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At least 397 records · Page 22

Two-phase choked flow of cryogenic fluids in converging-diverging nozzles

Data are presented for the two phase choked flow of three cryogenic fluids - nitrogen, methane, and hydrogen - in four converging-diverging nozzles. The data cover a range of inlet stagnation conditions, all single phase, from well below to well above the thermodynamic critical conditions. In almost all cases the nozzle throat conditions were two phase. The results indicate that the choked flow rates were not very sensitive to nozzle geometry. However, the axial pressure profiles, especially the throat pressure and the point of vaporization, were very sensitive to both nozzle geometry and operating conditions. A modified Henry-Fauske model correlated all the choked flow rate data to within + or - 10 percent. Neither the equilibrium model nor the Henry-Fauske model predicted throat pressures well over the whole range of data. Above the thermodynamic critical temperature the homogeneous equilibrium model was preferred for both flow rate and pressure ratio. The data of the three fluids could be normalized by the principle of corresponding states.

Simoneau, R. J.↗

Passive components for high temperature operation

The development of resistors, capacitors, and interconnect metalizations utilizing a low pressure chemical vapor deposition (LPCVD) process is described. The LPCVD process allows the passive components to be fabricated at temperatures higher than their highest operating temperatures. The deposition of thin films by LPCVD is accomplished by reacting one or more gases on the surface of a heated substrate. The substrates to be coated are placed on a graphite susceptor and then loaded into the center of a quartz reaction tube. The RF power is applied to the coil on the outside of the reaction tube which in turn is coupled into the graphite susceptor causing it to heat. Pressures of several torr or less are typical, with carrier flow rates of 0.1 to 2.0 liters/min. Nitrogen, hydrogen, and helium are typical carrier gases. These are controlled with mass flow controllers and the pressure is continuously monitored with a capacitive manometer. Materials selection and device testing are also discussed.

Raymond, L. S.↗

Numerical simulation of an atmospheric pressure plasma jet with coaxial shielding gas

A two-dimensional ( r, z ) numerical simulation of the discharge characteristics of an atmospheric pressure plasma jet (APPJ), with coaxial shielding gas, was performed. The helium working gas flowed in a central capillary tube, engulfing a needle electrode powered by 13.7 MHz radio frequency sinusoidal voltage. The N 2 shielding gas flowed in the annular space of a coaxial tube. These gases emerged, in laminar flow, in a 78%N 2 -21%O 2 -1%Ar dry air ambient. The characteristics of the APPJ with shielding gas were compared to those of the APPJ without shielding gas. The nitrogen shielding gas hindered the diffusion of oxygen and argon from the ambient air into the helium jet. With the shielding gas present, more nitrogen penetrated into the helium core, causing a shorter plasma ‘plume’. The flow rates of the working and shielding gas, critically affected the gas temperature, and in turn the discharge characteristics. For a He flow of 2 standard liters per minute (slm), switching on the nitrogen shielding gas flow (at 4.5 slm) reduced the on-axis O 2 and Ar mole fractions from 3.9 × 10 - 4 to 6.8 × 10 - 5 and from 1.9 × 10 - 5 to 3.3 × 10 - 6 , respectively, at an axial distance of 3 mm downstream of the nozzle. The radial profiles of the mole fractions of the ambient gases were monotonically and strongly decreasing towards the system axis, for short axial distances from the nozzle (~1 mm), but became progressively flatter at longer distances from the nozzle (3 mm and 5 mm). Simulation predictions captured the salient features of experimental data of ambient species mole fractions in the plasma jet, and the 706 nm optical emission intensity profiles of the He 3 3 S excited state.

Physics↗

Flame Design: A Novel Approach Developed to Produce Clean, Efficient Diffusion Flames

Soot formation and flame extinction are vital concerns in the combustion of fossil fuels. In particular, soot is responsible for pollutant emissions, and extinction can cause inefficient or unstable burning. Normal-gravity experiments have demonstrated that flames can be designed to improve both characteristics by redirecting some or all of the nitrogen from the oxidizer into the fuel. Such nitrogen exchange can produce permanently blue flames, which are soot free under all possible flame conditions. Furthermore, this approach can lead to stronger, extinction-resistant flames. Past investigations of nitrogen exchange were unable to identify the physical mechanisms responsible for its benefits because these mechanisms cannot be isolated when normal-gravity flames are studied. In contrast, the Diffusion Flame Extinction and Soot Inception (DESI) experiment considers spherical flames, where nearly perfect spherical symmetry affords new levels of control. Because of buoyancy, spherical flames cannot be created in Earth s gravity. DESI was conceived by principal investigator Professor R.L. Axelbaum of Washington University in St. Louis. Tests to date have utilized the 2.2-Second Drop Tower at the NASA Glenn Research Center at Lewis Field. The experiment is slated for testing aboard the International Space Station in a few years. Two mechanisms have been proposed to explain the connection between nitrogen exchange and permanently blue flames. These are the structure (chemical effects) and hydrodynamics (flow direction and speed). In normal-gravity flames, the structure and hydrodynamics are coupled, since nitrogen exchange simultaneously modifies both. Spherical microgravity flames, on the other hand, allow independent control of these factors. Specifically, structure can be modified via nitrogen exchange, and flow direction can be reversed by swapping the ambient and burner-feed gases. In DESI, these variations can be accomplished without changing the theoretical flame temperature.

