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DOE OSTI2019

Guidance on the Use of Existing ASTM Polymer Testing Standards for ABS Parts Fabricated Using FFF

When evaluating the static mechanical performance of fused filament fabrication (FFF) polymers, researchers have conducted tensile testing using American Society for Testing Materials International (ASTM) D3039 rectangular test specimens and ASTM D638 Type I and Type IV dogbone test specimens. The choice of ASTM D638 versus ASTM D3039 test specimen geometry is usually based on the perceived susceptibility of the ASTM D638 test specimens to failure within the fillet radius. ASTM polymer and plastic tensile test standards define criteria for acceptably tested specimens as requiring failure inside the narrow length (i.e., ASTM D638) or outside of the grips (i.e., ASTM D3039) for the results to be considered acceptable. There has been limited published research regarding the selection of an ASTM test specimen geometry for FFF polymer materials. This study provides evidence-based guidance through the comparison of the mechanical performance and failure acceptance rates of ASTM D3039 and ASTM D638 test specimen geometries, fabricated using FFF acrylonitrile butadiene styrene (ABS). Here, the purpose of the study is to provide guidance on the use of existing ASTM polymer testing standards for additively manufactured polymers. Results indicate there is an inherent benefit to using ASTM D3039 over ASTM D638 Type I and Type IV test specimens for tensile testing. ASTM D3039 test specimens provide the most consistent failure within the test specimen’s gage length, which is attributed to the rectangular design of the test specimen. Results also indicated that, like traditionally manufactured polymer composites, there will be differences in the tensile test results (e.g., ultimate tensile strength, elastic modulus) based on the different cross-sectional areas of the test specimen geometries.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Innovative thermal distillation method using solar heat localization

The thermal distillation uses energy to evaporate water and subsequently condense the vapor to liquid form. Waste energy from industrial processes, electricity, or solar energy are the examples of an input energy for thermal distillation systems. In this paper, we have designed, fabricated, and tested an eco-friendly and low- cost distillation system which uses solar heat localization for evaporation of water and later condense the vapor back to liquid as liquid water. The unique feature of this method is the high rate of evaporation when compared to other thermal solar distillation/desalination systems. In this method, the incoming heat is confined to the porous media where bottom layer acts a porous insulator. The capillary force in the porous structure pumps up the liquid water to the hot surface, within the porous medium, where liquid heats up and changes to vapor phase. Since there is no moving part in this method, and due to its independency to electricity, it a great candidate for deployment in remote areas that access to grid power is limited and maintenance is not feasible.

Jaladi, Divya↗

DOE OSTI2019

Used Fuel Storage Monitoring Using Helium-4 Scintillation Fast Neutron Detectors and Neutron Spectral Analysis

This project aimed to address the technology gap in the reliable methods to verify contents of sealed dry storage casks for spent nuclear fuel. Helium-4 gas scintillation neutron detectors was proposed to be developed into a neutron spectroscopy and imaging system for nuclear security and safeguards applications. 4 He gas is significantly more available than 3 He gas and it has unique advantages such as low gamma interaction probability and direct detection of fast neutrons. Due to the sheer amount of fissile materials in a single dry cask, there is a significant neutron fluence emitted whose energies range from thermal to uncollided high-energy neutrons suitable for the detection capability of the 4 He detectors. Our project demonstrated the first ever neutron spectroscopic capabilities using 4 He detectors, explored novel detector design and performed detector characterization. It further qualified the detectors for use in various applications including high-flux environments with significant gamma-fluence. Computer simulations were used to test various large cask measurement system designs and tests, beyond the compact prototype system and laboratory measurements exploring the feasibility of the neutron spectroscopic approach. Although some cask-characterization methods proved unfeasible, alternative characterization methods using the He-4 detectors were explored and generated promising results.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2020

CO 2 to Bioplastics: Beneficial Re-use of Carbon Emissions from Coal-fired Power Plants using Microalgae

