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At least 361 records · Page 20

Enhancement of superplastic formability in a high strength aluminum alloy

A 7475 aluminum alloy was developed for superplastic forming (SPF). By lowering the Fe and Si contents in this alloy significantly below their normal levels and optimizing the thermomechanical processing to produce sheet, over 2000 percent thickness strain to failure was obtained. The microstructure, elevated-temperature uniaxial and biaxial tension, and cavitation behavior of the alloy were determined. In addition, a constitutive model was used to form a generic structural shape from which mechanical test specimens were removed and post-SPF characteristics were evaluated. The constitutive model included both material strain hardening and strain rate hardening effects, and was verified by accurately predicting forming cycles which resulted in successful component forming. Stress-life fatigue, stress rupture, and room and elevated temperature tensile tests were conducted on the formed material.

Agrawal, S. P.↗

Heat treatment study of the SiC/Ti-15-3 composite system

The oxidation and aging behaviors of a continuous fiber SiC/Ti-15V-3Cr-3Sn-3Al composite (SiC/Ti-15-3) were investigated. The aging characteristic of the composite were compared with those of the unreinforced Ti-15-3 matrix material, which was processed in the same manner as the composite. Various age hardened conditions of both the unreinforced matrix and the composite were evaluated by using optical microscopy, hardness measurements, and room temperature tensile tests (unreinforced matrix only). The Ti-15-3 material formed a thick surface oxide at temperature at or above 550 C when heat treated in air. The in situ composite matrix was softer than the unreinforced matrix for equivalent aging conditions. Both materials hardened to a maximum, then softened during overaging. The temperature at which peak aging occurred was approx. 450 C for both the in situ composite matrix and the unreinforced matrix. The room temperature elastic modulus and ultimate tensile strength of the unreinforced matrix varied as a function of aging treatment and paralleled the hardness behavior. The modulus and tensile strength showed little response to aging up to temperatures of 300 C; however, these properties increased after aging at 550 C. Aging at temperatures above 550 C resulted in a decrease in the modulus and tensile strength. The failure strain was a function of the precipitation state and of the amount of oxidation resulting from the heat treatment. Aging in air at the higher temperatures (greater than 550 C) caused the formation of a thick oxide layer and reduced the ductility. Aging in vacuum at these temperatures resulted in significantly higher ductilities. Long term exposures at 700 C caused the formation of a large grain boundary alpha-phase which reduced the ductility, even though the specimens were heat treated in vacuum.

Lerch, Bradley A.↗

Thermomechanical deformation testing and modeling in the presence of metallurgical instabilities

A number of viscoplastic constitutive models were developed to describe deformation behavior under complex combinations of thermal and mechanical loading. Questions remain, however, regarding the validity of procedures used to characterize these models for specific structural alloys. One area of concern is that the majority of experimental data available for this purpose are determined under isothermal conditions. This experimental study is aimed at determining whether viscoplastic constitutive theories characterized using an isothermal data base can adequately model material response under the complex thermomechanical loading conditions typical of power generation service. The approach adopted was to conduct a series of carefully controlled thermomechanical experiments on a nickel-based superalloy, Hastelloy Alloy X. Previous investigations had shown that this material experiences metallurgical instabilities leading to complex hardening behavior, termed dynamic strain aging. Investigating this phenomenon under full thermomechanical conditions leads to a number of challenging experimental difficulties which up to the present work were unresolved. To correct this situation, a number of advances were made in thermomechanical testing techniques. Advanced methods for dynamic temperature gradient control, phasing control and thermal strain compensation were developed and incorporated into real time test control software. These advances allowed the thermomechanical data to be analyzed with minimal experimental uncertainty. The thermomechanical results were evaluated on both a phenomenological and microstructural basis. Phenomenological results revealed that the thermomechanical hardening trends were not bounded by those displayed under isothermal conditions. For the case of Hastelloy Alloy X (and similar dynamic strain aging materials), this strongly suggests that some form of thermomechanical testing is necessary when characterizing a thermoviscoplastic deformation model. Transmission electron microscopy was used to study the microstructural physics, and analyze the unique phenomenological behavior.

