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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 379 records · Page 21
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Parts-Per-Million Carbonate Mineral Quantification with Thermogravimetric Analysis–Mass Spectrometry

Mitigating the deleterious effects of climate change requires the development and implementation of carbon capture and storage technologies. To expand the monitoring, verification, and reporting (MRV) capabilities of geologic carbon mineralization projects, we developed a thermogravimetric analysis–mass spectrometry (TGA–MS) methodology to enable quantification of <100 ppm calcite (CaCO 3 ) in complex samples. We extended TGA–MS calcite calibration curves to enable a higher measurement resolution and lower limits of quantification for evolved CO 2 from a calcite–corundum mixture. We demonstrated <100 ppm carbonate mineral quantification with TGA–MS for the first time, an outcome applicable across earth, environmental, and materials science fields. We applied this carbonate quantification method to a suite of Columbia River Basalt Group (CRBG) well cuttings recovered in 2009 from Pacific Northwest National Laboratory’s Wallula #1 Well. Our execution of this new combined calcite and calcite–corundum calibration curve TGA–MS method on our CRBG sample suite indicated average carbonate contents of 0.050 wt % in flow interiors (caprocks) and 0.400 wt % in interflow zones (reservoirs) in the upper 1250 m of the Wallula #1 Well. Finally, by advancing our knowledge of continental flood basalt-hosted carbonates in the mafic subsurface and reaching new TGA–MS quantification limits for carbonate minerals, we expand MRV capabilities and support the commercial-scale deployment of carbon mineralization projects in the Pacific Northwest United States and beyond.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Improvement of circumferential ductility by reducing discontinuities in a high-Mn TWIP steel weldment

Highlights: • This study focused on two key ways to improve expandability of TWIP steel pipe. • The amount of penetrator is remarkably reduced at low PO{sub 2} welding atmosphere. • The effect of PWHT on the morphological change in the bond line was characterized. - Abstract: Recently, high-frequency electrical resistance welded (HF-ERW) pipes have been introduced as an application of high-Mn twinning induced plasticity (TWIP) steels. However, the excellent ductility of the TWIP steels has been underutilized in expandable pipe applications due to discontinuities in the weldment. This work presents two key ways to improve the pipe expandability or circumferential ductility. In-depth microstructural analysis and flaring tests were conducted to identify bond line discontinuities and to evaluate the circumferential ductility. These results indicate that ductility formed to be strongly related to the welding atmosphere and post-weld heat treatment (PWHT) conditions. The welding atmosphere was related to oxide defects, while the PWHT conditions were related to intrinsic discontinuities. The distribution and amount of penetrator defects along the bond line are the main factors related to the deterioration of the circumferential ductility, which is affected by the sheet metal compositions and decreased remarkably at low PO{sub 2} content. We also suggest that PWHT is necessary for improving the ductility by inducing changes in the bond line texture and hardness distribution. The results were verified based on changes in the crack path propagation.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Chemiluminescent Biosensors for Detection of Second Messenger Cyclic di-GMP

Bacteria colonize highly diverse and complex environments, from gastrointestinal tracts to soil and plant surfaces. This colonization process is controlled in part by the intracellular signal cyclic di-GMP, which regulates bacterial motility and biofilm formation. To interrogate cyclic di-GMP signaling networks, a variety of fluorescent biosensors for live cell imaging of cyclic di-GMP have been developed. However, the need for external illumination precludes the use of these tools for imaging bacteria in their natural environments, including in deep tissues of whole organisms and in samples that are highly autofluorescent or photosensitive. The need for genetic encoding also complicates the analysis of clinical isolates and environmental samples. Toward expanding the study of bacterial signaling to these systems, we have developed the first chemiluminescent biosensors for cyclic di-GMP. The biosensor design combines the complementation of split luciferase (CSL) and bioluminescence resonance energy transfer (BRET) approaches. Furthermore, we developed a lysate-based assay for biosensor activity that enabled reliable high-throughput screening of a phylogenetic library of 92 biosensor variants. The screen identified biosensors with very large signal changes (~40- and 90-fold) as well as biosensors with high affinities for cyclic di-GMP ($K_D$ < 50 nM). These chemiluminescent biosensors then were applied to measure cyclic di-GMP levels in $E. coli$. The cellular experiments revealed an unexpected challenge for chemiluminescent imaging in Gram negative bacteria but showed promising application in lysates. Taken together, this work establishes the first chemiluminescent biosensors for studying cyclic di-GMP signaling and provides a foundation for using these biosensors in more complex systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2023