This project sought to address the technical and economic barriers to carbon dioxide (CO 2 ) capture and utilization using microalgae. Specifically, a dual photobioreactor (PBR)/open raceway pond (ORP) cultivation system was evaluated with respect to capital and operational costs, productivity, and culture health, and compared to an ORP-only cultivation system. In the dual (or “hybrid”) system, a cyclic flow PBR was used to provide inoculum for two open raceway ponds after each harvest, with the hypothesis that this PBR + pond system should result in improved performance compared to traditional raceway ponds. Two other raceway ponds were operated conventionally as a control, the experiments being performed at Duke Energy’s East Bend Station in northern KY using coal-derived flue gas as the CO 2 source. Although algae productivity achieved was mediocre due to the fact that the experiments had to be performed late in the growing season when climatic conditions were not optimal for high growth, the hybrid cultivation system showed a higher level of algae productivity (statistically significant) compared to the traditional ponds. In order to realize the maximum value of the algal biomass produced, fractionation of the biomass was examined. Bioplastic compounding and material characterization was subsequently performed using three feed stocks: whole biomass, lipid-extracted biomass and the proteinaceous residue from full fractionation. In general, the whole and lipid-extracted biomass gave similar results in terms of the properties of the resulting bioplastics, while the proteinaceous residue showed promise for the production of a polybutylene adipate terephthalate (PBAT) blend. Finally, sustainability assessment of a putative biorefinery system was conducted, including techno-economic and life cycle impact assessment. Nine different production scenarios were considered, comprising combinations of the three different biomass growth architectures (ORP, PBR and dual PBR-ORP systems) coupled with three different algae biomass processing pathways (drying only, lipid extraction and fractionation). Results show that the minimum selling price of the bioplastic feed stock (BPFS) is within the realm of economic competition with prices as low as $970 USD tonne -1 . Additionally, life cycle impact assessment results indicate drastic improvements in performance of the produced BPFS, with reductions in greenhouse gas emissions ranging between 67 and 116% compared to a petroleum based plastic feedstock.

01 COAL, LIGNITE, AND PEAT↗

DOE OSTI2017

Using Systems Approaches to Improve Photosynthesis and Water Use Efficiency in Sorghum

Throughout the 5 years of this project, 8 labs coordinated to make significant progress on our understanding of how C4 grasses, which include some of our most important crops, can use water more efficiently. We took an integrated approach, using physiology to study how to improve photosynthesis, how to manipulate the pores that move water and CO2 in and out of leaves and the formation and structure of roots. We coupled that with genetic and computational approaches to identify the genes controlling these traits and then used modeling to understand how the genomic system integrates the functions of the genes. We then developed synthetic biology approaches to manipulate the genes and gene editing and plant transformation approaches to insert those traits into a model C4 grass and the bioenergy crop Sorghum bicolor. Through the course of the project, we developed new software tools and genetic resources, filed 5 patents and published 46 papers. We made significant contributions to the bioeconomy through the training of undergraduates, graduate students and postdoctoral researchers. In addition to addressing the specific objectives, our work on this project led to several new and exciting outcomes. We were also to use our expertise and efforts to contribute to many community efforts.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2017

Optimized Generator Designs for the DTU 10-MW Offshore Wind Turbine using GeneratorSE

