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At least 361 records · Page 20

Material response from Mach 0.3 burner rig combustion of a coal-oil mixture

Wedge shaped specimens were exposed to the combustion gases of a Mach 0.3 burner rig fueled with a mixture of 40 weight percent micron size coal particles dispersed in No. 2 fuel oil. Exposure temperature was about 900 C and the test duration was about 44 one hour cycles. The alloys tested were the nickel base superalloys, IN-100, U-700 and IN-792, and the cobalt base superalloy, Mar-M509. The deposits on the specimens were analyzed and the extent of corrosion/erosion was measured. The chemical compositions of the deposits were compared with the predictions from an equilibrium thermodynamic analysis. The experimental results were in very good agreement with the predictions.

Santoro, G. J.↗

A new transition radiation detector for cosmic ray nuclei

Test measurements on materials for transition radiation detectors at a low Lorentz factor are reported. The materials will be based on board Spacelab-2 for determining the composition and energy spectra of nuclear cosmic rays in the 1 TeV/nucleon range. The transition radiation detectors consist of a sandwich of radiator-photon detector combinations. The radiators emit X-rays and are composed of polyolefin fibers used with Xe filled multiwired proportional chamber (MWPC) detectors capable of detecting particle Lorentz factors of several hundred. The sizing of the detectors is outlined, noting the requirement of a thickness which provides a maximum ratio of transition radiation to total signal in the chambers. The fiber radiator-MWPC responses were tested at Fermilab and in an electron cyclotron. An increase in transition radiation detection was found as a square power law of Z, and the use of six radiator-MWPC on board the Spacelab-2 is outlined.

Lheureux, J.↗

Viking magnetic properties investigation - Further results

The amounts of magnetic particles held on the reference test chart and backhoe magnets on lander 2 and lander 1 are comparable, indicating the presence of an estimated 3 to 7 percent by weight of relatively pure, strongly magnetic particles in the soil at the lander 2 sampling site. Preliminary spectrophotometric analysis of the material held on the backhoe magnets on lander 1 indicates that its reflectance characteristics are indistinguishable from material within a sampling trench with which it has been compared. The material on the RTC magnet shows a different spectrum, but it is suspected that the difference is the result of a reflectance contribution from the magnesium metal covering on the magnet. It is argued that the results indicate the presence, now or originally, of magnetite, which may be titaniferous.

Hargraves, R. B.↗

Fabrication of Regolith-Derived Radiation Shields: Preliminary Results

Unlike the Earth, Mars and asteroids do not have a magnetosphere to protect humans, mechanisms and electronics from damaging Galactic Cosmic Radiation (GCR) and solar particle events (SPE). This presents one of the highest risks to crew and onboard electronics during interplanetary journeys. The goal of this project is to evaluate the effectiveness of carbonaceous asteroids and other hydrogen-rich materials as potential radiation shielding materials, which ultimately could be tested during planned crewed missions to a captured asteroid fragment (ARM). This type of investigation represents an initial effort to develop radiation shield material compositions, production methods and technologies, and optimization methodology for manufacturing radiation shields in deep space for large exploration human missions or by emerging new industries seeking to stage their spacecraft for the exploitation of the resources of asteroids. Carbonaceous chondrites (C-type) are of particular interest as sources of compounds such as water ice and hydrogen-rich carbon molecules, which can provide sufficient low Z element density to provide radiation protection at adequate shield thicknesses.

Regolith↗

The long-term effects of the micrometeoroid and orbital debris environments on materials used in space

The long-term effects of the orbital debris and micrometeoroid environments on materials that are current candidates for use on space vehicles are discussed. In addition, the limits of laboratory testing to determine these effects are defined and the need for space-based data is delineated. The impact effects discussed are divided into primary and secondary surfaces. Primary surfaces are those that are subject to erosion, pitting, the degradation and delamination of optical coatings, perforation of atomic oxygen erosion barriers, vapor coating of optics and the production of secondary ejecta particles. Secondary surfaces are those that are affected by the result of the perforation of primary surfaces, for example, vapor deposition on electronic components and other sensitive equipment, and the production of fragments with damage potential to internal pressurized elements. The material properties and applications that are required to prevent or lessen the effects described, are defined.