Double DAP-seq uncovered synergistic DNA binding of interacting bZIP transcription factors

Many eukaryotic transcription factors (TF) form homodimer or heterodimer complexes to regulate gene expression. Dimerization of BASIC LEUCINE ZIPPER (bZIP) TFs are critical for their functions, but the molecular mechanism underlying the DNA binding and functional specificity of homo- versus heterodimers remains elusive. To address this gap, we present the double DNA Affinity Purification-sequencing (dDAP-seq) technique that maps heterodimer binding sites on endogenous genomic DNA. Using dDAP-seq we profile twenty pairs of C/S1 bZIP heterodimers and S1 homodimers in Arabidopsis and show that heterodimerization significantly expands the DNA binding preferences of these TFs. Analysis of dDAP-seq binding sites reveals the function of bZIP9 in abscisic acid response and the role of bZIP53 heterodimer-specific binding in seed maturation. The C/S1 heterodimers show distinct preferences for the ACGT elements recognized by plant bZIPs and motifs resembling the yeast GCN4 cis -elements. This study demonstrates the potential of dDAP-seq in deciphering the DNA binding specificities of interacting TFs that are key for combinatorial gene regulation.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2025

Unveiling a pervasive DNA adenine methylation regulatory network in the early-diverging fungus Rhizopus microsporus

Development of the DNA affinity purification and sequencing (DAP-seq) technique has allowed genome-scale studies of transcription factor (TF)-binding sites with high reproducibility. Here, we apply this technique to the human opportunistic pathogen Rhizopus microsporus, a mucoralean fungus belonging to the understudied group of early-diverging fungi. We characterize genome-wide binding sites of 58 TFs encoded by genes regulated through adenine methylation and representing major TF families. This analysis reveals their binding profiles and recognized sequences, expanding and diversifying the catalog of known fungal motifs. By integrating this data with DNA 6-methyladenine profiling, we uncover the extensive direct and indirect impact of this epigenetic modification on the regulation of gene expression. Furthermore, we use the generated data to identify TFs involved in biologically relevant processes such as zinc metabolism and light response. Our work enhances our understanding of regulatory mechanisms in R. microsporus and provides broader insights into gene regulation across the fungal kingdom.

Lax, Carlos [Universidad de Murcia (Spain)] (ORCID↗
DOE OSTI2024

On the detectability of the moving lens signal in CMB experiments

Abstract Upcoming cosmic microwave background (CMB) experiments are expected to detect new signals probing interaction of CMB photons with intervening large-scale structure. Among these the moving-lens effect, the CMB temperature anisotropy induced by cosmological structures moving transverse to our line of sight, is anticipated to be measured to high significance in the near future. In this paper, we investigate two possible strategies for the detection of this signal: pairwise transverse-velocity estimation and oriented stacking. We expand on previous studies by including in the analysis realistic simulations of competing signals and foregrounds. We confirm that the moving lens effect can be detected at ≥ 10σlevel by a combination of CMB-S4 and LSST surveys. We show that the limiting factors in the detection depend on the strategy: for the stacking analysis, correlated extragalactic foregrounds, namely the cosmic infrared background and thermal Sunyaev Zel'dovich effect, play the most important role. The addition of foregrounds make the signal-to-noise ratio be most influenced by large and nearby objects. As for the pairwise detection, halo lensing and pair number counts are the main issues. In light of our findings, we elaborate on possible strategies to improve the analysis approach for the moving lens detection with upcoming experiments. We also deliver to the community all the simulations and tools we developed for this study.