Axelbaum, Richard L.↗

Density measurements in an expanding flow using holographic interferometry

A nonequilibrium expansion of nitrogen through a 2-dimensional nozzle of a reflected shock tunnel is investigated with laser holography, time resolved pressure measurements and emission spectroscopy to characterize the flow field for vibrational relaxation measurements. A 2D computation is used to simulate the nozzle flow field. Synthetic holograms are generated using the computed density profiles and are compared with the experimental holograms. Also, using a quasi 1-D approximation, populations for each vibrational level are computed by (1) solving the master equations and (2) using the Landau-Teller formulation. Computational accuracy of both models is assessed against the experimental data.

Sharma, Surendra P.↗

Calculation of eddy viscosity in a compressible turbulent boundary layer with mass injection and chemical reaction, volume 1

The turbulent kinetic energy equation is coupled with boundary layer equations to solve the characteristics of compressible turbulent boundary layers with mass injection and combustion. The Reynolds stress is related to the turbulent kinetic energy using the Prandtl-Wieghardt formulation. When a lean mixture of hydrogen and nitrogen is injected through a porous plate into the subsonic turbulent boundary layer of air flow and ignited by external means, the turbulent kinetic energy increases twice as much as that of noncombusting flow with the same mass injection rate of nitrogen. The magnitudes of eddy viscosity between combusting and noncombusting flows with injection, however, are almost the same due to temperature effects, while the distributions are different. The velocity profiles are significantly affected by combustion; that is, combustion alters the velocity profile as if the mass injection rate is increased, reducing the skin-friction as a result of a smaller velocity gradient at the wall. If pure hydrogen as a transpiration coolant is injected into a rocket nozzle boundary layer flow of combustion products, the temperature drops significantly across the boundary layer due to the high heat capacity of hydrogen. At a certain distance from the wall, hydrogen reacts with the combustion products, liberating an extensive amount of heat. The resulting large increase in temperature reduces the eddy viscosity in this region.

Omori, S.↗

Calculation of eddy viscosity in a compressible turbulent boundary layer with mass injection and chemical reaction

The turbulent kinetic energy equation is coupled with boundary layer equations to solve the characteristics of compressible turbulent boundary layers with mass injection and combustion. The Reynolds stress is related to the turbulent kinetic energy using the Prandtl-Wieghardt formulation. When a lean mixture of hydrogen and nitrogen is injected through a porous plate into the subsonic turbulent boundary layer of air flow and ignited by external means, the turbulent kinetic energy increases twice as much as that of noncombusting flow with the same mass injection rate of nitrogen. The magnitudes of eddy viscosity between combusting and noncombusting flows with injection, however, are almost the same due to temperature effects, while the distributions are different. The velocity profiles are significantly affected by combustion. If pure hydrogen as a transpiration coolant is injected into a rocket nozzle boundary layer flow of combustion products, the temperature drops significantly across the boundary layer due to the high heat capacity of hydrogen. At a certain distance from the wall hydrogen reacts with the combustion products, liberating an extensive amount of heat.

Omori, S.↗

Design and test of porous-tungsten mercury vaporizers

Future use of large size Kaufman thrusters and thruster arrays will impose new design requirements for porous plug type vaporizers. Larger flow rate coupled with smaller pores to prevent liquid intrusion will be desired. The results of testing samples of porous tungsten for flow rate, liquid intrusion pressure level, and mechanical strength are presented. Nitrogen gas was used in addition to mercury flow for approximate calibration. Liquid intrusion pressure levels will require that flight thruster systems with long feed lines have some way (a valve) to restrict dynamic line pressures during launch.