Cour-Palais, Burton G.↗

Spacecraft Fire Safety Research at NASA Glenn Research Center

Appropriate design of fire detection systems requires knowledge of both the expected fire signature and the background aerosol levels. Terrestrial fire detection systems have been developed based on extensive study of terrestrial fires. Unfortunately there is no corresponding data set for spacecraft fires and consequently the fire detectors in current spacecraft were developed based upon terrestrial designs. In low gravity, buoyant flow is negligible which causes particles to concentrate at the smoke source, increasing their residence time, and increasing the transport time to smoke detectors. Microgravity fires have significantly different structure than those in 1-g which can change the formation history of the smoke particles. Finally the materials used in spacecraft are different from typical terrestrial environments where smoke properties have been evaluated. It is critically important to detect a fire in its early phase before a flame is established, given the fixed volume of air on any spacecraft. Consequently, the primary target for spacecraft fire detection is pyrolysis products rather than soot. Experimental investigations have been performed at three different NASA facilities which characterize smoke aerosols from overheating common spacecraft materials. The earliest effort consists of aerosol measurements in low gravity, called the Smoke Aerosol Measurement Experiment (SAME), and subsequent ground-based testing of SAME smoke in 55-gallon drums with an aerosol reference instrument. Another set of experiments were performed at NASAs Johnson Space Center White Sands Test Facility (WSTF), with additional fuels and an alternate smoke production method. Measurements of these smoke products include mass and number concentration, and a thermal precipitator was designed for this investigation to capture particles for microscopic analysis. The final experiments presented are from NASAs Gases and Aerosols from Smoldering Polymers (GASP) Laboratory, with selected results focusing on realistic fuel preparations and heating profiles with regards to early detection of smoke. SAFFIRE is the upcoming large-scale fire experiment which will be executed in a Cygnus vehicle after it undocks from the ISS.

Aerosol↗

Constitutive and Stability Behavior of Soils in Microgravity Environment

All aspects of soil stability, bearing capacity, slope stability, the supporting capacity of deep foundations, and penetration resistance depend on soil strength. The stress-deformation and stress-deformation-time behavior of soils are of importance in any problem where ground movements are of interest. In most engineering materials, the strength is derived from internal chemical and physico-chemical forces of interaction, which bond the atoms, molecules, and particles together. In soils, the constitutive relations are mainly derived from interparticle friction between particles and particle groups and dilatancy, and to a lesser extent from particle bonding by weak electrostatic, physico-chemical, and coulomb forces. For engineering purposes, soils are classified as cohesive (clays and silts; typical particle sizes range from 10 nm to 10 micrometers) and cohesionless (sand and gravel; typical particle sizes range from 10 micrometers to 75 mm). The mechanical or constitutive properties of cohesionless soils or granular materials are highly fabric-dependent, highly non-linear, and non-conservative with engineering properties primarily depending on the effects of gravity through self-weight and on the tractions or forces applied to the soil mass. Under moderate-to-high stress levels, the influence of gravity on the behavior of laboratory test specimens may not be pronounced and, therefore, the test results in terrestrial (1-g) environment may be sufficiently conclusive. However at low interparticle stresses, which can result either from low applied (confining) stresses or from excess pore fluid pressures developed within the soil mass without corresponding changes in the applied stresses, the presence of gravitational body forces acting on solid particles and interstitial fluids exerts a pronounced influence on movement of individual particles or particle groups. Such motions, in turn, cause changes in soil fabric which results in significant changes in the interparticle friction forces contributing to the soil's strength and deformation characteristics.

Alshibli, Khalid A.↗

Results From Mars Show Electrostatic Charging of the Mars Pathfinder Sojourner Rover