Castelli, Michael G.↗

Characteristics of energetic solar flare electron spectra

A 55 event survey of energy spectra of 0.1-100 MeV interplanetary electrons originating from solar flares as measured by two spectrometers onboard the ISEE 3 (ICE) spacecraft for the years 1978-1982 has been completed. Spectra generated using the maximum flux of a given event in each energy channel were restricted to events with a well-defined flux rise time. Two broad groups of electron spectra are considered. In one group, the spectra are well represented by a single power law in rigidity with spectral index in the range 3-4.5. The spectra in the other group deviate from a power law in rigidity systematically in that they harden with increasing rigidity. Events with near power-law spectra are found to be correlated with long-duration soft X-ray events, whereas those with hardening spectra are correlated with short-duration events. The possible variation of acceleration and propagation processes with the properties of the flare site is discussed, using the duration of the soft X-ray flare emission as an indicator of the physical parameters of the flare site (flare volume, density, coronal height, and magnetic field geometry).

Moses, Dan↗

High temperature inelastic deformation of the B1900 + Hf alloy under multiaxial loading - Theory and experiment

The multiaxial deformation behavior of the Ni-based alloy B1900 + Hf has been studied at elevated temperatures in the range of 649-982 C. Combined tension/torsion cyclic tests were performed on thin-wall tubular specimens under both in-phase and out-of-phase strain-controlled loading cycles. Both straining conditions resulted in stress loci of comparable magnitude, exhibiting no difference in cyclic hardening response. A phase angle was observed between the deviatoric stress and the incremental plastic strain vectors during 90-deg out-of-phase strain cycling, and nonproportional stress relaxation occurred under biaxial strain hold. The overall results have been used to assess the flow law, the hardening equations, and the applicability of the J2-based, elastic-viscoplastic model of Bodner-Partom (1979) for multiaxial loading conditions. The overall agreement between theory and experiment is good. Discrepancies are discussed in relation to micromechanical considerations.

Chan, K. S.↗

Radial diffusion models of energetic electrons and Jupiter's synchrotron radiation. I - Steady state solution

The results of a computer code modeling of the radial diffusion of equatorially confined energetic electrons in Jupiter's inner magnetosphere are compared with spacecraft as well as ground-based radio (synchrotron radiation) data. It is found that the synchrotron radiation spectrum cannot be reproduced without a significant hardening of the electron spectrum between L = 3 and L = 1.5. This hardening may be due to energy degradation by Jupiter's ring particles. The calculations also suggest that there may be larger-sized material outside Jupiter's ring up to L of about 4 or Io's orbit.

De Pater, Imke↗

1989 IEEE Annual Conference on Nuclear and Space Radiation Effects, 26th, Marco Island, FL, July 25-29, 1989, Proceedings. Part 1

Various papers on nuclear science are presented. The general topics addressed include: basic mechanics of radiation effects, dosimetry and energy-dependent effects, hardness assurance and testing techniques, spacecraft charging and space radiation effects, EMP/SGEMP/IEMP phenomena, device radiation effects and hardening, radiation effects on isolation technologies, IC radiation effects and hardening, and single-event phenomena.

Ochoa, Agustin, Jr.↗

On the thermodynamics of stress rate in the evolution of back stress in viscoplasticity

A thermodynamic foundation using the concept of internal state variables is presented for the kinematic description of a viscoplastic material. Three different evolution equations for the back stress are considered. The first is that of classical, nonlinear, kinematic hardening. The other two include a contribution that is linear in stress rate. Choosing an appropriate change in variables can remove this stress rate dependence. As a result, one of these two models is shown to be equivalent to the classical, kinematic hardening model; while the other is a new model, one which seems to have favorable characteristics for representing ratchetting behavior. All three models are thermodynamically admissible.