Kerslake, W. R.↗

Quantitative Spectral Radiance Measurements in the HYMETS Arc Jet

Calibrated spectral radiance measurements of gaseous emission spectra have been obtained from the HYMETS (Hypersonic Materials Environmental Test System) 400 kW arc-heated wind tunnel at NASA Langley Research Center. A fiber-optic coupled spectrometer collected natural luminosity from the flow. Spectral radiance measurements are reported between 340 and 1000 nm. Both Silicon Carbide (SiC) and Phenolic Impregnated Carbon Ablator (PICA) samples were placed in the flow. Test gases studied included a mostly-N2 atmosphere (95% nitrogen, 5% argon), a simulated Earth Air atmosphere (75% nitrogen, 20% oxygen, 5% argon) and a simulated Martian atmosphere (71% carbon dioxide, 24% nitrogen, 5% argon). The bulk enthalpy of the flow was varied as was the location of the measurement. For the intermediate flow enthalpy tested (20 MJ/kg), emission from the Mars simulant gas was about 10 times higher than the Air flow and 15 times higher than the mostly-N2 atmosphere. Shock standoff distances were estimated from the spectral radiance measurements. Within-run, run-to-run and day-to-day repeatability of the emission were studied, with significant variations (15-100%) noted.

Danehy, Paul M.↗

Effects of various assumptions on the calculated liquid fraction in isentropic saturated equilibrium expansions

The saturated equilibrium expansion approximation for two phase flow often involves ideal-gas and latent-heat assumptions to simplify the solution procedure. This approach is well documented by Wegener and Mack and works best at low pressures where deviations from ideal-gas behavior are small. A thermodynamic expression for liquid mass fraction that is decoupled from the equations of fluid mechanics is used to compare the effects of the various assumptions on nitrogen-gas saturated equilibrium expansion flow starting at 8.81 atm, 2.99 atm, and 0.45 atm, which are conditions representative of transonic cryogenic wind tunnels. For the highest pressure case, the entire set of ideal-gas and latent-heat assumptions are shown to be in error by 62 percent for the values of heat capacity and latent heat. An approximation of the exact, real-gas expression is also developed using a constant, two phase isentropic expansion coefficient which results in an error of only 2 percent for the high pressure case.

Bursik, J. W.↗

WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Surface Water FTICR-MS, NPOC, TN, Anions, Stable Isotopes, Bacterial Abundance, and Dissolved Inorganic Carbon (v8)

The WHONDRS Summer 2019 Sampling (S19S) Campaign collected samples in 97 globally distributed river corridor systems between July and September 2019. Surficial streambed sediments were collected at three locations within each site (upstream, midstream, and downstream). Surface water was collected at the downstream site. This dataset includes a portion of the data types produced from the surface water samples and does not include any results from the sediment. Sediment data can be found at https://data.ess-dive.lbl.gov/view/doi:10.15485/1729719. The S19S campaign was designed with the science community to ask questions associated with links among core/transient metabolomes, microbial metabolism, biogeochemical function, and physical properties of watershed and river corridor systems. This data package was originally published in March 2020. It was updated in October 2020 (v2, new and modified files), July 2021 (v3, new and modified files), January 2023 (v4, new and modified files), February 2023 (v5, new and modified files), August 2023 (v6, new and modified files), July 2025 (v7,new and modified files), and August 2026 (v8, new and modified files). Version 8 includes major restructuring of the files and their formats. See the change history section in readme for more details. In addition to a readme, this data package also includes a file-level metadata (FLMD) file that describes each file and a data dictionary (DD) that describes all column/row headers and variable definitions. This dataset contains (1) readme, (2) data dictionary, (3) file level metadata, (4) sampling protocol, (5) a data checks report, (6) field metadata, (7) international generic sample number (IGSN) mapping file, (8) joint genome institute (JGI) mapping file, and (9) a folder of sample data. The sample data folder contains (1) dissolved organic carbon (DOC, measured as non-purgeable organic carbon, NPOC) and FTICR methods, (2) dissolved inorganic carbon (DIC), (3) stable water isotopes (O and H), (4) specific conductivity, (5) total dissolved nitrogen (TN), (6) anions, (7) flow cytometry bacterial abundance data, (8) laboratory methods, and (9) a folder containing unaligned, peak-picked high resolution characterization of dissolved organic matter from sediment via 12 Tesla Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) through the Environmental Molecular Sciences Laboratory (EMSL, https://www.pnnl.gov/environmental-molecular-sciences-laboratory), and (12) a folder containing processed FTICR-MS data. All files are .msa, .txt, .spx, .xml, .csv, .pdf, .txt, .html, .jpg, or .jpeg.

18-O↗

Effect of gas mass flux on cryogenic liquid jet breakup

A scattered-light scanning instrument developed at NASA Lewis Research Center was used to measure the characteristic drop size of clouds of liquid nitrogen droplets. The instrument was calibrated with suspensions of monosized polystyrene spheres. In this investigation of the mechanism of liquid nitrogen jet disintegration in a high-velocity gas flow, the Sauter mean diameter, D32, was found to vary inversely with the nitrogen gas mass flux raised to the power 1.33. Values of D32 varied from 5 to 25 microns and the mass flux exponent of 1.33 agrees well with theory for liquid jet breakup in high-velocity gas flows. The loss of very small droplets due to the high vaporization rate of liquid nitrogen was avoided by sampling the spray very close to the atomizer, i.e., 1.3 cm downstream of the nozzle orifice. The presence of high velocity and thermal gradients in the gas phase also made sampling of the particles difficult. As a result, it was necessary to correct the measurements for background noise produced by both highly turbulent gas flows and thermally induced density gradients in the gas phase.