Indirect evidence (dust accumulation) has been obtained indicating that the Mars Pathfinder rover, Sojourner, experienced electrostatic charging on Mars. Lander camera images of the Sojourner rover provide distinctive evidence of dust accumulation on rover wheels during traverses, turns, and crabbing maneuvers. The sol 22 (22nd Martian "day" after Pathfinder landed) end-of-day image clearly shows fine red dust concentrated around the wheel edges with additional accumulation in the wheel hubs. A sol 41 image of the rover near the rock "Wedge" (see the next image) shows a more uniform coating of dust on the wheel drive surfaces with accumulation in the hubs similar to that in the previous image. In the sol 41 image, note particularly the loss of black-white contrast on the Wheel Abrasion Experiment strips (center wheel). This loss of contrast was also seen when dust accumulated on test wheels in the laboratory. We believe that this accumulation occurred because the Martian surface dust consists of clay-sized particles, similar to those detected by Viking, which have become electrically charged. By adhering to the wheels, the charged dust carries a net nonzero charge to the rover, raising its electrical potential relative to its surroundings. Similar charging behavior was routinely observed in an experimental facility at the NASA Lewis Research Center, where a Sojourner wheel was driven in a simulated Martian surface environment. There, as the wheel moved and accumulated dust (see the following image), electrical potentials in excess of 100 V (relative to the chamber ground) were detected by a capacitively coupled electrostatic probe located 4 mm from the wheel surface. The measured wheel capacitance was approximately 80 picofarads (pF), and the calculated charge, 8 x 10(exp -9) coulombs (C). Voltage differences of 100 V and greater are believed sufficient to produce Paschen electrical discharge in the Martian atmosphere. With an accumulated net charge of 8 x 10(exp -9) C, and average arc time of 1 msec, arcs can also occur with estimated arc currents approaching 10 milliamperes (mA). Discharges of this magnitude could interfere with the operation of sensitive electrical or electronic elements and logic circuits. Sojourner rover wheel tested in laboratory before launch to Mars. Before launch, we believed that the dust would become triboelectrically charged as it was moved about and compacted by the rover wheels. In all cases observed in the laboratory, the test wheel charged positively, and the wheel tracks charged negatively. Dust samples removed from the laboratory wheel averaged a few ones to tens of micrometers in size (clay size). Coarser grains were left behind in the wheel track. On Mars, grain size estimates of 2 to 10 mm were derived for the Martian surface materials from the Viking Gas Exchange Experiment. These size estimates approximately match the laboratory samples. Our tentative conclusion for the Sojourner observations is that fine clay-sized particles acquired an electrostatic charge during rover traverses and adhered to the rover wheels, carrying electrical charge to the rover. Since the Sojourner rover carried no instruments to measure this mission's onboard electrical charge, confirmatory measurements from future rover missions on Mars are desirable so that the physical and electrical properties of the Martian surface dust can be characterized. Sojourner was protected by discharge points, and Faraday cages were placed around sensitive electronics. But larger systems than Sojourner are being contemplated for missions to the Martian surface in the foreseeable future. The design of such systems will require a detailed knowledge of how they will interact with their environment. Validated environmental interaction models and guidelines for the Martian surface must be developed so that design engineers can test new ideas prior to cutting hardware. These models and guidelines cannot be validated without actual flighata. Electrical charging of vehicles and, one day, astronauts moving across the Martian surface may have moderate to severe consequences if large potential differences develop. The observations from Sojourner point to just such a possibility. It is desirable to quantify these results. The various lander/rover missions being planned for the upcoming decade provide the means for doing so. They should, therefore, carry instruments that will not only measure vehicle charging but characterize all the natural and induced electrical phenomena occurring in the environment and assess their impact on future missions.