Astronomy & Astrophysics↗
DOE OSTI2020

Pump-induced motion of an interface between competing orders

In this work, we study the motion of an interface separating two regions with different electronic orders following a short-duration pump that drives the system out of equilibrium. Using a generalized Ginzburg-Landau approach and assuming that the main effect of the nonequilibrium drive is to transiently heat the system we address the question of the direction of interface motion—in other words, which ordered region expands and which contracts after the pump. Our analysis includes the effects of differences in free-energy landscape and in order parameter dynamics and identifies circumstances in which the drive may act to increase the volume associated with the subdominant order, for example when the subdominant order has a second-order free-energy landscape while the dominant order has a first-order one.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2025

Scanning transmission x-ray microscopy (STXM) of plutonium oxide

Scanning transmission x-ray microscopy was used to examine plutonium oxide particles formed by the corrosion of δ-phase plutonium alloy under high-humidity conditions. O K-edge spectra collected from eight distinct particles displayed significant spectral differences, revealing heterogeneity in oxidation states within a single sample batch. Here, this variation suggests complex chemical environments and formation histories, which are important considerations for nuclear forensic investigations. These findings highlight both the potential of synchrotron-based x-ray microscopy for nondestructive, high-resolution analysis of nuclear materials and the need for expanded reference datasets to improve the interpretation and forensic utility of such measurements.

organic↗
DOE OSTI2017

UNREVIEWED DISPOSAL QUESTION EVALUATION: Development of Inventory Screening Limits for the Area 5 Radioactive Waste Management Site, Nevada National Security Site, Nye County, Nevada

This Unreviewed Disposal Question Evaluation estimates the inventory of specific radionuclides that represent negligible risk for the Area 5 Radioactive Waste Management Site on the Nevada National Security Site. Radionuclides exceeding these screening limits are candidates for entry into the performance assessment and composite analysis model. Screening limits are developed for an expanded list of radionuclides. The screening limits are estimated as the total site inventory that would cause a receptor to receive 1/1000th of the 0.1 milliseivert (mSv) air pathway or 0.25 mSv all-pathways performance objectives. The receptor is assumed to be exposed to undiluted waste for a period of one year.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2020

Slycat Enables Synchronized 3D Comparison of Surface Mesh Ensembles [Brief]

In support of analyst requests for Mobile Guardian Transport studies, researchers at Sandia National Laboratories have expanded data types for the Slycat ensemble-analysis and visualization tool to include 3D surface meshes. This new capability represents a significant advance in our ability to perform detailed comparative analysis of simulation results. Analyzing mesh data rather than images provides greater flexibility for post-processing exploratory analysis.

36 MATERIALS SCIENCE↗
NASA NTRS1978

Remarks on future computational aerodynamics requirements

The development of upgraded and expanded computational aerodynamics methods for the design and analysis of aircraft configurations should be performed by both government and industry to ensure that the objectives for aircraft design are satisfied from both the industrial competitive design standpoint and from the government standpoint. Any programs developed must be heavily user-oriented and provide maximum visibility and creditability to management. Early consideration should be given to the adequate management of such a facility when it becomes available.

Bradley, R. G.↗
NASA NTRS1987

Computer-aided analysis for the Mechanics of Granular Materials (MGM) experiment, part 2

Computer vision based analysis for the MGM experiment is continued and expanded into new areas. Volumetric strains of granular material triaxial test specimens have been measured from digitized images. A computer-assisted procedure is used to identify the edges of the specimen, and the edges are used in a 3-D model to estimate specimen volume. The results of this technique compare favorably to conventional measurements. A simplified model of the magnification caused by diffraction of light within the water of the test apparatus was also developed. This model yields good results when the distance between the camera and the test specimen is large compared to the specimen height. An algorithm for a more accurate 3-D magnification correction is also presented. The use of composite and RGB (red-green-blue) color cameras is discussed and potentially significant benefits from using an RGB camera are presented.

