to differences of meshing engines used in these two codes. It is found that the local maximum thermal stresses may reach close to the ultimate tensile strength and yield strength of structural material depending on the heater power. Ultimately, the coupled thermal-structural analysis will help guide the current experimental plan and ensure the facility safety for future experimental study.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

NASA NTRS1985

Advanced Containerless Processing Technology

Breadboards for high temperature containerless processing systems are to be developed, the principles of operation are to be studied, the performance is to be characterized, the limitations identified, and the influence of the acoustic field on the samples established. The subjects to be addressed are experimental and theoretical studies of: (1) acoustic positioning and manipulation capabilities in a high temperature gradient environment (from 26 C to 990 C); (2) acoustic waveforms, harmonic contents, power transfer, sample transport and stability associated with high temperature gradient system; (3) high temperature ground based levitation systems which will allow melting, processing, and solidifying samples without crucibles in the laboratory, (4) KC-135 and laboratory tests of various acoustic geometries which may have spherical applications in the Materials Processing in Space Program; and (5) provide technical information to Acoustics Containerless Experimental System (ACES) engineering team and establish the operation conditions for ACES.

Wang, T. G.↗

DOE OSTI2018

Thermometry of an open spatially inhomogeneous flame by diode laser absorption spectroscopy

Features of a single-beam variant of diode laser absorption spectroscopy (DLAS) used for temperature measurements in a spatially inhomogeneous hot zone are studied. A flame temperature of a commercial burner is measured by using water molecule absorption lines. The flame is probed by a diode laser radiation at various heights and in various directions. The correctness of DLAS measurement results is verified by comparing DLAS data with temperatures measured by the method of coherent anti-Stokes scattering (CARS). It is shown that in homogeneous flame domains the temperatures obtained by both the methods coincide. Temperature inhomogeneity along the probe beam direction is a principal problem of DLAS, in which case the method yields information about some effective temperature along the light trace. The difference in data obtained by DLAS and CARS is estimated. In probing traces with temperature gradients the difference reaches 700 K. Possibilities of accounting for temperature inhomogeneities along the trace in DLAS measurements are discussed. A method of differential spectra is suggested, which in certain conditions can provide substantially better coincidence of results for the two methods. (laser spectroscopy)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2024

Flow-shear destabilization of multiscale electron turbulence

The impact of sheared ${\mathbf{E} \hskip -1pt \times \hskip -1pt \mathbf{B}}$ flow on multiscale turbulence is studied with nonlinear gyrokinetic simulations. Simulations are based on DIII-D-like, high-confinement mode (H-mode) pedestal parameters in the regime of low ion temperature gradient drive, where there is a broad spectrum of electron temperature gradient (ETG)-driven turbulence. It is found that ${\mathbf{E} \hskip -1pt \times \hskip -1pt \mathbf{B}}$ shear can have a significant effect on ETG-driven electron transport, with an unexpected transition from a turbulence stabilization regime at moderate to large shearing rates $γ_E$ to a novel turbulence destabilization regime at low levels of $γ_E$. In the turbulence stabilization regime, the electron energy flux decreases monotonically with $γ_E$, even when $γ_E$ is small compared to electron mode growth rates. The stabilizing effect comes dominantly from the electron, not ion, gyrokinetic equation. In the novel destabilization regime, reduction of zonal energy results from the interaction of $γ_E$-modulated nonlinear drive in the zonal ion gyrokinetic equation, increasing the electron transport over a broad range of shearing rates. Finally, neither of these effects has been observed in previous electron-scale simulations.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS2000

A Dynamical Model for The Jupiter Thermocline

A new conceptual model for the observed banded wind structure of the giant outer planets is proposed, assuming a smoothly distributed potential vorticity (PV) atop a layer of deeply seated, latitudinally variable stratification. With a vanishing horizontal entropy contrast presumably enforced at the bottom of the flow layer by the underlying convection, the thermal-wind balance of observed cloud-top motions implies a mapping of constant potential temperature surfaces, nearly vertical at upper tropospheric levels, down to a deeper, flatter, but variably sloped 'thermocline.' For a generally colder-poleward distribution of isentropes consistent with the strong equatorial jets of both Jupiter and Saturn, this kind of mapping would also imply a poleward decreasing static stability. The proposed temperature-stability distribution is just the reverse of the Earth's troposphere, where the strongest latitudinal potential temperature gradients are at the bottom instead of the top, with static stability generally increasing toward the pole. The warmer-stabler correlation for Jupiter would be consistent, however, with a nearly monotonic distribution of PV from low to high latitudes, over planetary scales for which the planetary vorticity dominates the relative vorticity of the jets. In this way efficient PV mixing for the isentropically bounded thermocline can account for the dynamical maintenance of the cyclonic flanks of the equatorial jet. Over latitudinal intervals comparable to the internal deformation scale, however, the gradient of the absolute vorticity is dominated by the flow curvature, with the local latitudinal gradient of the static stability proportional to the local potential temperature gradient and therefore the local variation in geostrophic velocity. The resulting correlation of velocities and vorticity gradients implies an alternation of the flow over the internal deformation radius set by the vertical entropy contrast.