Kolecki, Joseph C.↗

Formation of Nanophase Iron in Lunar Soil Simulant for Use in ISRU Studies

For the prospective return of humans to the Moon and the extensive amount of premonitory studies necessary, large quantities of lunar soil simulants are required, for a myriad of purposes from construction/engineering purposes all the way to medical testing of its effects from ingestion by humans. And there is only a limited and precious quantity of lunar soil available on Earth (i.e., Apollo soils) - therefore, the immediate need for lunar soil simulants. Since the Apollo era, there have been several simulants; of these JSC-1 (Johnson Space Center) and MLS-1 (Minnesota Lunar Simulant) have been the most widely used. JSC-1 was produced from glassy volcanic tuff in order to approximate lunar soil geotechnical properties; whereas, MLS-1 approximates the chemistry of Apollo 11 high-Ti soil, 10084. Stocks of both simulants are depleted, but JSC-1 has recently gone back into production. The lunar soil simulant workshop, held at Marshall Space Flight Center in January 2005, identified the need to make new simulants for the special properties of lunar soil, such as nanophase iron (np-Fe(sup 0). Hill et al. (2005, this volume) showed the important role of microscale Fe(sup 0) in microwave processing of the lunar soil simulants JSC-1 and MLS-1. Lunar soil is formed by space weathering of lunar rocks (e.g., micrometeorite impact, cosmic particle bombardment). Glass generated during micrometeorite impact cements rock and mineral fragments together to form aggregates called agglutinates, and also produces vapor that is deposited and coats soil grains. Taylor et al. (2001) showed that the relative amount of impact glass in lunar soil increases with decreasing grain size and is the most abundant component in lunar dust (less than 20 micrometer fraction). Notably, the magnetic susceptibility of lunar soil also increases with the decreasing grain size, as a function of the amount of nanophase-sized Fe(sup 0) in impact-melt generated glass. Keller et al. (1997, 1999) also discovered the presence of abundant np-Fe(sup 0) particles in the glass patinas coating most soil particles. Therefore, the correlation of glass content and magnetic susceptibility can be explained by the presence of the np-Feo particles in glass: small particles contain relatively more np-Fe(sup 0) as glass coatings because the surface area versus mass ratio of the grain size is so increased. The magnetic properties of lunar soil are important in dust mitigation on the Moon (Taylor et al. 2005). Thus material simulating this property is important for testing mitigation methods using electromagnetic field. This np- Fe(sup 0) also produces a unique energy coupling to normal microwaves, such as present in kitchen microwave ovens. Effectively, a portion of lunar soil placed in a normal 2.45 GHz oven will melt at greater than 1200 C before your tea will boil at 100 C, a startling and new discovery reported by Taylor and Meek (2004, 2005). Several methods have been investigated in attempts to make nanophase-sized Feo dispersed within silicate glass; like in the lunar glass. We have been successful in synthesizing such a product and continue to improve on our recipe. We have performed extensive experimentation on this subject to date. Ultimately it will probably be necessary to add this np-Fe(sup 0) bearing silicate glass to lunar soil stimulant, like JSC-1, to actually produce the desired magnetic and microwave coupling properties for use in appropriate ISRU experimentation.

Liu, Yang↗

Effects of high energy simulated space radiation on polymeric second-surface mirrors

A radiation effects experimental program was performed, in which second surface mirror type thermal control coatings were exposed to ultraviolet radiation, electrons, and protons simultaneously. Stability was assessed by making periodic spectral reflectance measurements in situ (and in air after testing for comparison). Solar absorption coefficients were derived by computer. Many of the exposed materials showed large amounts of degradation in reflectance absorptance, principally due to the electron exposure. A series of tests was conducted, leading to the identification of a modified second surface mirror that shows considerable improvement and promise for stability during thermal control applications in a charged particle space radiation environment.

Eogdall, L. B.↗

Apollo-Soyuz experiments summary

The science and technology program conducted by the Apollo crew during the Apollo Soyuz Test Project consisted of 28 separate experiments including five conducted jointly with the Soyuz crew. Experiments were classified in the broad categories of space sciences (astronomy and earth studies), life sciences (particle radiation effects on living cells, the human immune system, and the vestibular system), and materials processing (electrophoresis and solid processing). Experimental designs and results are summarized.

Giuli, R. T.↗

Development of high strength, high temperature ceramics

Improvement in the high-pressure turbopumps, both fuel and oxidizer, in the Space Shuttle main engine were considered. The operation of these pumps is limited by temperature restrictions of the metallic components used in these pumps. Ceramic materials that retain strength at high temperatures and appear to be promising candidates for use as turbine blades and impellers are discussed. These high strength materials are sensitive to many related processing parameters such as impurities, sintering aids, reaction aids, particle size, processing temperature, and post thermal treatment. The specific objectives of the study were to: (1) identify and define the processing parameters that affect the properties of Si3N4 ceramic materials, (2) design and assembly equipment required for processing high strength ceramics, (3) design and assemble test apparatus for evaluating the high temperature properties of Si3N4, and (4) conduct a research program of manufacturing and evaluating Si3N4 materials as applicable to rocket engine applications.

Hall, W. B.↗

Projectile Density Effects on Shield Performance

In the past, the orbital debris environment was modeled as consisting entirely of aluminum particles. As a consequence, most of the impact test database on spacecraft micro-meteoroid and orbital debris (MMOD) shields, and the resulting ballistic limit equations used to predict shielding performance, has been based on using aluminum projectiles. Recently, data has been collected from returned spacecraft materials and other sources that indicate higher and lower density components of orbital debris also exist. New orbital debris environment models such as ORDEM2008 provide predictions of the fraction of orbital debris in various density bins (high = 7.9 g/cu cm, medium = 2.8 g/cu cm, and low = 0.9-1.1 g/cu cm). This paper describes impact tests to assess the effects of projectile density on the performance capabilities of typical MMOD shields. Updates to shield ballistic limit equations are provided based on results of tests and analysis.