Parker, Joey K.↗
NASA NTRS1993

The 3-D Moons: The Voyager stereo atlas of the outer solar system

Comprehension and analysis of geologic features on any planet is enhanced manyfold by a clear perception between albedo and topography. On many of the icy satellites significant albedo contrasts due to mixtures of dark rocky and bright icy materials can be associated with topographic features. Subtle topographic features can be masked by albedo variation and under high solar illumination albedo and topography can be difficult to separate. To this end we are compiling an atlas of stereo image pairs of the outer solar system based on Voyager imaging for the investigation of various geologic problems and for general use. For the icy satellites, general perceptions of topography are usually gleaned from shape-from-shading information in the images processed by the human brain (i.e. visual inspection). With few exceptions, actual topography has been measured on a spot-by-spot basis using shadow heights or photoclinometry, or along limb profiles (where geographic context may be unavailable). Shadow heights are limited to regions within approximately 10 deg of the terminator and images with resolution better than approximately 1 km/pixel. Photoclinometric scans can be used more widely but are subject to a variety of errors, primarily uncertain assumptions of uniform scene albedo or poorly understood photometry. Stereoscopic analysis, where available, has the potential for greatly expanding topographic perception.

Schenk, P.↗
NASA NTRS2001

Comparison of X-31 Flight and Ground-Based Yawing Moment Asymmetries at High Angles of Attack

Significant yawing moment asymmetries were encountered during the high-angle-of-attack envelope expansion of the two X-31 aircraft. These asymmetries caused position saturations of the thrust-vectoring vanes and trailing-edge flaps during some stability-axis rolling maneuvers at high angles of attack. The two test aircraft had different asymmetry characteristics, and ship two has asymmetries that vary as a function of Reynolds number. Several aerodynamic modifications have been made to the X-31 forebody with the goal of minimizing the asymmetry. These modifications include adding transition strips on the forebody and noseboom, using two different length strakes, and increasing nose bluntness. Ultimately, a combination of forebody strakes, nose blunting, and noseboom transition strips reduced the yawing moment asymmetry enough to fully expand the high-angle-of-attack envelope. Analysis of the X-31 flight data is reviewed and compared to wind-tunnel and water-tunnel measurements. Several lessons learned are outlined regarding high-angle-of-attack configuration design and ground testing.

Cobleigh, Brent R.↗
NASA NTRS2003

Comparison of X-31 Flight and Ground-Based Yawing Moment Asymmetries at High Angles of Attack

Significant yawing moment asymmetries were encountered during the high-angle-of-attack envelope expansion of the two X-31 aircraft. These asymmetries caused position saturations of the thrust-vectoring vanes and trailing-edge flaps during some stability-axis rolling maneuvers at high angles of attack. The two test aircraft had different asymmetry characteristics, and ship 2 has asymmetries that vary as a function of Reynolds number. Several aerodynamic modifications have been made to the X-31 forebody with the goal of minimizing the asymmetry. These modifications include adding transition strips on the forebody and noseboom, using two different length strakes, and increasing nose bluntness. Ultimately, a combination of forebody strakes, nose blunting, and noseboom transition strips reduced the yawing moment asymmetry enough to fully expand the high-angle-of-attack envelope. Analysis of the X-31 flight data is reviewed and compared to wind-tunnel and water-tunnel measurements. Several lessons learned are outlined regarding high-angle-of-attack configuration design and ground testing.