Freed, Alan D.↗

On charging of snow particles in blizzard

The causes of the charge polarity on the blizzard, which consisted of fractured snow crystals and ice particles, were investigated. As a result, the charging phenomena showed that the characteristics of the blizzard are as follows: (1) In the case of the blizzard with snowfall, the fractured snow particles drifting near the surface of snow field (lower area: height 0.3 m) had positive charge, while those drifting at higher area (height 2 m) from the surface of snow field had negative charge. However, during the series of blizzards two kinds of particles positively and negatively charged were collected in equal amounts in a Faraday Cage. It may be considered that snow crystals with electrically neutral properties were separated into two kinds of snow flakes (charged positively and negatively) by destruction of the snow crystals. (2) In the case of the blizzard which consisted of irregularly formed ice drops (generated by peeling off the hardened snow field), the charge polarity of these ice drops salting over the snow field was particularly controlled by the crystallographic characteristics of the surface of the snow field hardened by the powerful wind pressure.

Shio, Hisashi↗

A bulk flow model of a brush seal system

Fibers can be readily fabricated into a variety of seal configurations that are compliant and responsive to high speed or lightly loaded systems. A linear, circular, or contoured brush seal system is a contact seal consisting of the bristle pattern and hardened interface. When compared to a labyrinth seal, the brush seal system is superior and features low leakage, dynamic stability, and permits compliant structures. But in turn, the system usually requires a hardened smooth interface and permits only limited pressure drops. Wear life and wear debris for operations with static or dynamic excitation are largely undetermined. A seal system involves control of fluid within specific boundaries. The brush and rub ring (or rub surface) form a seal system. Design similitudes, a bulk flow model, and rub ring (interface) coatings are discussed. The bulk flow model calculations are based on flows in porous media and filters. The coatings work is based on experience and expanded to include current practice.

Hendricks, R. C.↗

1991 IEEE Annual Conference on Nuclear and Space Radiation Effects, 28th, San Diego, CA, July 15-19, 1991, Proceedings

Various papers on nuclear science are presented. The general topics addressed are: basic mechanisms of radiation effects, dosimetry and energy-dependent effects, isolation technologies, device radiation response and hardening, microcircuit radiation response and hardening, single-event phenomena, hardness assurance and testing techniques, spacecraft charging, space environments and effects.

Millward, Douglas G.↗

Crushable Washers For Bolting Composite Panels

Crushable washers proposed for use in protecting composite-material (matrix/fiber) panels against overloads applied by nut-and-bolt fasteners. Intended for use at drilled holes, where strengths of composite panels reduced by exposure of ends of fibers. Washer consists of metal skin filled with microcapsules of epoxy resin and hardener. Alternatively, filled with fibers collapsing under given load. Crushing action simultaneously fractures microcapsules (if used), releasing components of epoxy. These components mix and fill bolthole and fiber-reinforcement interstices. Epoxy then hardens, locking fasteners in place.

Daech, Alfred F.↗

On the structure of nonlinear constitutive equations for fiber reinforced composites

The structure of constitutive equations for nonlinear multiaxial behavior of transversely isotropic fiber reinforced metal matrix composites subject to proportional loading was investigated. Results from an experimental program were combined with numerical simulations of the composite behavior for complex stress to reveal the full structure of the equations. It was found that the nonlinear response can be described by a quadratic flow-potential, based on the polynomial stress invariants, together with a hardening rule that is dominated by two different hardening mechanisms.