Christiansen, Eric L.↗

Potential Use of In Situ Material Composites such as Regolith/Polyethylene for Shielding Space Radiation

NASA has an extensive program for studying materials and methods for the shielding of astronauts to reduce the effects of space radiation when on the surfaces of the Moon and Mars, especially in the use of in situ materials native to the destination reducing the expense of materials transport. The most studied material from the Moon is Lunar regolith and has been shown to be as efficient as aluminum for shielding purposes (1). The addition of hydrogenous materials such as polyethylene should increase shielding effectiveness and provide mechanical properties necessary of structural materials (2). The neutron radiation shielding effectiveness of polyethylene/regolith stimulant (JSC-1A) composites were studied using confluent human fibroblast cell cultures exposed to a beam of high-energy spallation neutrons at the 30deg-left beam line (ICE house) at the Los Alamos Neutron Science Center. At this angle, the radiation spectrum mimics the energy spectrum of secondary neutrons generated in the upper atmosphere and encountered when aboard spacecraft and high-altitude aircraft. Cell samples were exposed in series either directly to the neutron beam, within a habitat created using regolith composite blocks, or behind 25 g/sq cm of loose regolith bulk material. In another experiment, cells were also exposed in series directly to the neutron beam in T-25 flasks completely filled with either media or water up to a depth of 20 cm to test shielding effectiveness versus depth and investigate the possible influence of secondary particle generation. All samples were sent directly back to JSC for sub-culturing and micronucleus analysis. This presentation is of work performed in collaboration with the NASA sponsored Center for Radiation Engineering and Science for Space Exploration (CRESSE) at Prairie View A&M.

Theriot, Corey A.↗

New Material for Surface-Enhanced Raman Spectroscopy

A chemical method of synthesis and application of coating materials that are especially suitable for surface-enhanced Raman spectroscopy (SERS) has been developed. The purpose of this development is to facilitate the utilization of the inherently high sensitivity of SERS to detect chemicals of interest (analytes) in trace amounts, without need for lengthy sample preparation. Up to now, the use of SERS has not become routine because the methods available have not been able to reproduce sampling conditions and provide quantitative measurements. In contrast, the coating materials of the present method enable analysis with minimum preparation of samples, and SERS measurements made using these materials are reproducible and reversible. Moreover, unlike in methods investigated in prior efforts to implement SERS, sampling is not restricted to such specific environments as electrolytes or specific solvents. The coating materials of this method are porous glasses, formed in sol-gel processes, that contain small particles of gold or silver metal. Materials of this type can be applied to the sample-contact surfaces of a variety of sampling and sensing devices, including glass slides, glass vials, fiber-optic probes, and glass tubes. Glass vials with their insides coated according to this method are particularly convenient for SERS to detect trace chemicals in solutions: One simply puts a sample solution containing the analyte(s) into a vial, then puts the vial into a Raman spectrometer for analysis. The chemical ingredients and the physical conditions of the sol-gel process have been selected so that the porous glass formed incorporates particles of the desired metal with size(s) to match the wavelength(s) of the SERS excitation laser in order to optimize the generation of surface plasmons. The ingredients and processing conditions have further been chosen to tailor the porosity and polarity of the glass to optimize the sample flow and the interaction between the analyte(s) and the plasmon field that generates Raman photons. The porous silica network of a sol-gel glass creates a unique environment for stabilizing SERS-active metal particles. Relative to other material structures that could be considered for SERS, the porous silica network offers higher specific surface area and thus greater interaction between analyte molecules and metal particles. Efforts to perform SERS measurements with the help of sampling devices coated by this method have been successful. In tests, numerous organic and inorganic chemicals were analyzed in several solvents, including water. The results of the tests indicate that the SERS measurements were reproducible within 10 percent and linear over five orders of magnitude. One measure of the limits of detectability of chemicals in these tests was found to be a concentration of 300 parts per billion. Further development may eventually make it possible to realize the full potential sensitivity of SERS for detecting some analytes in quantities as small as a single molecule.