Compared to land-based applications, offshore wind imposes challenges for the development of next generation wind turbine generator technology. Direct-drive generators are believed to offer high availability, efficiency, and reduced operation and maintenance requirements; however, previous research suggests difficulties in scaling to several megawatts or more in size. The resulting designs are excessively large and/or massive, which are major impediments to transportation logistics, especially for offshore applications. At the same time, geared wind turbines continue to sustain offshore market growth through relatively cheaper and lightweight generators. However, reliability issues associated with mechanical components in a geared system create significant operation and maintenance costs, and these costs make up a large portion of overall system costs offshore. Thus, direct-drive turbines are likely to outnumber their gear-driven counterparts for this market, and there is a need to review the costs or opportunities of building machines with different types of generators and examining their competitiveness at the sizes necessary for the next generation of offshore wind turbines. In this paper, we use GeneratorSE, the National Renewable Energy Laboratory's newly developed systems engineering generator sizing tool to estimate mass, efficiency, and the costs of different generator technologies satisfying the electromagnetic, structural, and basic thermal design requirements for application in a very large-scale offshore wind turbine such as the Technical University of Denmark's (DTU) 10-MW reference wind turbine. For the DTU reference wind turbine, we use the previously mentioned criteria to optimize a direct-drive, radial flux, permanent-magnet synchronous generator; a direct-drive electrically excited synchronous generator; a medium-speed permanent-magnet generator; and a high-speed, doubly-fed induction generator. Preliminary analysis of leveled costs of energy indicate that for large turbines, the cost of permanent magnets and reliability issues associated with brushes in electrically excited machines are the biggest deterrents for building direct-drive systems. The advantage of medium-speed permanent-magnet machines over doubly-fed induction generators is evident, yet, variability in magnet prices and solutions to address reliability issues associated with gearing and brushes can change this outlook. This suggests the need to potentially pursue fundamentally new innovations in generator designs that help avoid high capital costs but still have significant reliability related to performance.

17 WIND ENERGY↗

DOE OSTI2017

K-ε Turbulence Model Parameter Estimates Using an Approximate Self-similar Jet-in-Crossflow Solution

The k-ε turbulence model has been described as perhaps “the most widely used complete turbulence model.” This family of heuristic Reynolds Averaged Navier-Stokes (RANS) turbulence closures is supported by a suite of model parameters that have been estimated by demanding the satisfaction of well-established canonical flows such as homogeneous shear flow, log-law behavior, etc. While this procedure does yield a set of so-called nominal parameters, it is abundantly clear that they do not provide a universally satisfactory turbulence model that is capable of simulating complex flows. Recent work on the Bayesian calibration of the k-ε model using jet-in-crossflow wind tunnel data has yielded parameter estimates that are far more predictive than nominal parameter values. In this paper, we develop a self-similar asymptotic solution for axisymmetric jet-in-crossflow interactions and derive analytical estimates of the parameters that were inferred using Bayesian calibration. The self-similar method utilizes a near field approach to estimate the turbulence model parameters while retaining the classical far-field scaling to model flow field quantities. Our parameter values are seen to be far more predictive than the nominal values, as checked using RANS simulations and experimental measurements. They are also closer to the Bayesian estimates than the nominal parameters. A traditional simplified jet trajectory model is explicitly related to the turbulence model parameters and is shown to yield good agreement with measurement when utilizing the analytical derived turbulence model coefficients. Finally, the close agreement between the turbulence model coefficients obtained via Bayesian calibration and the analytically estimated coefficients derived in this paper is consistent with the contention that the Bayesian calibration approach is firmly rooted in the underlying physical description.

42 ENGINEERING↗

DOE OSTI2021

Using diglycolamides to improve rare-earth element separation

The family of 17 elements known as the “rare earth elements” are difficult to produce economically. Despite this, they are described as “critical raw materials” because of their unique properties and their various technological applications. This means their use is accelerating globally. Separation of these elements is a fundamental challenge, but this does not daunt Dr Santa Jansone-Popova and her team at Oak Ridge National Laboratory. In recovering praseodymium from neodymium using a variety of ligands known as diglycolamides, she has been demonstrating potentially game-changing advances in liquid-liquid separations that could realise more of these in-demand materials.

Jansone-Popova, Santa↗

DOE OSTI2016

Quantifying the interstellar medium and cosmic rays in the MBM 53, 54, and 55 molecular clouds and the pegasus loop using Fermi-LAT gamma-ray observations