Cobleigh, Brent↗
NASA NTRSDate not supplied

Flight Testing of In-Time Safety Assurance Technologies for UAS Operations

Ongoing research at NASA is driven by a strategic plan defined by the Aeronautics Research Mission Directorate and a vision for future In-Time Aviation Safety Management Systems (IASMS) as described by the National Academies. In both visions, system safety awareness and provision are expanded through increased access to relevant data; integrated analysis and predictive capabilities; improved real-time detection and alerting of domain-specific hazards; decision support, and in some cases, automated risk mitigation strategies. One primary research focus is to develop means by which more timely (i.e., “in-time”) actions may be taken to mitigate precursors, anomalies, or trends that are observed during operations. In this paper, we describe such means as a collection of Services, Functions, and Capabilities (SFCs) that are supported by an underlying information system. For example, an integrated risk assessment capability is envisioned that continuously monitors safety-related metrics and margins and recommends timely operational changes. Assessment functions and/or services can be based on data analytics and predictive models derived from heterogeneous data sets that span relevant indicator metrics and their time histories. Likewise, on-board functions can identify and reduce susceptibility to precursor conditions that have led (and can lead) to aircraft loss-of-control or out-of-control accidents. This paper summarizes development and testing of such an information system tailored to hazards anticipated for future highly autonomous flight missions near and over densely populated areas. Testing is accomplished via simulation and by using small, unmanned aircraft operating over a test range at NASA’s Langley Research Center. Flight plans and test scenarios are defined to emulate several use-cases, including package delivery; reconnaissance; fire management; and urban air taxi vertiport operations. Two test phases are summarized with Phase 1 occurring in (2019-2020) and Phase 2 ongoing (2021-present). Results focus on SFC performance, technology readiness level assessment, and requirements discovery/validation. Companion papers are cited throughout for additional details on the recent testing.

safety management↗
NASA NTRSDate not supplied

Keywords for All People: How Keyword Governance and Coordination with the NASA ESDIS Standards Coordination Office (ESCO) Improves GCMD Keywords for Discuvery and Use

The Global Change Master Directory (GCMD) Keywords, initiated over twenty years ago, are a hierarchical set of controlled Earth Science vocabularies that help ensure Earth science data, services, and variables are described in a consistent and comprehensive manner and allow for the precise searching of metadata and subsequent retrieval of data, services, and variables. GCMD keywords are periodically analyzed for relevancy and will continue to be refined and expanded in response to user needs. The periodic analysis is a result of successful coordination with the ESDIS Standards Coordination Office (ESCO), which is responsible for standards activities across ESDIS, and assists with providing valuable stakeholder and subject matter expert (SME) feedback on GCMD vocabularies. The ESCO is also turning to the GCMD to discuss how the keyword review process can be improved and more streamlined. In addition to the ESCO, keyword requests and feedback are also received through the GCMD Keyword Forum.

Tyler Stevens↗
NASA NTRS2023

General Services Administration Reclamation Yard Solid Waste Management Unit 010: 2022 Groundwater Monitoring Report Kennedy Space Center, Florida

This report presents a summary of the groundwater monitoring activities that occurred in September and October 2022 at General Services Administration Reclamation Yard, Solid Waste Management Unit 010, located at the John F. Kennedy Space Center (KSC), Florida. The site is monitored under KSC’s Resource Conservation and Recovery Act Corrective Action Program. This approach also meets the requirements of Chapter 62-780, Florida Administrative Code. For the purposes of this report, two separate plumes, known as the Polychlorinated Biphenyl (PCB)/Volatile Organic Aromatic (VOA) Plume and the Chlorinated Volatile Organic Compound (VOC) Plume, were identified for this site. The contaminants of concern (COCs) for the PCB/VOA Plume consist of PCBs, 1,2,4-trichlorobenzene, and breakdown products of 1,2,4-trichlorobenzene. The COCs for the Chlorinated VOC Plume were tetrachloroethene, trichloroethene, cis-1,2-dichloroethene, and vinyl chloride. Groundwater monitoring for VOCs in the Chlorinated VOC Plume area was discontinued following the December 2021 annual monitoring event. Annual groundwater monitoring for underground injection control (UIC) parameters continues for both the PCB/VOA Plume and the Chlorinated VOC Plume areas. The activities presented in this report include one field event: September and October 2022, which includes sitewide semi-annual water level measurements of 55 monitoring wells, redevelopment of all monitoring wells listed in the sampling plan, and groundwater sampling of 28 monitoring wells. The sampling and analysis demonstrated that the PCB/VOA plume is not expanding and is significantly reduced compared to before a 2018 source removal interim measure. Recommendations are made for the 2023 groundwater monitoring program.

groundwater↗