Jansson, Stefan↗

Wavelength tunable liquid crystal imaging filters for remote sensing from geosynchronous platforms

Recent advances in liquid crystal technology have enabled us to construct tunable birefringent filters with bandwidths between approximately 0.1 nm and 50 nm. The center wavelength of these filters can be selected electronically, in a few tens of milliseconds, with no moving parts. These liquid crystal tunable filters (LCTF's), together with existing CCD detectors, make possible a new generation of lightweight, rugged, high-resolution imaging spectrophotometers. Such instruments would be particularly interesting for remote sensing applications from geosynchronous platforms. Important advantages exist in the aperture, absence of image shift, power consumption, size, weight, and absence of high drive frequencies, compared to current instruments used or considered for multispectral scene analysis. In the present work, we have reviewed spectral requirements of planned NASA geosynchronous remote sensing missions and identified several applications of the liquid crystal tunable filter technology. We have modeled the LCTF performance in the visible and near-infrared, and carried out a literature study on space-hardening of the filter components, to evaluate the suitability of LCTF's for geosynchronous missions. We have also compared the power consumption, weight, size, reliability, and optical performance of an imaging spectrophotometer using a LCTF monochromator, to other instruments that have been put forward for remote sensing from geosynchronous platforms. We put forward some conceptual designs for LCTF's that seem to offer important reliability, over the mechanical filter wheels presently baselined for the HEPI and ALM experiments. The extremely wide acceptance angle achievable with LCTF's could also avoid the present need for large-aperture interference filters in the ALM (and LIS) experiments. Thermal vacuum testing and radiation damage analysis is required to investigate the space hardening of these new filters for geosynchronous flight.

Foukal, Peter↗

Low cycle fatigue behavior of polycrystalline NiAl at 300 and 1000 K

The low cycle fatigue behavior of polycrystalline NiAl was determined at 300 and 1000 K - temperatures below and above the brittle- to-ductile transition temperature (BDTT). Fully reversed, plastic strain-controlled fatigue tests were conducted on two differently fabricated alloy samples: hot isostatically pressed (HIP'ed) prealloyed powder and hot extruded castings. HIP'ed powder (HP) samples were tested only at 1000 K, whereas the more ductile cast-and-extruded (C+E) NiAl samples were tested at both 1000 and 300 K. Plastic strain ranges of 0.06 to 0.2 percent were used. The C+E NiAl cyclically hardened until fracture, reaching stress levels approximately 60 percent greater than the ultimate tensile strength of the alloy. Compared on a strain basis, NiAl had a much longer fatigue life than other B2 ordered compounds in which fracture initiated at processing-related defects. These defects controlled fatigue life at 300 K, with fracture occurring rapidly once a critical stress level was reached. At 1000 K, above the BDTT, both the C+E and HP samples cyclically softened during most of the fatigue tests in air and were insensitive to processing defects. The processing method did not have a major effect on fatigue life; the lives of the HP samples were about a factor of three shorter than the C+E NiAl, but this was attributed to the lower stress response of the C+E material. The C+E NiAl underwent dynamic grain growth, whereas the HP material maintained a constant grain size during testing. In both materials, fatigue life was controlled by intergranular cavitation and creep processes, which led to fatigue crack growth that was primarily intergranular in nature. Final fracture by overload was transgranular in nature. Also, HP samples tested in vacuum had a life three times longer than their counterparts tested in air and, in contrast to those tested in air, hardened continuously over half of the sample life, thereby indicating an environmentally assisted fatigue damage mechanism. The C+E samples were tested only in air. At 1000 K, NiAl exhibited a superior fatigue life when compared to most superalloys on a plastic strain basis, but was inferior to most superalloys on a stress basis.

Lerch, Bradley A.↗

Tungsten solution kinetics and amorphization of nickel in mechanically alloyed Ni-W alloys

The kinetics of solution of W, and the subsequent amorphization of Ni, in mechanically alloyed Ni-W alloys has been investigated. As W is a highly abrasive material in the energy intensive devices used for mechanical alloying, we studied the above reactions in different mills. One used hardened steel balls as the grinding media, and the other Al2O3. Abrasion is common to both mills, but Fe wear debris from the hardened steel enters into solution in the Ni rich phases whereas Al2O3 debris is present as small dispersoids. The kinetics of W solution and those of subsequent amorphization do not appear strongly affected by the Fe in solution or the Al2O3 dispersoid. Tungsten dissolves in crystalline Ni in amounts in excess of the equilibrium solubility during alloying. Amorphization of the Ni phase occurs if the W content in this phase exceeds ca. 28 at. pct.