A study of the interstellar medium (ISM) and cosmic rays (CRs) using Fermi Large Area Telescope (LAT) data, in a region encompassing the nearby molecular clouds MBM 53, 54, and 55 and a far-infrared loop-like structure in Pegasus, is reported. By comparing the Planck dust thermal emission model with Fermi-LAT γ-ray data, it was found that neither the dust radiance (R) nor the dust opacity at 353 GHz (τ {sub 353}) was proportional to the total gas column density N(H{sub tot}) primarily because N(H{sub tot})/R and N(H{sub tot})/τ {sub 353} depend on the dust temperature (T {sub d}). The N(H{sub tot}) distribution was evaluated using γ-ray data by assuming the regions of high T {sub d} to be dominated by optically thin atomic hydrogen (H I) and by employing an empirical linear relation of N(H{sub tot})/R to T {sub d}. It was determined that the mass of the gas not traced by the 21 cm or 2.6 mm surveys is ∼25% of the mass of H I in the optically thin case and is larger than the mass of the molecular gas traced by carbon monoxide by a factor of up to 5. The measured γ-ray emissivity spectrum is consistent with a model based on CR spectra measured at the Earth and a nuclear enhancement factor of ≤1.5. It is, however, lower than local H I emissivities reported by previous Fermi-LAT studies employing different analysis methods and assumptions on ISM properties by 15%–20% in energies below a few GeV, even if we take account of the statistical and systematic uncertainties. The origin of the discrepancy is also discussed.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2017

Search for Astrophysical Sources of Neutrinos Using Cascade Events in IceCube

The IceCube neutrino observatory has established the existence of a flux of high-energy astrophysical neutrinos, which is inconsistent with the expectation from atmospheric backgrounds at a significance greater than 5 σ . This flux has been observed in analyses of both track events from muon neutrino interactions and cascade events from interactions of all neutrino flavors. Searches for astrophysical neutrino sources have focused on track events due to the significantly better angular resolution of track reconstructions. To date, no such sources have been confirmed. Here we present the first search for astrophysical neutrino sources using cascades interacting in IceCube with deposited energies as small as 1 TeV. No significant clustering was observed in a selection of 263 cascades collected from 2010 May to 2012 May. We show that compared to the classic approach using tracks, this statistically independent search offers improved sensitivity to sources in the southern sky, especially if the emission is spatially extended or follows a soft energy spectrum. This enhancement is due to the low background from atmospheric neutrinos forming cascade events and the additional veto of atmospheric neutrinos at declinations ≲−30°.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2017

Reducing Uncertainties in the Production of the Gamma-emitting Nuclei {sup 26}Al, {sup 44}Ti, and {sup 60}Fe in Core-collapse Supernovae by Using Effective Helium Burning Rates

We have used effective reaction rates (ERRs) for the helium burning reactions to predict the yield of the gamma-emitting nuclei {sup 26}Al, {sup 44}Ti, and {sup 60}Fe in core-collapse supernovae (SNe). The variations in the predicted yields for values of the reaction rates allowed by the ERR are much smaller than obtained previously, and smaller than other uncertainties. A “filter” for SN nucleosynthesis yields based on pre-SN structure was used to estimate the effect of failed SNe on the initial mass function averaged yields; this substantially reduced the yields of all these isotopes, but the predicted yield ratio {sup 60}Fe/{sup 26}Al was little affected. The robustness of this ratio is promising for comparison with data, but it is larger than observed in nature; possible causes for this discrepancy are discussed.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2017

On-Board Particulate Filter Failure Prevention and Failure Diagnostics Using Radio Frequency Sensing

The increasing use of diesel and gasoline particulate filters requires advanced on-board diagnostics (OBD) to prevent and detect filter failures and malfunctions. Early detection of upstream (engine-out) malfunctions is paramount to preventing irreversible damage to downstream aftertreatment system components. Such early detection can mitigate the failure of the particulate filter resulting in the escape of emissions exceeding permissible limits and extend the component life. However, despite best efforts at early detection and filter failure prevention, the OBD system must also be able to detect filter failures when they occur. In this paper, radio frequency (RF) sensors were used to directly monitor the particulate filter state of health for both gasoline particulate filter (GPF) and diesel particulate filter (DPF) applications. The testing included controlled engine dynamometer evaluations, which characterized soot slip from various filter failure modes, as well as on-road fleet vehicle tests. The results show a high sensitivity to detect conditions resulting in soot leakage from the particulate filter, as well as potential for direct detection of structural failures including internal cracks and melted regions within the filter media itself. Finally and furthermore, the measurements demonstrate, for the first time, the capability to employ a direct and continuous monitor of particulate filter diagnostics to both prevent and detect potential failure conditions in the field.