Allison, Michael↗

NASA NTRS1990

Status of structural analysis of 30 cm diameter ion optics

Three structural finite element programs are compared with theory, experimental data, and each other to evaluate their usefulness for modeling the thermomechanical deflection of ion engine electrodes. Two programs, NASTRAN and MARC, used a Cray XMP and the third, Algor, used an IBM compatible personal computer. The shape of the applied temperature gradient greatly affects off-axis displacement, implying that an accurate temperature distribution is required to analyze new designs. The use of bulk material constants to model the perforated electrodes was investigated. The stress and displacement predictions are shown to be sensitive to the temperature gradient and the Young's modulus, and insensitive to number of nodes, above some minimum value, and the Poisson ratio used. The models are shown to be useful tools for evaluating designs. Experimental measurement of temperatures and displacements was identified as the most critical area for further work.

Macrae, Gregory S.↗

NASA NTRS1990

Status of structural analysis of 30 cm diameter ion optics

Three structural finite element programs are compared with theory, experimental data, and each other to evaluate their usefulness for modeling the thermomechanical deflection of ion engine electrodes. Two programs, NASTRAN and MARC, used a Cray XMP and the third, Algor, used an IBM compatible personal computer. The shape of the applied temperature gradient greatly affects off-axis displacement, implying that an accurate temperature distribution is required to analyze new designs. The use of bulk material constants to model the perforated electrodes was investigated. The stress and displacement predictions are shown to be sensitive to the temperature gradient and the Young's modulus, and insensitive to number of nodes, above some minimum value, and the Poisson ratio used. The models are shown to be useful tools for evaluating designs. Experimental measurements of temperatures and displacements was identified as the most critical area.

Macrae, Gregory S.↗

NASA NTRS1984

Linear models of acoustic waves in sunspot umbrae

The two-dimensional, linear hydrodynamics of quiet solar and umbral model atmospheres in a plane-parallel, adiabatic approximation are investigated. The 5.5-8.5 mHz oscillations observed in umbral chromospheres and transition regions are interpreted as acoustic waves propagating parallel, or nearly parallel, to the temperature gradient. These waves are not totally internally reflected by the steep temperature gradient and, thus, are not trapped. Partial reflections, however, are effective in modulating the transmission as a function of frequency. The resonant transmission mechanism of Zugzda, Locans, and Staude (1983) is found to produce a spectrum of resonances in the transmission of acoustic waves in any atmosphere with a temperature minimum. Since the observed umbral oscillations display power in only a narrow range of frequencies, characteristics of the umbral models, wave propagation, and observations that would tend to suppress the higher frequency resonances are examined.

Gurman, J. B.↗

DOE OSTI2019

Vectoring into Potential Blind Geothermal Systems in the Granite Springs Valley Area, Western Nevada: Application of the Play Fairway Analysis at Multiple Scales

The Great Basin region of the western USA is capable of generating much greater amounts of geothermal energy than currently produced. Most geothermal resources in this region are blind, and thus the favorable characteristics for geothermal activity must be synthesized and methodologies developed to discover new commercial-grade systems. The geothermal play fairway concept involves integration of multiple parameters indicative of geothermal activity as a means of identifying promising areas for new development. In the Nevada play fairway project, nine geologic, geochemical, and geophysical parameters were initially synthesized to produce a new geothermal potential map of 96,000 km2. Granite Springs Valley in western Nevada is a particularly promising site selected for detailed study. It contains several favorable structural settings, including terminations of major Quaternary normal faults and fault intersections. Geologic, geophysical, and geochemical techniques were employed to define the most likely sites for high permeability and select drilling targets for temperature-gradient holes. Local and intermediate permeability models were revised to reflect results of detailed analyses and generate new detailed play fairway maps of the area. The most promising site lies in the northeastern part of the basin directly east of Adobe Flat, where the horse-tailing termination of a major normal fault (as revealed by new gravity data), opaline sinter deposits, warm shallow wells, and a low-resistivity anomaly are collocated. Geothermometry suggests a blind system with temperatures as high as ~130°C in this area. Four new temperature-gradient holes document temperatures of ~80°C at ~150 m depth. Lessons learned in the detailed studies of this project include: 1) initially identified sites commonly include multiple favorable settings at a finer scale; 2) promising sites in Cenozoic basins cannot be well defined without detailed geophysical surveys; and 3) play fairway analysis is critical at multiple scales, providing a means to select regional prospects as well as vectoring into drilling targets at individual sites.