Farquharson, Stuart↗

Development of the Electrostatic Precipitator (ESP) for Mars and Electrodynamic Dust Shield (EDS)

Kennedy Space Center's Swamp Works is a fast-paced and diverse technology development laboratory that aims to advance commercial and government capabilities to colonize extraterrestrial environments. As a part of Swamp Works, the Electrostatic and Surface Physics Laboratory (ESPL) is currently developing new technologies that will further NASA's capabilities to colonize lunar and Martian environments. At the ESPL, the objective of the overall project is to aid in the dust mitigation of robotic and human exploration missions to the moon and Mars. The moon and Mars are covered with layers of dust, which can make long-term exploration missions very difficult. The team at the ESPL is developing an electrostatic precipitator (ESP) to aid in the reduction of interference from airborne Martian dust on equipment. The ESP is designed to mitigate the dust in an intake of CO2-rich dusty gas (i.e., the Martian atmosphere). The ESP is essentially a cylindrical tube with a coaxial wire electrode. Applying a high voltage through this electrode induces a corona discharge (a glowing plasma that envelops the electrode), which is used to charge the inflowing dust. The electric field caused by the corona pushes the charged dust to the walls of the precipitator, preventing the dust to flow out of the tube. Environmental dust can make long-term exploration missions very difficult, and settled dust is no exception. Settled lunar or Martian dust can hinder the performance and lifetime of equipment. For example, dust can settle on the solar panels of a lunar or Martian rover, decreasing its performance while increasing its charging time. To address this, the team at the ESPL is also developing an electrodynamic dust shield (EDS), which is designed to remove lunar or Martian dust from the surfaces of equipment. The EDS uses a non-uniform electric field to generate a dielectrophoretic force, which pushes the particles away from the surface of the shield. A number of dust shields will be tested on the exterior of the International Space Station (ISS) via MISSE-11, a flight payload to the ISS that will test the effects of long-term exposure to space on materials. During my internship at the ESPL, I aided in the development of these technologies. For the ESP, I helped characterize the electrical properties of various geometries and helped redesign the hardware of the testbed (the precipitator used to test this technology in the lab). To characterize the electrical properties of the ESP, I ran various tests of the precipitator, which consisted of varying the environmental conditions and geometry of the testbed. Analyzing the electrical properties of the ESP in various environmental conditions is necessary to characterize its collection efficiency, since it will be used in the dusty Martian environment. For the EDS, I helped analyze the dielectric strength of the surface of the shield via high-voltage testing. A dielectrically strong surface will help the shield survive the harsh environment of space, which will enable it to have both lunar and Martian applications.

Corona Discharge↗

Spacecraft material applications: Long-term stability questions

An examination of the materials concerns for a variety of spacecraft components shows that long-term stability within the space environments is a major issue in the design of large space antenna systems. This survey paper will review some of the more recent work on the effect of space environment on (1) thin films, (2) structural composites, and (3) thermal control materials. Degradation in thermal-mechanical and optical properties associated with atmospheric and trapped particles and ultraviolet light will be highlighted. Finally, the dimensional instability associated with microcracking during thermal cycling will be examined and a methodology for estimating thermal fatigue effects from results of mechanical fatigue tests will be presented.

Crossman, F. W.↗

Adhesive Wear of Rollers in Vacuum

This work was done to support NASA's James Webb Space Telescope that is equipped with a Near Infrared Camera and Spectrograph and Micro Shutter Assembly (MSA). A MSA mechanism's qualification test in cryogenic vacuum at 30deg K for 96K cycles resulted in roller wear and formation of some debris. Lab tests in vacuum were conducted at NASA Glenn Research Center (GRC) to understand the wear of Ti6Al4V mated with 440F steel rollers. Misalignment angle was found to have the most significant effect on debris formation. At misalignment angle of 1.4deg, significant amount of wear debris were formed within 50,000 cycles. Very few wear particles were found for a zero misalignment angle, and the total wear was small even after 367,000 cycles. The mode of wear in all the tests was attributed to adhesion, which was clearly evident from video records as well as the plate-like amalgamated debris material from both rollers. The adhesive wear rate was found to be approximately proportional to the misalignment angle. The wear is a two-way phenomenon, and the mixing of both roller materials in wear debris was confirmed by x-ray fluorescence (XRF) and EDX spectra. While there was a net loss of mass from the steel rollers, XRF and energy dispersive x-ray (EDX) spectra showed peaks of Ti on steel rollers, and peaks of Fe on Ti rollers. These results are useful for designers in terms of maintaining appropriate tolerances to avoid misalignment of rolling elements and the resulting severe wear

Shaeef, Iqbal↗