42 ENGINEERING↗

NASA NTRS1974

Investigation of land use of northern megalopolis using ERTS-1 imagery

Primary objective was to produce a color-coded land use map and digital data base for the northern third of Megalopolis. Secondary objective was to investigate possible applications of ERTS products to land use planning. Many of the materials in this report already have received national, dissemination as a result of unexpected interest in land use surveys from ERTS. Of special historical interest is the first comprehensive urban-type land use map from space imagery, which covered the entire state of Rhode Island and was made from a single image taken on 28 July 1972.

Simpson, R. B.↗

NASA NTRS1974

Automatic land use classification using Skylab S-192 multispectral data

Investigation of the accuracy attainable in automatic land use classification using 13 bands of multispectral data from the Skylab S-192 scanner. Classification to levels containing seven urban classes, five agricultural, and three water classes is shown to be achievable. With 17 classes, a classification accuracy of 72% was obtained. A wide spectral range, including the thermal band, appears to be most useful for distinguishing urban classes. Agricultural and water classes can be separated using spectral bands covering the visible to far IR.

Kirvida, L.↗

NASA NTRS1976

A methodology for producing small scale rural land use maps in semi-arid developing countries using orbital imagery

The author has identified the following significant results. Results have shown that it is feasible to design a methodology that can provide suitable guidelines for operational production of small scale rural land use maps of semiarid developing regions from LANDSAT MSS imagery, using inexpensive and unsophisticated visual techniques. The suggested methodology provides immediate practical benefits to map makers attempting to produce land use maps in countries with limited budgets and equipment. Many preprocessing and interpretation techniques were considered, but rejected on the grounds that they were inappropriate mainly due to the high cost of imagery and/or equipment, or due to their inadequacy for use in operational projects in the developing countries. Suggested imagery and interpretation techniques, consisting of color composites and monocular magnification proved to be the simplest, fastest, and most versatile methods.

Vangenderen, J. L.↗

NASA NTRS1980

Use of Landsat data in soil and agricultural land use studies

This paper describes how the synoptic, multispectral, and temporal characteristics of Landsat can be used to locate Soil Association boundaries. Then, using these techniques we describe how a low intensity soil survey was conducted and how some interpretive maps were developed from this. Finally, we describe how soil suitability and land use interpretations were made to aid in defining Agrophysical units used in crop inventories.

Westin, F. C.↗

NASA NTRS1981

Use of aerial photography in determining land use and streamflow relationships on small developing watersheds

Using aerial photographs dating back to 1937, the historical trends of five land use classes (crop, forest, open field, urban and suburban) are determined. The relationships between these and various flow regime parameters are investigated. Annual runoff is found to be 7.5 inches greater now than in the year 1932. It is also found that growing season runoff increased by 3.5 inches during the same period. This increase is approximately equivalent to 160 area inches of excess runoff during the 45-year period of observation. The increase in runoff is found to be positively correlated with the percent basin area in the urban, suburban and open field land use classes. A negative correlation is established with forest and crop land. Although poor correlations are found with high flow, low flow, flow interval and flow date data, it is thought that a more precise quantification of land use or a smaller basin area may possibly have yielded more positive results for streamflow timing data.

Owe, M.↗

NASA NTRS1981

Ground water use inventory in Minnesota using LANDSAT data

An irrigation ground water use inventory in Sherburne County, Minnesota, was attempted by indirectly locating irrigation wells by determining the location of irrigated lands. Digital classification of LANDSAT MSS imagery was employed using the IDIMS at Goddard Space Flight Center. Single-date classification proved moderately successful after accurate ground truth data were obtained. A combination of supervised and unsupervised classification was used. Multitemporal analysis using August 10 and May 21, 1978 imagery was also attempted. This unsupervised classification proved most successful in identifying crops and irrigated fields.

Beissel, D. R.↗