Ingebo, R. D.↗

Case Study of Using Flocad to Model a Ground Test Station Ln2 Heat Exchanger

This paper presents a case study of using FLOCAD to model the heat transfer and boiling flow behavior of a Liquid Nitrogen (LN2) ground station equipment heat exchanger. The unique aspect of this work is that is one of very few studies documenting the use of FLOCAD in the spacecraft thermal control community. The results of the simulations described herein were used to guide and plan the execution of thermal vacuum testing spacecraft hardware using a ground test heat exchanger such as the one modeled herein. The paper will review the theory of two-phase boiling flow and correlations used by SINDA/FLUINT as well as the terminology and nomenclature used within Thermal Desktop / FLOCAD regarding two-phase boiling flow heat transfer modeling and simulation. Results for using the ground station heat exchanger as a heat sink in a thermal vacuum test set up are shown in order to demonstrate the set-up and execution of a typical FLOCAD model. Results indicate that properly modeling of the two-phase behavior is critical in order to ascertain the time constant associated with the heat exchanger, as well as understanding the temperature distribution across the test equipment and prediction of required LN2 flowrates to be used during testing. The paper is meant to augment the FLOCAD user’s manual and serve as a tutorial for thermal engineers and analysts wishing to learn and apply FLOCAD to industrial problems.

Anderson, Kevin R.↗

A method for generating quantitative vapor-phase infrared spectra of solids: results for phenol, camphor, menthol, syringol, dicyclopentadiene and naphthalene

Here, a method is presented to generate quantitative vapor-phase infrared spectra from substances that naturally occur as solids with moderate volatility. The solid is gravimetrically dissolved into a solvent that has few infrared spectral features, typically CS 2 and CCl 4 separately. The solution is flowed at a constant rate from a linearly pumped syringe into a metered stream of nitrogen carrier gas regulated by a mass flow controller. The analyte/solvent mix is flash vaporized by volatilizing the solution across a heated stainless-steel surface as it emanates from the syringe tip. The N 2 gas-solution mixture is flowed into a long-path White cell thermostatted at a desired temperature, the long optical path compensating for the modest analyte mixing ratio. A composite spectrum is generated from typically ten or more 760-Torr pressure-broadened spectra over the 600 to 6500 cm -1 spectral range at 0.1 cm -1 spectral resolution. The solid analytes reported here using this novel technique include dicyclopentadiene, menthol, syringol, phenol, camphor, and naphthalene.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Laser-induced fluorescence technique for velocity field measurements in subsonic gas flows

A nonintrusive optical technique is reported for multiple-point velocity measurements in subsonic flows. The technique is based on the detection of fluorescence from a Doppler-shifted absorption line of seeded iodine molecules excited at a laser frequency fixed in the wing of the line. Counterpropagating laser sheets are used to illuminate the flow, in the present case a nitrogen round jet, thereby eliminating the need for an unshifted reference signal. The fluorescence is detected simultaneously at 10,000 points in a plane of the flow using a 100 x 100 element photodiode-array camera. The velocity at each point is computed from four successive camera frames, each recorded with a different beam direction. The measured mean velocities between 5 and 50 m/sec agree well with data from the literature.

Hiller, B.↗

Nitrogen precooling heat exchanger replacement and control system upgrade in superfluid cryoplant at CMTF

Liquid nitrogen precooling is used in most cryoplants to achieve cooldown to 80 K temperature range. In one such system at Fermilab’s CMTF superfluid cryoplant, where the helium supply directly exchanges heat with liquid nitrogen, freezing of nitrogen occurred inside the heat exchanger due to heat exchanger flow imbalance during a cryoplant trip. Trapped vapor pockets of nitrogen within the frozen heat exchanger channels were formed while warming up the heat exchanger, creating high localized pressure and subsequent damage/rupture of the heat exchanger. Replacement of the heat exchanger was done, and modifications were made in the system to rectify future occurrences. The control system was updated to bypass the heat exchanger entirely if the incoming helium stream temperature drops below 76 K. This was done by repurposing two control valves as heat exchanger bypass valves that were previously used for a redundant 80 K adsorber in the coldbox. Additional modifications were made to further prevent return of large amount of cold helium gas from cold end during abrupt cryoplant shutdown. This modification has ensured high reliability of heat exchanger with prevention of freezing of nitrogen which can damage the heat exchanger.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