Aning, A. O.↗

NiAl alloys for structural uses

Alloys based on the intermetallic compound NiAl are of technological interest as high temperature structural alloys. These alloys possess a relatively low density, high melting temperature, good thermal conductivity, and (usually) good oxidation resistance. However, NiAl and NiAl-base alloys suffer from poor fracture resistance at low temperatures as well as inadequate creep strength at elevated temperatures. This research program explored macroalloying additions to NiAl-base alloys in order to identify possible alloying and processing routes which promote both low temperature fracture toughness and high temperature strength. Initial results from the study examined the additions of Fe, Co, and Hf on the microstructure, deformation, and fracture resistance of NiAl-based alloys. Of significance were the observations that the presence of the gamma-prime phase, based on Ni3Al, could enhance the fracture resistance if the gamma-prime were present as a continuous grain boundary film or 'necklace'; and the Ni-35Al-20Fe alloy was ductile in ribbon form despite a microstructure consisting solely of the B2 beta phase based on NiAl. The ductility inherent in the Ni-35Al-20Fe alloy was explored further in subsequent studies. Those results confirm the presence of ductility in the Ni-35Al-20Fe alloy after rapid cooling from 750 - 1000 C. However exposure at 550 C caused embrittlement; this was associated with an age-hardening reaction caused by the formation of Fe-rich precipitates. In contrast, to the Ni-35Al-20Fe alloy, exploratory research indicated that compositions in the range of Ni-35Al-12Fe retain the ordered B2 structure of NiAl, are ductile, and do not age-harden or embrittle after thermal exposure. Thus, our recent efforts have focused on the behavior of the Ni-35Al-12Fe alloy. A second parallel effort initiated in this program was to use an alternate processing technique, mechanical alloying, to improve the properties of NiAl-alloys. Mechanical alloying in the conventional sense requires ductile powder particles which, through a cold welding and fracture process, can be dispersion strengthened by submicron-sized oxide particles. Using both the Ni-35Al-Fe alloys to contain approx. 1 v/o Y2O3. Preliminary results indicate that mechanically alloyed and extruded NiAl-Fe + Y2O3 alloys when heat treated to a grain-coarsened condition, exhibit improved creep resistance at 1000 C when compared to NiAl; oxidation resistance comparable to NiAl; and fracture toughness values a factor of three better than NiAl. As a result of the research initiated on this NASA program, a subsequent project with support from Inco Alloys International is underway.

Koss, D. A.↗

Single event effects and laser simulation studies

The single event upset (SEU) linear energy transfer threshold (LETTH) of radiation hardened 64K Static Random Access Memories (SRAM's) was measured with a picosecond pulsed dye laser system. These results were compared with standard heavy ion accelerator (Brookhaven National Laboratory (BNL)) measurements of the same SRAM's. With heavy ions, the LETTH of the Honeywell HC6364 was 27 MeV-sq cm/mg at 125 C compared with a value of 24 MeV-sq cm/mg obtained with the laser. In the case of the second type of 64K SRAM, the IBM640lCRH no upsets were observed at 125 C with the highest LET ions used at BNL. In contrast, the pulsed dye laser tests indicated a value of 90 MeV-sq cm/mg at room temperature for the SEU-hardened IBM SRAM. No latchups or multiple SEU's were observed on any of the SRAM's even under worst case conditions. The results of this study suggest that the laser can be used as an inexpensive laboratory SEU prescreen tool in certain cases.

Kim, Q.↗