15 GEOTHERMAL ENERGY↗

DOE OSTI2023

Electrostatic turbulence in EAST plasmas with internal transport barrier

Based on first-principles nonlinear gyrokinetic simulations, the electrostatic turbulence properties in the internal transport barrier (ITB) region of an Experimental Advanced Superconducting Tokamak discharge (#93890) are investigated. Specifically, ITBs with steep density and temperature gradients are located in the weakly negative magnetic shear region at the plasma center. In the linear stage, the growth rate and frequency of the ion temperature gradient (ITG) mode increase significantly due to resonant excitation by trapped electrons. That is, the resonance between trapped electrons and the ITG becomes strong due to the precession drift reversal of trapped electrons by the negative magnetic shear and Shafranov shift. Meanwhile, the trapped electron mode is stable in the ITB region due to only a very small fraction of electrons precessing in the direction of the electron diamagnetic drift. Nonlinear simulations show that, after considering the non-adiabatic effect of trapped electrons, the heat conductivity of ions and the turbulence intensity increase by at least a factor of 7 compared with the results only considering the adiabatic effect of electrons. The zonal charge density of trapped electrons can partially cancel that of ions, which weakens the intensity of the zonal flow, and consequently reduces the zonal flow regulation and enhances the turbulent transport.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS2010

Development and Acceptance Testing of the Dual Wheel Mechanism for the Tunable Filter Imager Cryogenic Instrument on the JWST

The James Webb Space Telescope (JWST) will carry four scientific instruments, one of which is the Tunable Filter Imager (TFI), which is an instrument within the Fine Guidance Sensor. The Dual Wheel (DW) mechanism is being designed, built and tested by COM DEV Ltd. under contract from the Canadian Space Agency. The DW mechanism includes a pupil wheel (PW) holding seven coronagraphic masks and two calibration elements and a filter wheel (FW) holding nine blocking filters. The DW mechanism must operate at both room temperature and at 35K. Successful operation at 35K comprises positioning each optical element with the required repeatability, for several thousand occasions over the five year mission. The paper discusses the results of testing geared motors and bearings at the cryogenic temperature. In particular bearing retainer design and PGM-HT material, the effects of temperature gradients across bearings and the problems associated with cooling mechanisms down to cryogenic temperatures. The results of additional bearing tests are described that were employed to investigate an abnormally high initial torque experienced at cryogenic temperatures. The findings of these tests, was that the bearing retainer and the ball/race system could be adversely affected by the large temperature change from room temperature to cryogenic temperature and also the temperature gradient across the bearing. The DW mechanism is now performing successfully at both room temperature and at cryogenic temperature. The life testing of the mechanism is expected to be completed in the first quarter of 2010.

Leckie, Martin↗

NASA NTRS1985

Differential photometry of magnetic faculae

New observations extending the differential continuum photometry technique to the near-infrared are presented which demonstrate that the main factor determining the facular visibility near the solar disk center is the difference in H(-) opacity (and thus in penetration depth) between the continuum passbands. It is shown how the difference signal obtained depends on the temperature gradient difference between the two faculae and photosphere. The measured facular temperature gradient is compared with that given by empirical facular models based on Fraunhofer line observations, and with theoretical predictions. An explanation for the enhanced visibility of faculae against granular noise in the difference signal is suggested.

Foukal, P.↗

NASA NTRS1988

Effect of vertical magnetic field on convection and segregation in vertical Bridgman crystal growth

A previous finite-element analysis of vertical Bridgman growth for dilute and nondilute alloys is extended to include the effect of a vertically-aligned magnetic field in the limit of zero magnetic Reynolds number. Calculations are presented for growth of a dilute gallium-germanium alloy in a vertically stabilized Bridgman-Stockbarger system and in a furnace with a uniform temperature gradient imposed along the ampoule. Steady cellular convection driven by radial temperature gradients causes good axial and radial mixing in both systems without a magnetic field. A weak magnetic field decreases the intensity of convection and the effectiveness of solute mixing. The radial nonuniformity is greatest for an intermediate field strength. Stronger fields suppress flow recirculation completely, and lead to uniform solute segregation across the crystal and to diffusion-controlled axial segregation.

Kim, Do Hyun↗

NASA NTRS1974

Geophysical, geochemical, and geological investigations of the Dunes geothermal system, Imperial Valley, California

The Dunes anomaly is a water-dominated geothermal system in the alluvium of the Salton Trough, lacking any surface expression. It was discovered by shallow-temperature gradient measurements. A 612-meter-deep test well encountered several temperature-gradient reversals, with a maximum of 105 C at 114 meters. The program involves surface geophysics, including electrical, gravity, and seismic methods, down-hole geophysics and petrophysics of core samples, isotopic and chemical studies of water samples, and petrological and geochemical studies of the cores and cuttings. The aim is (1) to determine the source and temperature history of the brines, (2) to understand the interaction between the brines and rocks, and (3) to determine the areal extent, nature, origin, and history of the geothermal system. These studies are designed to provide better definition of exploration targets for hidden geothermal anomalies and to contribute to improved techniques of exploration and resource assessment.

Elders, W. A.↗